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公开(公告)号：US3998764A
公开(公告)日：1976-12-21
申请号：US521501
申请日：1974-11-06
CPC分类号： C08G79/04 , C07F9/091 , C07F9/093 , C08G18/5084
摘要： Production of agents reducing the flammability of polyurethane moulding compositions. The agents are more particularly comprised of compounds of the following general formula (I) ##STR1## IN WHICH R stands for an alkylene radical having from 2 to 6 carbon atoms, which may be halogen-substituted, if desired, a --CH.sub.2 --CH.sub.2 --O--CH.sub.2 --CH.sub.2 -- radical, a phenylene radical or an alkyl- or halogenoalkyl-substituted diphenylene methane radical, R.sub.1 and R.sub.2, respectively, stand for a hydrogen atom, an alkyl radical or a halogen-substituted alkyl radical having from 1 to 4 carbon atoms, x + y stand for a number between 0.1 and 3, and n stands for 1 or 2.
摘要翻译： 生产降低聚氨酯模塑组合物的可燃性的试剂。 这些试剂更具体地由以下通式（I）的化合物组成：其中R代表具有2至6个碳原子的亚烷基，如果需要可以被卤素取代 ，-CH 2 -CH 2 -O-CH 2 -CH 2 - 基，亚苯基或烷基 - 或卤代烷基取代的亚苯基甲烷基，R 1和R 2分别代表氢原子，烷基或卤素取代 具有1至4个碳原子的烷基，x + y表示0.1至3之间的数，n表示1或2。
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公开(公告)号：US3978170A
公开(公告)日：1976-08-31
申请号：US521529
申请日：1974-11-06
摘要： Production of polyols containing halogen and phosphorus. The polyols are more particularly comprised of compounds the following general formula (I) ##EQU1## in which R stands for an alkylene radical having from 2 to 6 carbon atoms, which may be halogen-substituted, if desired, a --CH.sub.2 --CH.sub.2 --O--CH.sub.2 --CH.sub.2 -- radical, a phenylene radical or an alkyl- or halogenoalkyl-substituted diphenylene methane radical, R.sub.1 and R.sub.2, respectively stand for a hydrogen atom, an alkyl radical or a halogen-substituted alkyl radical having from 1 to 4 carbon atoms, x + y stand for a number between 0.1 and 3, and n stands for 1 or 2. The polyols find use as flameproofing agents in plastics, particularly in polyurethane foams.
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33.发明授权
公开(公告)号：US4347334A
公开(公告)日：1982-08-31
申请号：US231377
申请日：1981-02-04
CPC分类号： C08J9/009 , C08K9/10 , C09K21/12 , C09K21/14 , C08J2375/04
摘要： The invention relates to a particulate agent based on a free-flowing pulverulent ammonium polyphosphate for impeding the combustibility of combustible substances, the agent containing(a) about 75 to 99.9 weight % of ammonium polyphosphate and(b) about 0.1 to 25 weight % of a hardened, water-insoluble phenol resin (phenol/formaldehyde-resin) enveloping the individual ammonium polyphosphate particles.
摘要翻译： 本发明涉及一种基于自由流动的粉状多磷酸铵，用于阻止可燃物质的可燃性的颗粒剂，该试剂含有（a）约75-99.9重量％的多磷酸铵和（b）约0.1-25重量％的 包封单个多磷酸铵颗粒的硬化的水不溶性酚醛树脂（酚/甲醛树脂）。
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公开(公告)号：US4315961A
公开(公告)日：1982-02-16
申请号：US167219
申请日：1980-07-09
CPC分类号： B24D3/28 , C06F3/08 , Y10T428/3179 , Y10T428/31866
摘要： The invention relates to a process for making striking surfaces wherein red phosphorus, abrasive agents, and binders which are in the form of aqueous urea/formaldehyde or melamine/formaldehyde-condensates, are made into an aqueous suspension which is applied on to a striking surface substrate. More particularly, the suspension, based on the solid matter content of the condensates used as binder, is admixed with 5 to 20 weight %, calculated as solid matter, of an agent cross-linking the amine resin, the cross-linking agent being a polyester or copolymer produced by subjecting an acryl and/or methacryl ester to copolymerization with vinyl acetate in a ratio by weight of 1:9 to 9:1. A pH-value within the range 6.5 to 8.0 is established in the mixture, in the event of the cross-linking agent being a copolymer, or a pH-value within the range 7 to 11 is established, in the event of the cross-linking agent being a polyester.
摘要翻译： 本发明涉及一种制造冲击表面的方法，其中以尿素/甲醛水溶液或三聚氰胺/甲醛 - 缩合物的形式将红磷，研磨剂和粘合剂制成水性悬浮液， 基质。 更具体地，基于用作粘合剂的冷凝物的固体物质含量的悬浮液与作为固体物质的5至20重量％的交联胺树脂的试剂混合，交联剂为 通过使丙烯酰基和/或甲基丙烯酸酯与乙酸乙烯酯以1:9至9:1的重量比进行共聚而制备的聚酯或共聚物。 在交联剂为共聚物的情况下，或建立了7〜11的pH值的情况下，在混合物中建立pH值为6.5〜8.0的pH值， 交联剂为聚酯。
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公开(公告)号：US4170508A
公开(公告)日：1979-10-09
申请号：US919472
申请日：1978-06-27
CPC分类号： H05K1/0373 , B32B27/18 , C08K3/32 , H05K2201/012 , H05K2201/0284 , H05K2201/0293
摘要： Self-extinguishing laminates are made by an improved process, wherein individual layers of a carrier material are impregnated with a thermosetting phenolic resin containing a flame-retardant agent and the impregnated layers are placed one above another and bonded together by compressing them at elevated temperature and under elevated pressure to give a hardened laminate. More specifically, finely pulverulent phosphorus pentanitride as a flame-retarding agent is dispersed in the plasticized or non-plasticized thermosetting phenolic resin, with or without a diluent; the phenolic resin, based on its solid matter content, and the phosphorus pentanitride being used in an approximate ratio by weight of 100:4 to 100:15; and the phenolic resin, based on its solid matter content, and the carrier being used in an approximate ratio by weight of 100:80 to 100:150.
摘要翻译： 通过改进的方法制造自熄性层压体，其中载体材料的各层用含有阻燃剂的热固性酚醛树脂浸渍，并且将浸渍层一个放置在另一个上，并将其通过在高温下压缩而粘合在一起， 在高压下得到硬化层压板。 更具体地，作为阻燃剂的细粉状磷化磷酸铝分散在具有或不具有稀释剂的增塑或未塑化的热固性酚醛树脂中; 基于其固体物质含量的酚醛树脂和近似重量比为100:4至100:15使用的五氮化磷; 和酚醛树脂，基于其固体成分含量，载体的使用重量比约为100:80至100:50。
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公开(公告)号：US4166743A
公开(公告)日：1979-09-04
申请号：US873974
申请日：1978-01-31
CPC分类号： C09K21/04 , C09D5/185 , Y10S260/24 , Y10S428/921
摘要： Intumescent flame-retardant coating composition consisting substantially of a film-forming agent, an ammonium polyphosphate, one or more substances which are carbonizable under the action of heat, a dispersant, and optionally a filler. The coating composition additionally contains an ammonium polyphosphate activator weighing 0.5 to 50% of the weight of ammonium polyphosphate. The activator is constituted by at least one salt which contains water of crystallization which is liberated upon the composition being heated to about 35.degree. C.
摘要翻译： 基本上由成膜剂，多磷酸铵，一种或多种在加热作用下可碳化的物质，分散剂和任选的填料组成的膨胀型阻燃涂料组合物。 涂料组合物另外含有重量为聚磷酸铵重量的0.5-50％的聚磷酸铵活化剂。 活化剂由至少一种含有结晶水的盐构成，该组合物被加热至约35℃时释放。
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公开(公告)号：US4097656A
公开(公告)日：1978-06-27
申请号：US674573
申请日：1976-04-07
IPC分类号： C08K3/00 , C08K3/02 , C08K3/04 , C08L1/00 , C08L23/00 , C08L27/00 , C08L101/00 , C09C1/56 , C09K3/16
CPC分类号： C09C1/56 , C08K3/04 , C09K3/16 , C01P2006/10 , C01P2006/12 , C01P2006/40 , Y10S524/91
摘要： Antistatic properties are imparted to plastics by blending a pulverulent plastics material and, if desired further addends, with conductive carbon black and making the resulting blend into a moulding composition. The plastics are more particularly blended with 4 to 12 weight % of conductive carbon black having a water absorption stiffness (AS-number) of 15 to 35, a specific electric resistance of 10.sup.-1 up to 10.sup.-3 ohms . cm under a moulding pressure of 100 to 180 atmospheres absolute, a bulk density of 100 to 180 g/liter, a BET-surface area of 100 to 1000 m.sup.2 /g. The carbon black is made by a process wherein an aqueous suspension of carbon black having an AS-number higher than 15 is intimately blended at temperatures within the range 5.degree. and 120.degree. C, under pressure within the range 1 and 20 atmospheres absolute, in liquid phase at a pH-value of 7 to 10, and for a period of 1 to 20 minutes, with vaporizable liquid aliphatic or cycloaliphatic hydrocarbons, the carbon black is separated from liquid matter, then heated and thereby freed from hydrocarbons and water, and finally annealed for 20 to 30 minutes at 200.degree. up to 2200.degree. C. The aqueous suspension is prepared by subjecting hydrocarbons, which are liquid at room temperature, to thermal conversion at 1200.degree. to 2000.degree. C, under pressures within the range 1 and 80 atmospheres absolute, and in the presence of oxygen or an oxygen-containing gas, and water scrubbing the resulting carbon black-containing reaction gas.
摘要翻译： 通过将粉状塑料材料和如果需要的话进一步加成物与导电炭黑混合并将所得共混物制成模塑组合物，赋予塑料抗静电性能。 塑料更具体地与4至12重量％的吸水刚度（AS-数）为15至35，比电阻为10-1至10-3欧姆的导电炭黑共混。 在100至180绝对大气压的模制压力下，堆积密度为100至180g /升，BET表面积为100至1000m2 / g。 炭黑通过以下方法制备，其中AS值高于15的炭黑的水性悬浮液在5℃和120℃的温度下，在1和20大气压绝对压力范围内，在 液相，pH值为7〜10，时间为1〜20分钟，用可汽化的液体脂族或脂环族烃，将炭黑与液体物质分离，然后加热，从而从碳氢化合物和水中除去， 最后在200℃至2200℃下退火20分钟至30分钟。水悬浮液是通过在室温下将液体烃在1200℃至2000℃下，在1℃范围内的压力下进行热转化， 80个绝对大气压，在氧气或含氧气体的存在下，水洗涤所得含炭黑反应气体。
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