Aqueous slurries of finely divided fillers, their preparation and their use for the production of filler-containing papers
    22.
    发明申请
    Aqueous slurries of finely divided fillers, their preparation and their use for the production of filler-containing papers 有权
    精细分散的填料的水性浆料,它们的制备及其用于生产含填料的纸的用途

    公开(公告)号:US20050197278A1

    公开(公告)日:2005-09-08

    申请号:US11082904

    申请日:2005-03-18

    Abstract: Aqueous slurries of finely divided fillers which are at least partly coated with polymers and which are obtainable by treating aqueous slurries of finely divided fillers with at least one water-soluble amphoteric copolymer which is obtainable by copolymerization of (a) at least one N-vinylcarboxamide of the formula  where R1 and R2 are H or C1- to C6-alkyl, (b) at least one monoethylenically unsaturated carboxylic acid having 3 to 8 carbon atoms in the molecule and/or the alkali metal, alkaline earth metal or ammonium salts thereof and, if required, (c) other monoethylenically unsaturated monomers which are free of nitrile groups and, if required, (d) compounds which have at least two ethylenically unsaturated double bonds in the molecule and subsequent partial or complete elimination of the groups —CO—R1 from the monomers III incorporated in the form of polymerized units in the copolymer are used as an additive to the paper stock in the production of filler-containing paper, filler-containing cardboard or filler-containing board by draining of the paper stock.

    Abstract translation: 至少部分涂覆有聚合物的细分散填料的水性浆料,其可通过用至少一种水溶性两性共聚物处理细分散填料的水性浆料而获得,所述水溶性两性共聚物可通过(a)至少一种N-乙烯基甲酰胺 其中R 1和R 2均为H或C 1至C 6 - 烷基,( b)分子中具有3-8个碳原子的至少一种单烯属不饱和羧酸和/或其碱金属,碱土金属或铵盐,如果需要,(c)不含腈基的其它单烯属不饱和单体 并且如果需要,(d)在分子中具有至少两个烯键式不饱和双键的化合物以及随后部分或完全从形式的所述单体III中部分或完全消除基团-CO-R 1 的共聚物中的聚合单元用作纸料i的添加剂 n通过排干纸料来生产含填料的纸,含填料​​的纸板或含填料的板。

    Preparation of 3-methylquinoline-8-carboxylic acid
    26.
    发明授权
    Preparation of 3-methylquinoline-8-carboxylic acid 失效
    3-甲基喹啉-8-羧酸的制备

    公开(公告)号:US5130434A

    公开(公告)日:1992-07-14

    申请号:US571232

    申请日:1990-08-23

    CPC classification number: C07D215/48

    Abstract: 3-Methylquinoline-8-carboxylic acid I ##STR1## and derivatives thereof are prepared by reacting o-toluidine II or a derivative thereof ##STR2## with methacrolein II ##STR3## in 70-90% strength by weight sulfuric acid in the presence of iodine or of an iodine compound, and oxidizing the resulting 3,8-dimethylquinoline IV or a derivative thereof ##STR4## with nitric acid in a solution containing sulfuric acid, in the presence of vanadium ions, by a process in which, in the sulfuric acid-containing reaction solution of the 3,8-dimethylquinoline IV, the byproducts of the reaction are first decomposed by oxidation, the resulting 3,8-dimethylquinoline solution is concentrated by distillation and the 3,8-dimethylquinoline is then oxidized in situ with nitric acid to give the 3-methylquinoline-carboxylic acid.

    Abstract translation: 3-甲基喹啉-8-羧酸I I及其衍生物通过邻甲苯胺II或其衍生物II与甲基丙烯醛II III在70-90%重量比的硫酸中反应制备 碘或碘化合物的存在,并且在钒离子存在下,通过硝酸在含硫酸溶液中氧化得到的3,8-二甲基喹啉IV或其衍生物IV,其中 在3,8-二甲基喹啉IV的含硫酸的反应溶液中,首先通过氧化分解反应的副产物,然后通过蒸馏浓缩所得的3,8-二甲基喹啉溶液,然后将3,8-二甲基喹啉 用硝酸原位氧化得到3-甲基喹啉羧酸。

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