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公开(公告)号：US20080183014A1
公开(公告)日：2008-07-31
申请号：US12020264
申请日：2008-01-25
IPC分类号： C07C51/487
摘要： A process for preparing acrylic acid, in which an acrylic acid-comprising product gas mixture obtained by catalytic gas phase partial oxidation of a C3 precursor of acrylic acid is fractionally condensed in a condensation column provided with internals ascending into itself with side draw removal of crude acrylic acid and with liquid phase draw removal of acrylic acid-comprising acid water, and acrylic acid present in acid water is taken up into an extractant and then removed from the extractant and recycled into the condensation column, or taken up in aqueous metal hydroxide, or sent to further purification of the crude acrylic acid.
摘要翻译： 制备丙烯酸的方法，其中通过丙烯酸C 3/3前体的催化气相部分氧化获得的含丙烯酸的产物气体混合物在具有内部升降的冷凝塔中分级冷凝 用丙烯酸粗抽出去除丙烯酸的酸性水，并将存在于酸性水中的丙烯酸吸收到萃取剂中，然后从萃取剂中除去并再循环到冷凝塔中， 或吸收在金属氢氧化物水溶液中，或者进一步纯化粗丙烯酸。
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22.发明申请Method for cleaning plate columns used for rectifying liquids containing (meth)acrylic acid and/or the esters thereof 有权用于清洁含有（甲基）丙烯酸和/或其酯的液体的精馏塔的柱的方法公开(公告)号：US20050115590A1
公开(公告)日：2005-06-02
申请号：US10505163
申请日：2003-03-04
申请人： Juergen Schroeder , Klaus Muller-Engel , Volker Schliephake , Ulrich Hammon , Volker Diehl , Ulrich Jager
发明人： Juergen Schroeder , Klaus Muller-Engel , Volker Schliephake , Ulrich Hammon , Volker Diehl , Ulrich Jager
摘要： In process for cleaning tray columns which are used for the purposes of rectifiying liquids comprising (meth)acrylic compounds, a basic liquid is conveyed downward through the tray column and a gas is passed through the column in countercurrent to the basic liquid at an average gas phase differential pressure over all trays of at least 0.5 mbar/tray.
摘要翻译： 在清洁用于整流包含（甲基）丙烯酸类化合物的液体的托盘列的过程中，碱性液体向下传送通过塔盘塔，气体以平均气体与碱性液体逆流通过塔 至少0.5 mbar /托盘的所有托盘上的相位差压。
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23.发明授权Method for removing by-products obtained when producing acrylic acid or methacrylic acids 有权用于除去制备丙烯酸或甲基丙烯酸时得到的副产物的方法公开(公告)号：US06348638B1
公开(公告)日：2002-02-19
申请号：US09147416
申请日：1998-12-21
申请人： Volker Schliephake , Ulrich Hammon , Wolfgang Pies , Ulrich Rauh
发明人： Volker Schliephake , Ulrich Hammon , Wolfgang Pies , Ulrich Rauh
IPC分类号： A62D300
摘要： In a process for the disposal of low, mediun, and high-boiling secondary components formed during the preparation of (meth)acrylic acid the gaseous low-boiling secondary components are burned, whilst low-boiling and medium-boiling secondary components that are dissolved in water optionally together with high-boiling secondary components treated with solvent are added.
摘要翻译： 在处理在（甲基）丙烯酸制备期间形成的低，中和和高沸点次要组分的方法中，气态低沸点次级组分被燃烧，而溶解的低沸点和中沸点次要组分 在水中任选加入用溶剂处理的高沸点次级组分。
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24.发明授权Method for the rectifying separation of fluids containing (meth)acryl monomers 有权含有（甲基）丙烯酸单体的流体的精馏分离方法公开(公告)号：US07520964B2
公开(公告)日：2009-04-21
申请号：US10515639
申请日：2003-07-02
CPC分类号： B01D3/22 , B01D3/225 , C07C51/44 , Y10S203/11 , Y10S203/22 , C07C57/04
摘要： A process for rectificatively separating at least one (meth)acrylic monomer-containing fluid by feeding the fluid into a rectification column containing at least one sieve tray without a runoff segment, wherein an elementary cell is obtained from a number of centers of passages in a sieve tray, and the cell shifts regularly and repeatedly along its edges, the lengths of two shifting vectors being the lengths of the edges of the cell along which the shifting is effected; an arrangement of the centers is such that the positions of an ideal center and a real center are separated by ≦1% of half of the sum of the lengths of the two shifting vectors; and an arrangement of the passages is such that the sum of non-overlapping surface areas of an ideal passage with a real passage and vice versa is ≦1% of the surface area of the ideal passage.
摘要翻译： 将含有至少一种（甲基）丙烯酸系单体的流体通过将流体供给至含有至少一个不具有径流段的多孔塔的精馏塔的方法，其中从多个通道中心获得基本单元， 筛板，并且单元沿其边缘规则地且重复地移动，两个移动向量的长度是实现移位的单元的边缘的长度; 中心的布置使得理想中心和实心的位置被两个移位矢量的长度之和的一半的<= 1％分开; 并且通道的布置使得理想通道的非重叠表面面积与实际通道的总和相反，<=理想通道的表面积的1％。
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25.发明申请Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion 有权以结构化方式对催化剂管束的催化剂管进行充电的方法公开(公告)号：US20060045825A1
公开(公告)日：2006-03-02
申请号：US11118433
申请日：2005-05-02
IPC分类号： B01D53/34
CPC分类号： B01J8/0015 , B01J8/003 , B01J8/06 , B01J8/067 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/026 , B01J2208/00212 , B01J2208/00752 , B01J2208/00814 , B01J2208/025 , B01J2523/00 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion, in which uniformly predispensed portions of formulations of shaped catalyst bodies are used for producing a section of charge.
摘要翻译： 以结构方式装载一束催化剂管的催化剂管的方法，其中使用成形催化剂体的制剂的均匀预分配部分来产生一部分电荷。
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公开(公告)号：US20050109377A1
公开(公告)日：2005-05-26
申请号：US10989277
申请日：2004-11-17
CPC分类号： F28G9/00 , B01J8/0015 , B01J8/06 , B01J2208/00761 , B08B9/0436 , B08B9/045 , B23B51/0406 , F28G3/02 , F28G3/10
摘要： The invention described herein relates to a process for removing solids from tubes of a tube bundle heat exchanger, wherein a drill driven by a drilling machine is inserted into a tube of the tube bundle heat exchanger and clears out solids present in the tube. In a first variant of the process according to the invention, the drill is a spiral drill and has, cut out in the outer casing of the drill, a spiral conveyor groove in which the solids particles loosened and isolated by the drill tip on insertion of the drill into the tube can be transported out of the tube. More preferably, the drill is a hollow drill 10 which is provided with a substantially circular drill tip 11 and has a central recess running along the rotational axis in the longitudinal direction of the drill and opening into the drill tip 11 at the free end of the drill. At the drill tip 11 are provided toothlike projections 12.
摘要翻译： 本文所述的本发明涉及从管束热交换器的管中除去固体的方法，其中由钻机驱动的钻头插入管束热交换器的管中并清除管中存在的固体。 在根据本发明的方法的第一变型中，钻头是螺旋钻，并且在钻头的外壳中切出螺旋输送槽，在该螺旋输送槽中固体颗粒在钻头插入时由钻头松动和隔离 钻进管子可以被运送出管。 更优选地，钻头是中空钻机10，其设置有基本上圆形的钻头11，并且具有在钻头的纵向方向上沿着旋转轴线延伸的中心凹部，并在钻头的自由端处开入钻头尖端11 钻头。 在钻尖11处设有齿状突起12。
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27.发明授权Process for operating a continuous removal of a target product X in the form of fine crystals 有权用于以细晶体的形式连续移除靶产物X的方法公开(公告)号：US07732624B2
公开(公告)日：2010-06-08
申请号：US12208737
申请日：2008-09-11
申请人： Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel , Volker Schliephake , Dieter Baumann
发明人： Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel , Volker Schliephake , Dieter Baumann
IPC分类号： C07D207/26 , C07C51/43 , C07C7/14
CPC分类号： B01D9/0013 , B01D9/004 , B01D9/005 , B01D9/0063 , C07C7/14 , C07C51/43 , C07C15/08 , C07C57/04
摘要： A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in an indirect heat transferer, in which the crystal suspension formed is conducted out of the heat transferer first into a mixed buffer tank and, from there, fed to an apparatus for separating the crystal suspension into crystals and liquid phase, and wherein external measures dissipade the oversaturation of the crystal suspension fed to the buffer vessel with target product X.
摘要翻译： 通过在间接热转移体中冷却悬浮液结晶，从包含目标产物X和除了目标产物X的成分的液相P连续除去目标产物X的形式的方法，其中形成的晶体悬浮液为 首先从热转移器中导出到混合缓冲罐中，从那里进料到用于将晶体悬浮液分离成晶体和液相的装置，并且其中外部措施消除了用目标物供给缓冲容器的晶体悬浮液的过饱和 产品X.
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28.发明授权Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion 有权以结构化方式对催化剂管束的催化剂管进行充电的方法公开(公告)号：US07731916B2
公开(公告)日：2010-06-08
申请号：US11118433
申请日：2005-05-02
IPC分类号： B65B1/04
CPC分类号： B01J8/0015 , B01J8/003 , B01J8/06 , B01J8/067 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/026 , B01J2208/00212 , B01J2208/00752 , B01J2208/00814 , B01J2208/025 , B01J2523/00 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion, in which uniformly predispensed portions of formulations of shaped catalyst bodies are used for producing a section of charge.
摘要翻译： 以结构方式装载一束催化剂管的催化剂管的方法，其中使用成形催化剂体的制剂的均匀预分配部分来产生一部分电荷。
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公开(公告)号：US07566804B2
公开(公告)日：2009-07-28
申请号：US12020264
申请日：2008-01-25
摘要： A process for preparing acrylic acid, in which an acrylic acid-comprising product gas mixture obtained by catalytic gas phase partial oxidation of a C3 precursor of acrylic acid is fractionally condensed in a condensation column provided with internals ascending into itself with side draw removal of crude acrylic acid and with liquid phase draw removal of acrylic acid-comprising acid water, and acrylic acid present in acid water is taken up into an extractant and then removed from the extractant and recycled into the condensation column, or taken up in aqueous metal hydroxide, or sent to further purification of the crude acrylic acid.
摘要翻译： 制备丙烯酸的方法，其中通过丙烯酸的C3前体的催化气相部分氧化获得的含丙烯酸的产物气体混合物在冷凝塔中分级冷凝，所述内部装有自身上升的侧向抽出粗品 丙烯酸和含丙烯酸的酸性水的液相萃取和酸性水中存在的丙烯酸被吸收到萃取剂中，然后从萃取剂中除去并循环到冷凝柱中，或者被吸收在金属氢氧化物水溶液中， 或者进一步纯化粗丙烯酸。
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30.发明授权Safe operation of a continuous heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound 有权至少一种有机化合物的连续不均匀催化气相部分氧化的安全操作公开(公告)号：US07074955B2
公开(公告)日：2006-07-11
申请号：US10459782
申请日：2003-06-12
申请人： Ulrich Hammon , Jochen Meschke , Ulrich Rauh , Klaus Joachim Müller-Engel , Peter Schlemmer , Volker Schliephake
发明人： Ulrich Hammon , Jochen Meschke , Ulrich Rauh , Klaus Joachim Müller-Engel , Peter Schlemmer , Volker Schliephake
IPC分类号： C07C51/16
CPC分类号： C07C51/215 , C07C45/33 , C07C45/34 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A continuously operated heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound in an oxidation reactor is operated safely by a process in which an explosion diagram for the feed gas mixture is deposited as the basis of a cut-out mechanism in a computer.
摘要翻译： 在氧化反应器中连续操作的至少一种有机化合物的气相部分氧化被安全地通过其中沉积原料气体混合物的爆炸图作为计算机中的切断机构的基础的方法来操作 。
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