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    Polymerizable bicyclic cyclopropane derivatives and their use for the preparation of dental materials
    21.
    发明授权
    Polymerizable bicyclic cyclopropane derivatives and their use for the preparation of dental materials 有权
    可聚合双环环丙烷衍生物及其在牙科材料制备中的应用

    公开(公告)号：US07585901B2

    公开(公告)日：2009-09-08

    申请号：US11752652

    申请日：2007-05-23

    申请人： Norbert Moszner ,  Armin de Meijere ,  Frank Zeuner ,  Urs Karl Fischer

    发明人： Norbert Moszner ,  Armin de Meijere ,  Frank Zeuner ,  Urs Karl Fischer

    IPC分类号： A61K6/083 ,  A61C5/00 ,  C08F232/08

    CPC分类号： A61K6/0023 ,  A61K6/0017 ,  A61K6/083 ,  A61K6/09 ,  C07C69/608 ,  C07C69/675 ,  C07C69/716 ,  C07C271/28 ,  C07C2602/18 ,  C07D307/93 ,  C07D311/94 ,  C07D335/04 ,  C08L33/00 ,  C08L75/16

    摘要： Bicyclic cyclopropane derivatives of the general Formula (I) in which n+m is 0 to 8; r is 1 to 4; R1 is absent or is a C1-C20 alkylene radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, a bicyclic C4-C12 radical, a C6-C14 arylene or C7-C20 alkylenearylene radical; R2 is for r=1 a C1-C20 alkyl radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, a bicyclic C4-C12 radical, a C6-C14 aryl or a C7-C20 alkylaryl radical; is for r>1 an r-times substituted aliphatic C1 to C20 radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, an aromatic C6-C14 radical or aliphatic-aromatic C7-C20 radical; X is absent or is —CO—O—, —CO—NH— or —O—CO—NH—, and Y is CH2, O or S which is suitable in particular for the preparation of dental materials.

    摘要翻译： 通式（I）的双环环丙​​烷衍生物，其中n + m为0至8; r为1〜4; R1不存在或是可被O或S间隔的C 1 -C 20亚烷基，脂环族C 4 -C 12基团，双环C 4 -C 12基团，C 6 -C 14亚芳基或C 7 -C 20亚烷基亚芳基基团; R2为r = 1，可被O或S间隔的C1-C20烷基，脂环族C 4 -C 12基，双环C 4 -C 12基，C 6 -C 14芳基或C 7 -C 20烷基芳基; 对于r> 1，可以被O或S间隔的r-次取代的脂族C1至C20基团，脂环族C 4 -C 12基团，芳族C 6 -C 14基团或脂族 - 芳族C 7 -C 20基团; X不存在或是-CO-O-，-CO-NH-或-O-CO-NH-，Y是CH2，O或S，其特别适用于制备牙科材料。

    Polymerizable compositions with acylgermanes as initiatiors
    22.
    发明申请
    Polymerizable compositions with acylgermanes as initiatiors 审中-公开
    具有酰基作为起始物的可聚合组合物

    公开(公告)号：US20080076847A1

    公开(公告)日：2008-03-27

    申请号：US11730533

    申请日：2007-04-02

    申请人： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    发明人： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    IPC分类号： C08F2/50 ,  A61K6/08 ,  C08J3/28 ,  C08F2/46

    CPC分类号： A61K6/0023 ,  A61K6/0017 ,  A61K6/0052 ,  A61K6/083 ,  C08F2/50 ,  C08F4/72 ,  C08F222/1006 ,  C08F230/10 ,  C08L33/00

    摘要： Composition with at least one polymerizable binder and a polymerization initiator, which contains at least one acylgermane according to general Formula (I), in which R0 is a substituted or unsubstituted C1-18-alkyl radical or an acyl group; R1 and R2 are H, an acyl group or have one of the meanings given for R3; R3 is a branched or linear C1-18-alkyl radical which can be unsubstituted or substituted one or more times by —O—, —NH—, —NR—, —S— or interrupted by other groups, trimethylsilyl, hal-(CH3)2Si—[OSi(CH3)2]r−, (CH3)3Si—[OSi(CH3)2]r—, —COOH, —COO—R10, —CO—NR11R12, —CO-vinyl, —CO-phenyl, phenyl-C1-4-alkyl, phenyl, naphthyl or biphenyl, C5-12 cycloalkyl, a 5 or 6-membered O, S or N-containing heterocyclic ring, halogen, OH, an aromatic C6-30 radical which can be substituted or unsubstituted and/or interrupted by O, S or —NR—, or a branched, cyclic or linear C1-20 alkyl, -alkenyl, -alkoxy or -alkenoxy radical; m is 1, 2 or 3; n is 0 or 1 and p is 0 or 1; and the use of acyl germanes of Formula (I) for example as initiator for radical polymerization.

    摘要翻译： 含有至少一种可聚合粘合剂和聚合引发剂的组合物，其含有至少一种根据通式（I）的酰基锗烷，其中R 0是取代或未取代的C 1-18烷基， /烷基或酰基; R 1和R 2均为H，酰基或具有R 3给出的含义之一; R 3是支链或直链C 1-18 - 烷基，其可以是未取代的或被-O - ， - NH-，-NR- ，-S-或被其它基团中断，三甲基甲硅烷基，卤代（CH 3）2 Si- [OSi（CH 3）3） （CH 3）3 Si- [OSi（CH 3）3） -COOH，-COO-R 10，-CO-NR， - ， - SO 2 - ， - 11- 12，-CO-乙烯基，-CO-苯基，苯基-C 1-4 - 烷基，苯基，萘基或联苯基，C

    Polymerizable compositions with acylgermanium compounds
    24.
    发明授权
    Polymerizable compositions with acylgermanium compounds 有权
    具有酰基锗化合物的可聚合组合物

    公开(公告)号：US07605190B2

    公开(公告)日：2009-10-20

    申请号：US11902865

    申请日：2007-09-26

    申请人： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    发明人： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    IPC分类号： A61C13/00 ,  A61C13/225 ,  A61K6/00 ,  C08F2/50 ,  C08J3/28

    CPC分类号： C08F2/50 ,  A61K6/083 ,  C08F4/72 ,  Y10S522/908 ,  C08L33/00

    摘要： Composition with at least one polymerizable binder and at least one polymerization initiator, which contains at least one acylgermanium compound according to general Formula (I), in which R0 is a substituted or unsubstituted C1-18-alkyl radical or an acyl group; R1 and R2 are H, an acyl group or have one of the meanings given for R3; R3 is a branched or linear C1-18-alkyl radical which can be unsubstituted or substituted one or more times by —O—, —NH—, —NR—, —S— or interrupted by other groups, trimethylsilyl, hal-(CH3)2Si—[OSi(CH3)2]r−, (CH3)3Si—[OSi(CH3)2]r—, —COOH, —COO—R10, —CO—NR11R12, —CO-vinyl, —CO-phenyl, phenyl-C1-4-alkyl, phenyl, naphthyl or biphenyl, C5-12 cycloalkyl, a 5 or 6-membered O, S or N-containing heterocyclic ring, halogen, OH, an aromatic C6-30 radical which can be substituted or unsubstituted and/or interrupted by O, S or —NR—, or a branched, cyclic or linear C1-20 alkyl, -alkenyl, -alkoxy or -alkenoxy radical; m is 1, 2 or 3; n is 0 or 1 and p is 0 or 1; wherein in each case two of the radicals R0, R1, R2 or R3 can be connected to each other accompanied by the formulation of a 5 to 8 member ring; and the use of acylegermanium compounds of Formula (I), for example, as initiator for radical polymerization.

    摘要翻译： 含有至少一种可聚合粘合剂和至少一种聚合引发剂的组合物，其含有至少一种根据通式（I）的酰基锗化合物，其中R 0是取代或未取代的C 1-18 - 烷基或酰基; R 1和R 2是H，酰基或具有R 3给出的含义之一; R3是支链或直链的C1-18 - 烷基，其可以是未取代的或被-O - ， - NH - ， - NR - ， - S-取代或被其它基团间隔的一个或多个，三甲基甲硅烷基，hal-（CH 3 ）2Si- [OSi（CH 3）2] r - ，（CH 3）3 Si- [OSi（CH 3）2] r - ，-COOH，-COO-R 10，-CO-NR 11 R 12，-CO-乙烯基， 苯基，C 1-4 - 烷基，苯基，萘基或联苯基，C 5-12环烷基，5或6元O，S或N的杂环，卤素，OH，可被取代的芳族C 6-30基团 或未取代和/或被O，S或-NR-或支链，环状或直链的C 1-20烷基， - 烯基， - 烷氧基或 - m为1,2或3; n为0或1，p为0或1; 其中在每种情况下，基团R 0，R 1，R 2或R 3中的两个可以相互连接，伴随着5-8元环的配制; 以及使用式（I）的乙烯基锗化合物，例如作为自由基聚合的引发剂。

    Dental materials with unusual fluorine distribution
    25.
    发明授权
    Dental materials with unusual fluorine distribution 有权
    具有不寻常氟分布的牙科材料

    公开(公告)号：US07595354B2

    公开(公告)日：2009-09-29

    申请号：US11338034

    申请日：2006-01-24

    申请人： Norbert Moszner ,  Urs Karl Fischer ,  Volker M Rheinberger ,  Giancarlo Galli ,  Marina Ragnoli ,  Emo Chiellini

    发明人： Norbert Moszner ,  Urs Karl Fischer ,  Volker M Rheinberger ,  Giancarlo Galli ,  Marina Ragnoli ,  Emo Chiellini

    IPC分类号： A61C5/04 ,  A61K6/083 ,  C08F12/20 ,  C08F232/04

    CPC分类号： A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  C08L33/00 ,  C08L25/00

    摘要： A composition comprising (A) at least one fluorinated vinylcyclopropane according to Formula (I) wherein R1 is H or —CO—O—(CH2CH2)p—R7; R2 is H or forms together with R6 a —CH2—C(R9)(R10)—CH2— residue; R3 is H; R4 is H or forms together with R5—CH2—C(R9)(R10)—CH2— residue; R5 is H, —CO—O—R8, —CO—O—(CH2CH2)p—R7 or forms together with R4—CH2—C(R9)(R10)—CH2— residue; R6 is H, —CO—O—R8, —CO—O—(CH2CH2)p—R7 or forms together with R2 a —CH2—C(R9)(R10)—CH2— residue; R7 is perfluorinated C2-C20 aliphatic or alicyclic group; R8 is H, phenyl, benzyl, or a linear or branched C1-C12 aliphatic or alicyclic group; R9 is a H, benzoyl, acetyl or a C1-C5-alkyl group; R10H or a —CO—O—R8; p is 1, 2, 3, or 4, provided that the compound of Formula (I) comprises at least one —CO—O—(CH2CH2)p—R7 residue; (B) at least one non-fluorinated vinylcyclopropane derivative; (C) a bisphenol-A-ether di(meth)acrylate according to Formula (II) wherein R18 is H or CH3, R19 is CH3 or CF3, Y is a C2-C5-alkylen residue which can be substituted by an OH group or is preferably unsubstituted.

    摘要翻译： 一种组合物，其包含（A）至少一种根据式（I）的氟化乙烯基环丙烷，其中R 1是H或-CO-O-（CH 2 CH 2）p -R 7; R2是H或与R6一起形成-CH 2 -C（R 9）（R 10）-CH 2 - 残基; R3为H; R4是H或与R5-CH2-C（R9）（R10）-CH2-残基一起形成; R5是H，-CO-O-R8，-CO-O-（CH2CH2）p-R7或与R4-CH2-C（R9）（R10）-CH2-残基一起形成; R6是H，-CO-O-R8，-CO-O-（CH2CH2）p-R7或与R2一起形成-CH2-C（R9）（R10）-CH2-残基; R7是全氟化C 2 -C 20脂族或脂环基; R8是H，苯基，苄基或直链或支链C 1 -C 12脂族或脂环基; R9是H，苯甲酰基，乙酰基或C1-C5-烷基; R10H或-CO-O-R8; p为1,2,3或4，条件是式（I）化合物包含至少一个-CO-O-（CH 2 CH 2）p-R 7残基; （B）至少一种非氟化乙烯基环丙烷衍生物; （C）式（II）的双酚A - 醚二（甲基）丙烯酸酯，其中R18为H或CH3，R19为CH3或CF3，Y为可被OH基取代的C2-C5-亚烷基基团 或优选未被取代。

    Dental materials based on multicyclic allyl sulphides
    26.
    发明授权
    Dental materials based on multicyclic allyl sulphides 有权
    基于多环烯丙基硫化物的牙科材料

    公开(公告)号：US07501457B2

    公开(公告)日：2009-03-10

    申请号：US11482164

    申请日：2006-07-07

    申请人： Jörg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    发明人： Jörg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    IPC分类号： A61K6/083 ,  C08F28/06

    CPC分类号： A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  C08L33/00

    摘要： Dental materials and associated methods are described based on multicyclic allyl sulphides with general Formula (I): in which R1 is H or a C1-C10 alkyl radical; R2 is H or a C1-C10 alkyl radical; R3 is absent or is a C1-C20 alkylene radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, a bicyclic C6-C12 radical, a C6-C14 arylene or C7-C20 alkylene arylene radical; R4 is an n-times substituted aliphatic C2 to C20 hydrocarbon radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, an aromatic C6-C14 radical, an aliphatic-aromatic C7-C20 radical or a heterocyclic radical which can contain 4 to 20 carbon atoms and 1 to 6 heteroatoms which are selected from N, O, P and/or S atoms, or which is formed exclusively by these heteroatoms; R5 is absent or is a C1-C10 alkylene radical; X is absent or is O, S, —O—CO— or —O—CO—NH—; Y is absent or is O, S, —O—CO— or —O—CO—NH—; m is 0 or 1 and n is an integer from 3 to 6.

    摘要翻译： 基于具有通式（I）的多环烯丙基硫化物描述牙科材料和相关方法：其中R1是H或C1-C10烷基; R2是H或C1-C10烷基; R3不存在或是可被O或S间隔的C 1 -C 20亚烷基，脂环族C 4 -C 12基，双环C 6 -C 12基，C 6 -C 14亚芳基或C 7 -C 20亚烷基亚芳基; R4是可被O或S间隔的n次取代的脂族C 2 -C 20烃基，脂环族C 4 -C 12基团，芳族C 6 -C 14基团，脂族 - 芳族C 7 -C 20基团或杂环基团，其可以 含有4至20个碳原子和1至6个选自N，O，P和/或S原子的杂原子，或仅由这些杂原子形成的杂原子; R5不存在或是C1-C10亚烷基; X不存在或为O，S，-O-CO-或-O-CO-NH-; Y不存在或为O，S，-O-CO-或-O-CO-NH-; m为0或1，n为3至6的整数。

    Dental materials based on multicyclic allyl sulphides
    27.
    发明申请
    Dental materials based on multicyclic allyl sulphides 有权
    基于多环烯丙基硫化物的牙科材料

    公开(公告)号：US20070203256A1

    公开(公告)日：2007-08-30

    申请号：US11482164

    申请日：2006-07-07

    申请人： Jorg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    发明人： Jorg Angermann ,  Peter Burtscher ,  Urs Karl Fischer ,  Norbert Moszner ,  Volker M. Rheinberger

    IPC分类号： A61K6/08

    CPC分类号： A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  C08L33/00

    摘要： Dental materials and associated methods are described based on multicyclic allyl sulphides with general Formula (I): in which R1 is H or a C1-C10 alkyl radical; R2 is H or a C1-C10 alkyl radical; R3 is absent or is a C1-C20 alkylene radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, a bicyclic C6-C12 radical, a C6-C14 arylene or C7-C20 alkylene arylene radical; R4 is an n-times substituted aliphatic C2 to C20 hydrocarbon radical which can be interrupted by O or S, a cycloaliphatic C4-C12 radical, an aromatic C6-C14 radical, an aliphatic-aromatic C7-C20 radical or a heterocyclic radical which can contain 4 to 20 carbon atoms and 1 to 6 heteroatoms which are selected from N, O, P and/or S atoms, or which is formed exclusively by these heteroatoms; R5 is absent or is a C1-C10 alkylene radical; X is absent or is O, S, —O—CO— or —O—CO—NH—; Y is absent or is O, S, —O—CO— or —O—CO—NH—; m is 0 or 1 and n is an integer from 3 to 6.

    摘要翻译： 牙科材料和相关方法基于通式（I）的多环烯丙基硫化物来描述：其中R 1是H或C 1 -C 10烷基， 烷基; R 2是H或C 1 -C 10烷基; R 3不存在或是可以被O或S中断的C 1 -C 20亚烷基，脂环族C 1 -C 20烷基， 4个-C 12 - 基团，双环C 6 -C 12 - 基团，C 6 - -C 14亚芳基或C 7 -C 20亚烷基亚芳基; R 4是可以被O或S间隔的n 20取代的C 20烃基C 2〜C 20烃基， 芳族C 6 -C 14 - 基团，脂族 - 芳族C 1 -C 12烷基，芳基C 6 -C 14 - 或者可以含有4至20个碳原子和1至6个选自N，O，P和/或S原子的杂原子的杂环基团，或其中 完全由这些杂原子形成; R 5不存在或者是C 1 -C 10亚烷基; X不存在或为O，S，-O-CO-或-O-CO-NH-; Y不存在或为O，S，-O-CO-或-O-CO-NH-; m为0或1，n为3至6的整数。

    Polymerizable compositions with acylgermanium compounds
    30.
    发明申请
    Polymerizable compositions with acylgermanium compounds 有权
    具有酰基锗化合物的可聚合组合物

    公开(公告)号：US20080277814A1

    公开(公告)日：2008-11-13

    申请号：US11902865

    申请日：2007-09-26

    申请人： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    发明人： Norbert Moszner ,  Ulrich Salz ,  Urs Karl Fischer ,  Robert Liska ,  Heinrich Gruber ,  Beate Ganster

    IPC分类号： A61C13/087

    CPC分类号： C08F2/50 ,  A61K6/083 ,  C08F4/72 ,  Y10S522/908 ,  C08L33/00

    摘要： Composition with at least one polymerizable binder and at least one polymerization initiator, which contains at least one acylgermanium compound according to general Formula (I), in which R0 is a substituted or unsubstituted C1-18-alkyl radical or an acyl group; R1 and R2 are H, an acyl group or have one of the meanings given for R3; R3 is a branched or linear C1-18-alkyl radical which can be unsubstituted or substituted one or more times by —O—, —NH—, —NR—, —S— or interrupted by other groups, trimethylsilyl, hal-(CH3)2Si—[OSi(CH3)2]r−, (CH3)3Si—[OSi(CH3)2]r—, —COOH, —COO—R10, —CO—NR11R12, —CO-vinyl, —CO-phenyl, phenyl-C1-4-alkyl, phenyl, naphthyl or biphenyl, C5-12 cycloalkyl, a 5 or 6-membered O, S or N-containing heterocyclic ring, halogen, OH, an aromatic C6-30 radical which can be substituted or unsubstituted and/or interrupted by O, S or —NR—, or a branched, cyclic or linear C1-20 alkyl, -alkenyl, -alkoxy or -alkenoxy radical; m is 1, 2 or 3; n is 0 or 1 and p is 0 or 1; wherein in each case two of the radicals R0, R1, R2 or R3 can be connected to each other accompanied by the formulation of a 5 to 8 member ring; and the use of acylegermanium compounds of Formula (I), for example, as initiator for radical polymerization.

    摘要翻译： 含有至少一种可聚合粘合剂和至少一种聚合引发剂的组合物，其含有至少一种根据通式（I）的酰基锗化合物，其中R 0是取代或未取代的C 1 -18-烷基或酰基; R 1和R 2均为H，酰基或具有R 3给出的含义之一; R 3是支链或直链C 1-18 - 烷基，其可以是未取代的或被-O - ， - NH-，-NR- ，-S-或被其它基团中断，三甲基甲硅烷基，卤代（CH 3）2 Si- [OSi（CH 3）3） （CH 3）3 Si- [OSi（CH 3）3） -COOH，-COO-R 10，-CO-NR， - ， - SO 2 - ， - 11- 12，-CO-乙烯基，-CO-苯基，苯基-C 1-4 - 烷基，苯基，萘基或联苯基，C