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    POLYCYCLOPENTADIENE COMPOUNDS
    1.
    发明申请
    POLYCYCLOPENTADIENE COMPOUNDS 失效
    聚环氧乙烷化合物

    公开(公告)号：US20130046065A1

    公开(公告)日：2013-02-21

    申请号：US13643321

    申请日：2011-04-21

    申请人： Robert E. Hefner, JR. ,  Michael J. Mullins ,  Michael L. Tulchinsky ,  Ernesto Occhiello

    发明人： Robert E. Hefner, JR. ,  Michael J. Mullins ,  Michael L. Tulchinsky ,  Ernesto Occhiello

    IPC分类号： C07C47/445 ,  C08G8/32 ,  C08G8/04

    CPC分类号： C07C261/02 ,  C07C39/17 ,  C07C2603/68 ,  C07C2603/91

    摘要： Embodiments of the present disclosure include polycyclopentadiene compounds represented by Formula (I): in which each X is either a hydrogen or a cyano group (N≡C—), n has an average value from zero to 20; each m independently has a value of zero to 3; p has a value of zero to 20; each R is independently a halogen, a nitrile group, a nitro group, an alkyl group, an alkoxy group, an alkenyl group, or an alkenyloxy group, where the alkyl group, the alkoxy group, the alkenyl group, and the alkenyloxy group each independently contain 1 to 6 carbon atoms; and each Q is independently hydrogen or an alkyl group containing 1 to 6 carbon atoms. Embodiments of the present disclosure also include a curable composition that includes the polycyclopentadiene compound(s) of Formula (I) and a curing amount of a resin or a catalyst amount of a catalyst and/or a cure accelerating amount of an accelerating agent.

    摘要翻译： 本公开的实施方案包括由式（I）表示的聚环戊二烯化合物：其中每个X为氢或氰基（N≡C-），n的平均值为0至20; 每个m独立地具有零到3的值; p的值为零到20; 每个R独立地是卤素，腈基，硝基，烷基，烷氧基，烯基或烯氧基，其中烷基，烷氧基，烯基和烯氧基各自 独立地含有1至6个碳原子; 并且每个Q独立地是氢或含有1至6个碳原子的烷基。 本公开的实施方案还包括包含式（I）的聚环戊二烯化合物和树脂的固化量或催化剂的催化剂量和/或加速剂的固化促进量的可固化组合物。

    Process for preparing TCD-alcohol DM
    2.
    发明授权
    Process for preparing TCD-alcohol DM 失效
    制备TCD-醇DM的方法

    公开(公告)号：US06939997B2

    公开(公告)日：2005-09-06

    申请号：US10967580

    申请日：2004-10-18

    申请人： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    发明人： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    IPC分类号： B01J31/24 ,  C07B61/00 ,  C07C29/141 ,  C07C29/16 ,  C07C31/27 ,  C07C45/50 ,  C07C47/347 ,  C07C47/445 ,  C07C35/22

    CPC分类号： C07C29/141 ,  C07C29/16 ,  C07C45/50 ,  C07C47/347 ,  C07C2603/68 ,  C07C31/278 ,  C07C47/12 ,  C07C47/02

    摘要： A process for preparing 3(4),8(9)-dihydroxymethyltricyclo[5.2.1.02,6]decane by hydroformylating dicyclopentadiene with subsequent distillation wherein the hydroformylation of dicyclopentadiene is carried out in two stages, and, in a first hydroformylation stage, the reaction is effected in a heterogeneous reaction system using an aqueous solution of transition metal compounds, containing water-soluble organic phosphorus (III) compounds in complex-bound form, of group VIII of the Periodic Table to give 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene, and, in a second hydroformylation stage, the thus obtained 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene is converted, in homogeneous organic phase in the presence of transition metal compounds of group VIII of the Periodic Table of the Elements to 3(4),8(9)-bisformyltricyclo[5.2.1.02,6]decane.

    摘要翻译： 通过加氢甲酰化二环戊二烯制备3（4），8（9） - 二羟基甲基三环[5.2.1.0 2,6]癸烷的方法，随后蒸馏，其中二环戊二烯的加氢甲酰化分两个阶段进行， 在第一加氢甲酰化阶段，反应在非均相反应体系中使用过渡金属化合物的水溶液进行，该过渡金属化合物含有复合结合形式的元素周期表第Ⅷ族的水溶性有机磷（III）化合物，得到 8（9） - 甲酰三环[5.2.1.0 2,6]癸-3-烯，并在第二加氢甲酰化阶段，由此得到的8（9） - 甲酰基三环[5.2.1.0 < 在3元周期表的第Ⅷ族过渡金属化合物存在下，在均相有机相中转变为3,6-亚甲基三环，8（9） - 二甲基三环 [5.2.1.0 2,6]癸烷。

    Process for preparing TCD-diamine
    3.
    发明申请
    Process for preparing TCD-diamine 失效
    制备TCD-二胺的方法

    公开(公告)号：US20050101796A1

    公开(公告)日：2005-05-12

    申请号：US10967597

    申请日：2004-10-18

    申请人： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    发明人： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    IPC分类号： C07C209/24 ,  C07B61/00 ,  C07C47/347 ,  C07C47/445 ,  C07C209/26 ,  C07C211/19 ,  C07C211/38 ,  C07C255/31 ,  C07C29/24

    CPC分类号： C07C209/26 ,  C07C47/347 ,  C07C47/445 ,  C07C2603/68 ,  C07C211/19

    摘要： A process for preparing 3(4),8(9)-bis(aminomethyl)tricycle-[5.2.1.02,6]decane by hydroformylating dicyclopentadiene with subsequent reductive amination wherein the hydroformylation of dicyclopentadiene is carried out in two stages, and, in a first hydroformylation stage, the reaction is effected in a heterogeneous reaction system using an aqueous solution of transition metal compounds, containing water-soluble organic phosphorus (III) compounds in complex-bound form, of group VIII of the Periodic Table to give 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene, and, in a second hydroformylation stage, the thus obtained 8(9)-formyltricyclo[5.2.1.02,6]dec-3-ene is converted, in a homogeneous organic phase in the presence of transition metal compounds of group VIII of the Periodic Table of the Elements to 3(4),8(9)-bisformyltricyclo[5.2.1.02,6]decane

    摘要翻译： 通过加氢甲酰化二环戊二烯制备3（4），（9） - 双（氨基甲基）三环[5.2.1.0 2,6]癸烷的方法，随后还原胺化，其中携带二环戊二烯的加氢甲酰化 在两个阶段中，并且在第一加氢甲酰化阶段中，使用过渡金属化合物的水溶液在非均相反应体系中进行反应，所述过渡金属化合物含有复合结合形式的水溶性有机磷（III）化合物，第VIII族 的化合物，得到8（9） - 甲酰基三环[5.2.1.0 2,6]癸-3-烯，并在第二加氢甲酰化阶段，由此得到的8（9） - 甲酰三环 在[...]元素周期表第Ⅷ族过渡金属化合物存在下，在均相有机相中将[5.2.1.0 2,6]癸烯转化为3（4） ，8（9） - 二甲基三环[5.2.1.0 2,6]癸烷

    Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same
    7.
    发明授权
    Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same 失效

    公开(公告)号：US4476042A

    公开(公告)日：1984-10-09

    申请号：US546384

    申请日：1983-10-28

    申请人： Mark A. Sprecker ,  Marie R. Hanna ,  Richard J. Tokarzewski ,  Robert P. Belko ,  Hugh Watkins ,  Manfred H. Vock

    发明人： Mark A. Sprecker ,  Marie R. Hanna ,  Richard J. Tokarzewski ,  Robert P. Belko ,  Hugh Watkins ,  Manfred H. Vock

    IPC分类号： A24B15/34 ,  C07C47/347 ,  C07C47/445 ,  A61K7/46 ,  C11B9/00

    CPC分类号： A24B15/345 ,  C07C47/347 ,  C07C47/445

    摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represents hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

    Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same
    8.
    发明授权
    Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same 失效

    公开(公告)号：US4446060A

    公开(公告)日：1984-05-01

    申请号：US478353

    申请日：1983-03-24

    申请人： Mark A. Sprecker ,  Marie R. Hanna ,  Richard J. Tokarzewski ,  Robert P. Belko ,  Hugh Watkins ,  Manfred H. Vock

    发明人： Mark A. Sprecker ,  Marie R. Hanna ,  Richard J. Tokarzewski ,  Robert P. Belko ,  Hugh Watkins ,  Manfred H. Vock

    IPC分类号： A24B15/34 ,  C07C47/347 ,  C07C47/445 ,  A61K7/46 ,  C11B9/00

    CPC分类号： C07C47/445 ,  A24B15/345 ,  C07C47/347

    摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 take separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

    Flavoring with carboalkoxy alkyl norbornanes
    10.
    发明授权
    Flavoring with carboalkoxy alkyl norbornanes 失效
    用烷氧基烷基降冰片烷调味

    公开(公告)号：US4312888A

    公开(公告)日：1982-01-26

    申请号：US206466

    申请日：1980-11-13

    申请人： Philip T. Klemarczyk ,  James M. Sanders ,  Manfred H. Vock ,  Joaquin F. Vinals ,  Frederick L. Schmitt ,  Edward J. Granda

    发明人： Philip T. Klemarczyk ,  James M. Sanders ,  Manfred H. Vock ,  Joaquin F. Vinals ,  Frederick L. Schmitt ,  Edward J. Granda

    IPC分类号： A24B15/34 ,  C07C45/62 ,  C07C45/69 ,  C07C47/347 ,  C07C47/445 ,  C07C61/13 ,  C11B9/00 ,  C11D3/50 ,  A23L1/226

    CPC分类号： C11D3/50 ,  A24B15/345 ,  C07C45/62 ,  C07C45/69 ,  C07C47/347 ,  C07C47/445 ,  C07C61/13 ,  C11B9/0046

    摘要： Described is a process for augmenting or enhancing the aroma or taste of a foodstuff or chewing gum comprising the step of adding to a foodstuff or chewing gum an aroma augmenting or enhancing quantity of a product comprising a major proportion of compounds defined according to the structure: ##STR1## wherein the dashed line is either a carbon-carbon single bond or a carbon-carbon double bond and each of the R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.6 and R.sub.7 represents hydrogen or methyl with the proviso that one of R.sub.1, R.sub.2, R.sub.6 and R.sub.7 is methyl and each of the other of R.sub.1, R.sub.2, R.sub.6 and R.sub.7 is hydrogen and R.sub.3 and R.sub.4 are not both methyl; wherein R.sub.5 represents C.sub.1 -C.sub.4 produced according to the process of reacting an alkyl acrylate compound with a methyl cyclopentadiene in the presence of or in the absence of catalyst to form a norbornane carboxylate ester-containing mixture and using the resulting mixture for its organoleptic properties or further reacting the mixture with hydrogen to produce a norbornane carboxylate-containing mixture and using that mixture for its organoleptic properties in augmenting or enhancing the aroma or taste of footstuffs or chewing gums.

    摘要翻译： 描述了一种用于增强或增强食品或口香糖的香味或味道的方法，其包括向食品或口香糖中加入香味增加或增加量的包含主要比例的根据以下结构定义的化合物的产品的步骤： 其中虚线是碳 - 碳单键或碳 - 碳双键，R 1，R 2，R 3，R 4，R 6和R 7各自表示氢或甲基，条件是R 1，R 2， ，R 6和R 7是甲基，R 1，R 2，R 6和R 7中的每一个是氢，R 3和R 4不是甲基; 其中R 5表示根据丙烯酸烷基酯化合物与甲基环戊二烯在催化剂存在下或在不存在催化剂的情况下反应生成的含降冰片烷羧酸酯的混合物制备的C1-C4，并使用所得混合物的感官特性或 进一步使混合物与氢气反应以产生含降冰片烷羧酸盐的混合物，并且使用该混合物在增强或增强脚料或口香糖的香味或味道中的感官特性。