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    Walking beam furnace
    21.
    发明授权
    Walking beam furnace 失效
    步行梁炉

    公开(公告)号：US4330262A

    公开(公告)日：1982-05-18

    申请号：US166684

    申请日：1980-07-01

    Applicant: Franz A. Kranzl ,  Helmut Springer

    Inventor： Franz A. Kranzl ,  Helmut Springer

    IPC: F27B9/20 ,  F27D1/16 ,  B65G25/00 ,  F27B9/14

    CPC classification number: F27B9/203

    Abstract: The invention relates to a walking beam furnace, the hearth of which consists, at least partially, of longitudinal beams arranged side by side and alternately formed as fixed beams and walking beams. Each walking beam is lifted and lowered with the aid of lifting rollers, which run on ramps. The ramps are prolonged downwards by a longer distance than is required for the working lift of the walking beams. The walking beams are depressed, step by step, into a repair and maintenance plane which lies appreciably below the plane of the hearth, by moving down the lifting rollers into the region of the lower prolongation of the ramps. For this purpose, a lifting rod which connects all the lifting rollers belonging to a walking beam, is connected to an associated actuating cylinder via a pivotally movable perforated arm mounted at a fixed point, the lifting rod being extended piece by piece by means of extension sections and with the aid of a holding device, and being in each case reinserted into a lower hole in the perforated arm.

    Abstract translation: 本发明涉及一种步进梁炉，其炉膛至少部分地包括并排布置的纵向梁，并且交替地形成为固定梁和步进梁。 借助于在斜坡上运行的提升辊，每个步进梁被提升和降低。 坡道比步行梁的工作电梯所需的距离更长，向下延伸。 通过将升降辊向下移动到斜坡下延伸的区域，步进梁被逐步地压入维修和维护平面，该维修和维护平面明显地低于炉床平面。 为此，将属于步进梁的所有提升辊连接的提升杆通过安装在固定点处的可枢转移动的穿孔臂连接到相关联的致动缸，提升杆通过延伸件逐个延伸 并且借助于保持装置，并且在每种情况下重新插入穿孔臂的下孔中。

    Process for preparing methyl-nonyl-acetaldehyde
    22.
    发明授权
    Process for preparing methyl-nonyl-acetaldehyde 失效
    制备甲基壬基乙醛的方法

    公开(公告)号：US4263460A

    公开(公告)日：1981-04-21

    申请号：US106299

    申请日：1979-12-21

    Applicant: Jurgen Weber ,  Helmut Springer

    Inventor： Jurgen Weber ,  Helmut Springer

    IPC: C07C45/00 ,  C07C45/50 ,  C07C45/62 ,  C07C45/75 ,  C07C47/02 ,  C07C47/21 ,  C07C67/00 ,  C07C47/06

    CPC classification number: C07C47/02 ,  C07C45/50 ,  C07C45/62 ,  C07C45/75

    Abstract: In a process for preparing methyl-nonyl-acetaldehyde from undecanal and formaldehyde or a source of formaldehyde, e.g., a substance which forms formaldehyde, in the presence of catalytic amounts of a secondary amine, the improvement whereinA. the undecanal is used in the form of the reaction mixture obtained by hydroformylation of 1-decene, andB. di-n-butylamine is used as the catalyst,C. the molar ratio of catalyst to undecanal is 0.025 to 0.050 to 1,D. the reaction is carried out at 90.degree. to 100.degree. C., andE. the 2-methylene-undecanal formed is then converted by partial hydrogenation into methyl-nonyl-acetaldehyde.

    Abstract translation: 在催化量的仲胺存在下，从十一醛和甲醛或甲醛源（例如形成甲醛的物质）制备甲基壬基乙醛的方法中，其中A.十一烷醛用于 使用通过1-癸烯的加氢甲酰化获得的反应混合物的形式和B.二正丁胺作为催化剂，C.催化剂与十一烷醛的摩尔比为0.025〜0.050〜1，D反应 在90℃至100℃，然后将形成的2-亚甲基 - 十一烷醛通过部分氢化转化成甲基 - 壬基乙醛。

    Catalytic process for preparing aliphatic straight-chain and β-alkyl-branched carboxylic acids
    23.
    发明授权
    Catalytic process for preparing aliphatic straight-chain and β-alkyl-branched carboxylic acids 有权
    用于制备脂族直链和/或烷基支链羧酸的催化方法

    公开(公告)号：US07799945B2

    公开(公告)日：2010-09-21

    申请号：US11787868

    申请日：2007-04-18

    Applicant: Helmut Springer

    Inventor： Helmut Springer

    IPC: C07C51/235

    CPC classification number: C07C51/235 ,  C07C53/126

    Abstract: A catalytic process for preparing aliphatic straight-chain and β-alkyl-branched carboxylic acids of 5 to 13 carbon atoms by catalytic oxidation of the corresponding aldehydes by means of oxygen or oxygen-containing gas mixtures in the liquid phase in the presence of a catalyst system contains alkali metal carboxylates or alkaline earth metal carboxylates or a mixture thereof in an amount, calculated as alkali metal or alkaline earth metal, of 0.5 mmol to 15 mmol per mol of aldehyde used and also metals of groups 4 to 12 of the Periodic Table of the Elements, cerium or lanthanum in amounts of not more than 5 ppm, based on the aldehyde used, or compounds of such metals, with the catalyst system being the reaction product from an aldehyde oxidation reaction.

    Abstract translation: 通过在液相存在下通过含氧或含氧气体混合物的相应醛催化氧化制备具有5至13个碳原子的脂族直链和/或 - 烷基支链羧酸的催化方法 催化剂体系含有碱金属或碱土金属的碱金属羧酸盐或碱土金属羧酸盐或其混合物，其量为碱金属或碱土金属计算，每摩尔使用的醛为0.5mmol至15mmol，以及周期表中第4至12族的金属 表中的元素，铈或镧的量不大于5ppm，基于所使用的醛，或这些金属的化合物，催化剂体系是醛醛氧化反应的反应产物。

    3(4),7(8)-Dihydroxymethylbicyclo[4,3,0]nonane and a process for its preparation
    24.
    发明申请
    3(4),7(8)-Dihydroxymethylbicyclo[4,3,0]nonane and a process for its preparation 审中-公开
    3（4），7（8） - 二羟甲基双环[4,3,0]壬烷及其制备方法

    公开(公告)号：US20070179323A1

    公开(公告)日：2007-08-02

    申请号：US11657771

    申请日：2007-01-25

    Applicant: Helmut Springer ,  Paolo Bavaj

    Inventor： Helmut Springer ,  Paolo Bavaj

    IPC: C07C35/20

    CPC classification number: C07C29/16 ,  C07C31/278 ,  C07C45/50 ,  C07C47/347 ,  C07C2602/08 ,  C07C2602/24

    Abstract: The novel chemical compound, 3(4),7(8)-dihydroxymethylbicyclo[4.3.0]nonane and a process for its preparation, wherein bicyclo[4.3.0]nona-3,7-diene is reacted with synthesis gas in homogeneous organic phase in the presence of transition metal compounds of Group VIII of the Periodic Table containing complex-bound organophosphorus compound, at 70 to 160° C. and pressures of 5 to 35 MPa, and the 3(4),7(8)-bisformylbicyclo[4.3.0]nonane thus obtained is hydrogenated.

    Abstract translation: 新型化合物3（4），7（8） - 二羟甲基双环[4.3.0]壬烷及其制备方法，其中双环[4.3.0]壬-3,7-二烯与合成气同质化 在含有复合结合有机磷化合物的元素周期表第Ⅷ族过渡金属化合物存在下，在70至160℃和5至35MPa的压力以及3（4），7（8） - 由此获得的双甲酰基双环[4.3.0]壬烷被氢化。

    Process for preparing TCD-alcohol DM
    25.
    发明授权
    Process for preparing TCD-alcohol DM 失效
    制备TCD-醇DM的方法

    公开(公告)号：US06939997B2

    公开(公告)日：2005-09-06

    申请号：US10967580

    申请日：2004-10-18

    Applicant: Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    Inventor： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    IPC: B01J31/24 ,  C07B61/00 ,  C07C29/141 ,  C07C29/16 ,  C07C31/27 ,  C07C45/50 ,  C07C47/347 ,  C07C47/445 ,  C07C35/22

    CPC classification number: C07C29/141 ,  C07C29/16 ,  C07C45/50 ,  C07C47/347 ,  C07C2603/68 ,  C07C31/278 ,  C07C47/12 ,  C07C47/02

    Abstract: A process for preparing 3(4),8(9)-dihydroxymethyltricyclo[5.2.1.02,6]decane by hydroformylating dicyclopentadiene with subsequent distillation wherein the hydroformylation of dicyclopentadiene is carried out in two stages, and, in a first hydroformylation stage, the reaction is effected in a heterogeneous reaction system using an aqueous solution of transition metal compounds, containing water-soluble organic phosphorus (III) compounds in complex-bound form, of group VIII of the Periodic Table to give 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene, and, in a second hydroformylation stage, the thus obtained 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene is converted, in homogeneous organic phase in the presence of transition metal compounds of group VIII of the Periodic Table of the Elements to 3(4),8(9)-bisformyltricyclo[5.2.1.02,6]decane.

    Abstract translation: 通过加氢甲酰化二环戊二烯制备3（4），8（9） - 二羟基甲基三环[5.2.1.0 2,6]癸烷的方法，随后蒸馏，其中二环戊二烯的加氢甲酰化分两个阶段进行， 在第一加氢甲酰化阶段，反应在非均相反应体系中使用过渡金属化合物的水溶液进行，该过渡金属化合物含有复合结合形式的元素周期表第Ⅷ族的水溶性有机磷（III）化合物，得到 8（9） - 甲酰三环[5.2.1.0 2,6]癸-3-烯，并在第二加氢甲酰化阶段，由此得到的8（9） - 甲酰基三环[5.2.1.0 < 在3元周期表的第Ⅷ族过渡金属化合物存在下，在均相有机相中转变为3,6-亚甲基三环，8（9） - 二甲基三环 [5.2.1.0 2,6]癸烷。

    Process for preparing TCD-diamine
    26.
    发明申请
    Process for preparing TCD-diamine 失效
    制备TCD-二胺的方法

    公开(公告)号：US20050101796A1

    公开(公告)日：2005-05-12

    申请号：US10967597

    申请日：2004-10-18

    Applicant: Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    Inventor： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    IPC: C07C209/24 ,  C07B61/00 ,  C07C47/347 ,  C07C47/445 ,  C07C209/26 ,  C07C211/19 ,  C07C211/38 ,  C07C255/31 ,  C07C29/24

    CPC classification number: C07C209/26 ,  C07C47/347 ,  C07C47/445 ,  C07C2603/68 ,  C07C211/19

    Abstract: A process for preparing 3(4),8(9)-bis(aminomethyl)tricycle-[5.2.1.02,6]decane by hydroformylating dicyclopentadiene with subsequent reductive amination wherein the hydroformylation of dicyclopentadiene is carried out in two stages, and, in a first hydroformylation stage, the reaction is effected in a heterogeneous reaction system using an aqueous solution of transition metal compounds, containing water-soluble organic phosphorus (III) compounds in complex-bound form, of group VIII of the Periodic Table to give 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene, and, in a second hydroformylation stage, the thus obtained 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene is converted, in a homogeneous organic phase in the presence of transition metal compounds of group VIII of the Periodic Table of the Elements to 3(4),8(9)-bisformyltricyclo[5.2.1.02,6]decane

    Abstract translation: 通过加氢甲酰化二环戊二烯制备3（4），（9） - 双（氨基甲基）三环[5.2.1.0 2,6]癸烷的方法，随后还原胺化，其中携带二环戊二烯的加氢甲酰化 在两个阶段中，并且在第一加氢甲酰化阶段中，使用过渡金属化合物的水溶液在非均相反应体系中进行反应，所述过渡金属化合物含有复合结合形式的水溶性有机磷（III）化合物，第VIII族 的化合物，得到8（9） - 甲酰基三环[5.2.1.0 2,6]癸-3-烯，并在第二加氢甲酰化阶段，由此得到的8（9） - 甲酰三环 在[...]元素周期表第Ⅷ族过渡金属化合物存在下，在均相有机相中将[5.2.1.0 2,6]癸烯转化为3（4） ，8（9） - 二甲基三环[5.2.1.0 2,6]癸烷

    Method for the synthesis of straight-chain aliphatic carboxylic acids from aldehydes
    27.
    发明授权
    Method for the synthesis of straight-chain aliphatic carboxylic acids from aldehydes 失效
    从醛合成直链脂族羧酸的方法

    公开(公告)号：US06680395B2

    公开(公告)日：2004-01-20

    申请号：US10204495

    申请日：2002-09-05

    Applicant: Helmut Springer

    Inventor： Helmut Springer

    IPC: C07C5116

    CPC classification number: C07C51/235 ,  Y02P20/582 ,  C07C53/126 ,  C07C53/124

    Abstract: The invention relates to a non-catalysed method for the synthesis of straight-chain aliphatic carboxylic acids by oxidation of straight-chain aldehydes with oxygen-containing gas mixtures. The invention is characterised in that during the novel process of oxidation branched aldehydes are present in the reaction mixture.

    Abstract translation: 本发明涉及通过用含氧气体混合物氧化直链醛来合成直链脂族羧酸的非催化方法。 本发明的特征在于在氧化过程中，在反应混合物中存在支链醛。

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