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公开(公告)号:US20230057214A1
公开(公告)日:2023-02-23
申请号:US17396242
申请日:2021-08-06
Applicant: The Boeing Company
Inventor: Patrick J. KINLEN , Dimitris Priftis
IPC: C09D5/24 , C09D175/04 , C09D129/14 , C09D133/04 , C09D163/00 , C09D167/00 , C09D171/12 , C09D181/04 , C09D7/65 , C09D7/20 , B64C7/00
Abstract: The present disclosure provides methods of coating a substrate. A method includes depositing a conductive coating including an electrically conductive material over the substrate to form a conductive layer having a sheet resistivity of about 10 Ω/□ to about 1000 Ω/□. The method includes depositing an anti-icing layer comprising nanomaterials over the conductive layer to form a coating system.
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公开(公告)号:US20230019695A1
公开(公告)日:2023-01-19
申请号:US17376618
申请日:2021-07-15
Applicant: The Boeing Company
Inventor: Kamaraj KANDHASAMY , Om PRAKASH , Patrick J. KINLEN , Stephen P. GAYDOS
Abstract: A conductive polymer coating composition including a conductive fibrillated structure and a base polymer, wherein the conductive fibrillated structure includes a fibrillated polymer and a conductive polymer grafted on the fibrillated polymer, and wherein the conductive polymer coating composition has an electrical conductivity from about 10−5 S/cm to about 10+1 S/cm and a thermal conductivity from about 1.1 W/m K to about 3 W/m K.
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公开(公告)号:US20220162384A1
公开(公告)日:2022-05-26
申请号:US17669450
申请日:2022-02-11
Applicant: THE BOEING COMPANY
Inventor: Patrick J. KINLEN , Matthew A. FLACK , Eric A. BRUTON
Abstract: The present disclosure provides polyanilines, articles thereof, and methods of forming polyanilines. In at least one aspect, a polyaniline has a thermal stability of about 100° C. or greater, a weight average molecular weight (Mw) of from about 50,000 g/mol to about 150,000 g/mol and a molecular weight distribution (Mw/Mn) of from about 1 to about 5. In at least one aspect, a film includes a polyaniline, the film having a hydrocarbon content of about 1 wt % or less, based on the total weight of the film. In at least one aspect, a method includes introducing an emulsion of an aqueous solution of an aniline and an alkyl-substituted aryl sulfonic acid having 1 wt % or less of hydrocarbon content into a flow reactor, the flow reactor having a length of tubing having an inner diameter. The method includes polymerizing the monomer within the tube to form a polyaniline.
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公开(公告)号:US20180208777A1
公开(公告)日:2018-07-26
申请号:US15414150
申请日:2017-01-24
Applicant: THE BOEING COMPANY
Inventor: Waynie M. SCHUETTE , Patrick J. KINLEN
IPC: C09D5/08 , C09D185/00 , B64D45/00
Abstract: Aspects described herein generally relate to a sol-gel that is the reaction product of a hydroxy organosilane, a metal alkoxide, an acid stabilizer, and a corrosion inhibitor. The hydroxy organosilane is represented by Formula (I): wherein R is selected from alkyl, cycloalkyl, ether, and aryl. The acid stabilizer is at a molar ratio of acid stabilizer to metal alkoxide of 1:1 or greater and the sol-gel has a pH from about 3 to about 4.
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公开(公告)号:US20240336785A1
公开(公告)日:2024-10-10
申请号:US18737608
申请日:2024-06-07
Applicant: THE BOEING COMPANY
Inventor: Patrick J. KINLEN
IPC: C09D5/24 , C09D7/20 , C09D179/02 , C09D183/04 , H05K1/03
CPC classification number: C09D5/24 , C09D7/20 , C09D179/02 , C09D183/04 , H05K1/0353
Abstract: Aspects of the present disclosure include compositions and methods of making and use thereof. In at least one aspect, a composition, includes a polyaniline and a polysiloxane having a density of about 1.05 g/cm3 or greater. The composition optionally includes a solvent. In at least one aspect, a method includes introducing a polyaniline with a polysiloxane having a density of about 1.05 g/cm3 or greater to form a composition. In at least one aspect, a method includes disposing a composition onto a substrate. The composition includes a polyaniline and a polysiloxane having a density of about 1.05 g/cm3 or greater.
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公开(公告)号:US20240084150A1
公开(公告)日:2024-03-14
申请号:US18258619
申请日:2021-12-21
Inventor: Patrick J. KINLEN , Eric Alan BRUTON , Thomas Matthew KOHL , Maria ESPIRITU
IPC: C09D5/24 , C09D5/18 , C09D7/20 , C09D7/40 , C09D7/48 , C09D7/62 , C09D7/63 , C09D179/02 , H01B1/12
CPC classification number: C09D5/24 , C09D5/18 , C09D7/20 , C09D7/48 , C09D7/62 , C09D7/63 , C09D7/69 , C09D179/02 , H01B1/128
Abstract: The present disclosure generally relates to coatings and compositions comprising conductive polymers. The present disclosure also relates to thermally stable coatings and compositions comprising solution processable polyaniline conducting polymers and thermal stability agents, and to processes for preparing the coatings and compositions.
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公开(公告)号:US20220112336A1
公开(公告)日:2022-04-14
申请号:US17407850
申请日:2021-08-20
Applicant: THE BOEING COMPANY
Inventor: Vijaykumar IJERI , Stephen P. GAYDOS , Patrick J. KINLEN
IPC: C08G73/02 , C08G59/24 , C08G59/50 , C08G59/44 , C08K3/22 , C08K3/36 , C08K5/098 , C08K5/3472 , C08K5/47 , C08K5/3437 , C08K5/378 , C08K5/42 , C08K3/32
Abstract: The present disclosure provides compositions, articles thereof, and methods of forming compositions. In at least one aspect, a composition includes (1) an epoxy, (2) an amino or amido hardener, (3) a polyaniline, (4) a dopant selected from a triazolyl, a thiazolyl, a quinolinyl, a salicylate, a benzoate, a glycolate, a phosphate, a sulfonate, an oxalate, or combination(s) thereof; and (5) a pigment selected from titanium dioxide, silica, talc, mica, aluminium stearate, or combination(s) thereof. The polyaniline+dopant comprises greater than 6 wt %, by weight of the composition. In at least one aspect, a method includes introducing an acid form of a polyaniline to a hydroxide to form a polyaniline hydroxide. The method includes introducing a dopant to the polyaniline hydroxide to form a doped polyaniline.
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公开(公告)号:US20210349008A1
公开(公告)日:2021-11-11
申请号:US17281164
申请日:2019-01-18
Applicant: The Boeing Company
Inventor: Patrick J. KINLEN , Waynie M. SCHUETTE
IPC: G01N17/02 , G01N33/44 , G01N27/403
Abstract: A system for measuring corrosion includes a first electrode configured to be connected to a first structure and a second electrode configured to be connected to a second structure. The first and second structures are galvanically-coupled together, and the first and second structures are made of different materials. A chamber is configured to run through one or more cycles while the first electrode, the first structure, the second electrode, and the second structure are positioned inside the chamber. A measurement device is configured to receive data from the first and second electrodes and to measure one or more parameters based at least partially upon the data. A level of corrosion on the first structure, the second structure, or both is configured to be determined based at least partially upon the one or more parameters.
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公开(公告)号:US20200325276A1
公开(公告)日:2020-10-15
申请号:US16818517
申请日:2020-03-13
Applicant: THE BOEING COMPANY
Inventor: Patrick J. KINLEN , Matthew A. FLACK , Eric A. BRUTON
Abstract: The present disclosure provides polyanilines, articles thereof, and methods of forming polyanilines. In at least one aspect, a polyaniline has a thermal stability of about 100° C. or greater, a weight average molecular weight (Mw) of from about 50,000 g/mol to about 150,000 g/mol and a molecular weight distribution (Mw/Mn) of from about 1 to about 5. In at least one aspect, a film includes a polyaniline, the film having a hydrocarbon content of about 1 wt % or less, based on the total weight of the film. In at least one aspect, a method includes introducing an emulsion of an aqueous solution of an aniline and an alkyl-substituted aryl sulfonic acid having 1 wt % or less of hydrocarbon content into a flow reactor, the flow reactor having a length of tubing having an inner diameter. The method includes polymerizing the monomer within the tube to form a polyaniline.
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公开(公告)号:US20200286640A1
公开(公告)日:2020-09-10
申请号:US16883629
申请日:2020-05-26
Applicant: THE BOEING COMPANY
Inventor: Patrick J. KINLEN , Daniel A. CHARLES
IPC: H01B1/12 , B32B27/08 , C09D7/61 , C09D7/40 , C09D7/62 , B64D45/02 , C09D5/24 , C09D125/18 , C09D133/00 , C09D153/00 , C09D163/00 , C09D165/00 , C09D175/04 , C09D179/02 , H01B1/04
Abstract: Methods of forming an electrically conductive carbon allotrope material comprise depositing a first material comprising a polymer and a sulfonic acid onto a carbon allotrope material to form a second material. The methods comprise curing the second material. Methods of heating a surface of a vehicle component comprise applying a voltage to a material comprising a carbon allotrope material, a polymer, and a sulfonic acid. The material is disposed on a surface of a vehicle component. Electrically conductive materials comprise at least one polymer, at least one sulfonic acid, and a carbon allotrope material.
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