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    Process for preparing allyl alcohol alkoxylates
    32.
    发明授权
    Process for preparing allyl alcohol alkoxylates 有权
    制备烯丙醇烷氧基化物的方法

    公开(公告)号：US09073836B2

    公开(公告)日：2015-07-07

    申请号：US13197336

    申请日：2011-08-03

    申请人： Markus Klumpe ,  Thomas Ostrowski ,  Matthias Zipplies

    发明人： Markus Klumpe ,  Thomas Ostrowski ,  Matthias Zipplies

    IPC分类号： C07C41/03 ,  C08G65/26

    CPC分类号： C07C41/03 ,  C08G65/2696 ,  C07C43/1785

    摘要： A process for preparing polyether alcohols by reacting one or more unsaturated starters having at least one active hydrogen atom per molecule with one or more alkylene oxides in the liquid phase in the presence of a basic catalyst in a reactor, wherein the one or more alkylene oxides are introduced into the reactor in such a way that the concentration of unreacted alkylene oxide in the liquid reaction mixture in the reactor is increased as far as possible with increasing degree of addition of the alkylene oxide onto the starter, with the proviso that the temperature at the end of a runaway reaction is at any point in time at least 100 K below the onset temperature of the decomposition reaction of the liquid reaction mixture, is proposed.

    摘要翻译： 一种制备聚醚醇的方法，其通过使反应器中碱性催化剂存在下，使每一分子中具有至少一个活性氢原子的一种或多种不饱和起始物与液相中的一种或多种烯化氧反应，其中所述一种或多种烯化氧 以使得反应器中的液体反应混合物中未反应的烯化氧的浓度尽可能地增加到起始物上的环氧烷加成程度增加的方式引入反应器，条件是温度在 失控反应的结束是在液体反应混合物的分解反应的起始温度以下至少100K的任何时间点。

    METHOD FOR PRODUCING POLYETHER POLYOLS
    40.
    发明申请
    METHOD FOR PRODUCING POLYETHER POLYOLS 失效
    生产聚醚多元醇的方法

    公开(公告)号：US20090203874A1

    公开(公告)日：2009-08-13

    申请号：US12302162

    申请日：2007-05-22

    申请人： Achim Löffler ,  Wolfgang Loth ,  Ralf Böhling ,  Thomas Ostrowski ,  Michael Stösser ,  Hartwig Voss ,  Axel Schimpf

    发明人： Achim Löffler ,  Wolfgang Loth ,  Ralf Böhling ,  Thomas Ostrowski ,  Michael Stösser ,  Hartwig Voss ,  Axel Schimpf

    IPC分类号： C08G65/02 ,  C08G65/28

    CPC分类号： C08G65/2696 ,  C08G18/4866

    摘要： A process for preparing polyether polyols by reaction of the following starting materials: a) one or more alkylene oxides and, if appropriate, carbon dioxide and also b) one or more H-functional starter substances, in the presence of a catalyst, in a reaction unit having a plurality of parallel layers A, B which are microstructured so that each layer has a multiplicity of channels which are arranged parallel to one another and form a continuous flow path from one side of the plate to the opposite side of this, wherein a distribution device for introduction of the starting materials and the catalyst is provided at one end of the channels of the layers A and a collection device for the reaction mixture is provided at the other end of these is proposed.

    摘要翻译： 一种通过以下原料反应制备聚醚多元醇的方法：a）一种或多种环氧烷烃，如果合适的话，二氧化碳，以及b）一种或多种H官能起始物质，在催化剂存在下，在 反应单元具有多个平行层A，B，它们被微结构化，使得每个层具有多个彼此平行布置的通道，并形成从板的一侧到其相反侧的连续流动路径，其中 在层A的通道的一端设置用于引入起始材料和催化剂的分配装置，并且在另一端提供了用于反应混合物的收集装置。