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    Process for the preparation of polyether alcohols from unsaturated starters having active hydrogen atoms
    1.
    发明授权
    Process for the preparation of polyether alcohols from unsaturated starters having active hydrogen atoms 有权
    从具有活性氢原子的不饱和起始物制备聚醚醇的方法

    公开(公告)号：US08399608B2

    公开(公告)日：2013-03-19

    申请号：US12681789

    申请日：2007-10-25

    申请人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    发明人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    IPC分类号： C08G65/10 ,  C08G65/30 ,  C08G65/34 ,  C08F8/06 ,  C08F6/08

    CPC分类号： C08G65/2609 ,  C08G65/2648 ,  C08G65/2696

    摘要： A process for the preparation of polyether alcohols by reacting at least one alkylene oxide with at least one unsaturated starter having at least one active hydrogen atom per molecule under basic catalysis, that the alkoxylation is carried out in at least two stages, in stage (I) the alkoxylation of the starter or starters being carried out with not more than 10 mol of alkylene oxide per mole of starter with a catalyst concentration of not more than 0.0085 mol of basic catalyst per mole and in stage (II) and the optionally following stages, the alkoxylated starter or starters from stage (I) being reacted with further alkylene oxide at a catalyst concentration of at least 0.01 mol of basic catalyst per mole of starter.

    摘要翻译： 通过在碱性催化下使至少一种烯化氧与至少一种具有至少一个活性氢原子的不饱和起始物在每个分子中反应来制备聚醚醇的方法，该烷氧基化在至少两个阶段中在阶段（I ）起始物或起动器的烷氧基化作用，每摩尔起始物不超过10摩尔环氧烷烃，每摩尔催化剂浓度不大于0.0085摩尔碱性催化剂和（II）阶段和任选的后续阶段 ，来自阶段（I）的烷氧基​​化起始物或起始物与另外的烯化氧反应，每摩尔起始物的催化剂浓度为至少0.01摩尔碱性催化剂。

    Process for preparing allyl alcohol alkoxylates
    2.
    发明授权
    Process for preparing allyl alcohol alkoxylates 有权
    制备烯丙醇烷氧基化物的方法

    公开(公告)号：US09073836B2

    公开(公告)日：2015-07-07

    申请号：US13197336

    申请日：2011-08-03

    申请人： Markus Klumpe ,  Thomas Ostrowski ,  Matthias Zipplies

    发明人： Markus Klumpe ,  Thomas Ostrowski ,  Matthias Zipplies

    IPC分类号： C07C41/03 ,  C08G65/26

    CPC分类号： C07C41/03 ,  C08G65/2696 ,  C07C43/1785

    摘要： A process for preparing polyether alcohols by reacting one or more unsaturated starters having at least one active hydrogen atom per molecule with one or more alkylene oxides in the liquid phase in the presence of a basic catalyst in a reactor, wherein the one or more alkylene oxides are introduced into the reactor in such a way that the concentration of unreacted alkylene oxide in the liquid reaction mixture in the reactor is increased as far as possible with increasing degree of addition of the alkylene oxide onto the starter, with the proviso that the temperature at the end of a runaway reaction is at any point in time at least 100 K below the onset temperature of the decomposition reaction of the liquid reaction mixture, is proposed.

    摘要翻译： 一种制备聚醚醇的方法，其通过使反应器中碱性催化剂存在下，使每一分子中具有至少一个活性氢原子的一种或多种不饱和起始物与液相中的一种或多种烯化氧反应，其中所述一种或多种烯化氧 以使得反应器中的液体反应混合物中未反应的烯化氧的浓度尽可能地增加到起始物上的环氧烷加成程度增加的方式引入反应器，条件是温度在 失控反应的结束是在液体反应混合物的分解反应的起始温度以下至少100K的任何时间点。

    PROCESS FOR THE PREPARATION OF POLYETHER ALCOHOLS FROM UNSATURATED STARTERS HAVING ACTIVE HYDROGEN ATOMS
    3.
    发明申请
    PROCESS FOR THE PREPARATION OF POLYETHER ALCOHOLS FROM UNSATURATED STARTERS HAVING ACTIVE HYDROGEN ATOMS 有权
    从具有活性氢原子的不饱和起动器制备聚醚醇的方法

    公开(公告)号：US20100216968A1

    公开(公告)日：2010-08-26

    申请号：US12681789

    申请日：2007-10-25

    申请人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    发明人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    IPC分类号： C08G65/26

    CPC分类号： C08G65/2609 ,  C08G65/2648 ,  C08G65/2696

    摘要： A process for the preparation of polyether alcohols by reacting at least one alkylene oxide with at least one unsaturated starter having at least one active hydrogen atom per molecule under basic catalysis, that the alkoxylation is carried out in at least two stages, in stage (I) the alkoxylation of the starter or starters being carried out with not more than 10 mol of alkylene oxide per mole of starter with a catalyst concentration of not more than 0.0085 mol of basic catalyst per mole and in stage (II) and the optionally following stages, the alkoxylated starter or starters from stage (I) being reacted with further alkylene oxide at a catalyst concentration of at least 0.01 mol of basic catalyst per mole of starter.

    摘要翻译： 通过在碱性催化下使至少一种烯化氧与至少一种具有至少一个活性氢原子的不饱和起始物在每个分子中反应来制备聚醚醇的方法，该烷氧基化在至少两个阶段中在阶段（I ）起始物或起动器的烷氧基化作用，每摩尔起始物不超过10摩尔环氧烷烃，每摩尔催化剂浓度不大于0.0085摩尔碱性催化剂和（II）阶段和任选的后续阶段 ，来自阶段（I）的烷氧基​​化起始物或起始物与另外的烯化氧反应，每摩尔起始物的催化剂浓度为至少0.01摩尔碱性催化剂。

    METHOD FOR PRODUCING MONOHYDROXYPOLYALKYLENE OXIDES
    5.
    发明申请
    METHOD FOR PRODUCING MONOHYDROXYPOLYALKYLENE OXIDES 有权
    生产单羟基烷基亚甲基氧化物的方法

    公开(公告)号：US20120078019A1

    公开(公告)日：2012-03-29

    申请号：US13322743

    申请日：2010-06-16

    申请人： Markus Klumpe ,  Matthias Zipplies

    发明人： Markus Klumpe ,  Matthias Zipplies

    IPC分类号： C07C41/03

    CPC分类号： C08G65/2609 ,  C08G65/2612 ,  C08G65/2645

    摘要： The present invention relates to a process for the preparation of monohydroxypolyalkylene oxides (MPAO) which are substantially free of diols, comprising the reaction of at least one monoalcohol as a starter with at least one alkylene oxide in the presence of at least one basic catalyst, the catalyst being used as a solution in water or alcohol or in solvent mixtures which comprise water and/or alcohol.

    摘要翻译： 本发明涉及一种制备基本上不含二醇的单羟基聚环氧烷（MPAO）的方法，包括至少一种一元醇作为起始物与至少一种烯化氧在至少一种碱性催化剂存在下的反应， 该催化剂用作在水或醇或包含水和/或醇的溶剂混合物中的溶液。

    C10 alkanolalkoxylate mixtures and use thereof as novel low-foaming wetting agents
    8.
    发明申请
    C10 alkanolalkoxylate mixtures and use thereof as novel low-foaming wetting agents 有权
    C10链烷醇烷氧基化物混合物及其作为新型低泡润湿剂的用途

    公开(公告)号：US20070065391A1

    公开(公告)日：2007-03-22

    申请号：US10575760

    申请日：2004-10-14

    申请人： Markus Klumpe ,  Jurgen Tropsch ,  Dieter Kahl ,  Roland Bohn ,  Susanne Stutz ,  Ralf Norenberg

    发明人： Markus Klumpe ,  Jurgen Tropsch ,  Dieter Kahl ,  Roland Bohn ,  Susanne Stutz ,  Ralf Norenberg

    IPC分类号： C07C41/03 ,  A61K8/33

    CPC分类号： C11D3/0026 ,  C07C43/11 ,  C11D1/72 ,  C11D1/722 ,  C11D1/8255

    摘要： The alkoxylate mixtures comprise alkoxylates of the formula (I) C5H11CH(C3H7)CH2O(B)p(A)n(B)m(A)qH  (I) where A is ethyleneoxy, B, in each case independently, are C3-10-alkyleneoxy or mixtures thereof, groups A and B being present in the form of blocks in the stated sequence, p is a number from 0 to 10, n is a number greater than 0 to 20, m is a number greater than 0 to 20, q is a number greater than 0 to 10, p+n+m+q is at least 1, from 70 to 99% by weight of alkoxylates A1, in which C5H11 is n-C5H11, and from 1 to 30% by weight of alkoxylates A2, in which C5H11 is C2H5CH(CH3)CH2 and/or CH3CH(CH3)CH2CH2, being present in the mixture.

    摘要翻译： 烷氧基化物混合物包括式（I）的烷氧基​​化物：在线式描述=“In-line Formulas”end =“lead”→> 5 （C 3 H 2）（CH 3）H（O）B（A）N （B）m（A）H（I）<？in-line-formula description =“In-line Formulas”end =“tail” 其中A是亚乙基氧基，B在每种情况下独立地是C 3-10 - 亚烷基氧基或其混合物，基团A和B以所述序列以块的形式存在，p是 0至10的数，n为大于0至20的数，m为大于0至20的数，q为大于0至10的数，p + n + m + q至少为1，从 70重量％至99重量％的烷氧基化物A1，其中C 5 H 11 N 11是n C 5 H 11， 和1至30重量％的烷氧基化物A2，其中C 5 H 11 H 11是C 2 H 5 H CH（CH 3 CH 3）CH 2和/或CH 3 CH（CH 3 CH 3）CH 3 2 2， 存在于混合物中。

    Comb Polymers and Their Use as Additives for Preparations of Mineral Binders
    9.
    发明申请
    Comb Polymers and Their Use as Additives for Preparations of Mineral Binders 有权
    梳子聚合物及其作为添加剂用于矿物粘合剂的制备

    公开(公告)号：US20080300343A1

    公开(公告)日：2008-12-04

    申请号：US12092586

    申请日：2006-11-06

    申请人： Stefan Becker ,  Markus Klumpe ,  Joachim Pakusch ,  Thomas Gotz ,  Christian Knoll ,  Rolf Gulden

    发明人： Stefan Becker ,  Markus Klumpe ,  Joachim Pakusch ,  Thomas Gotz ,  Christian Knoll ,  Rolf Gulden

    IPC分类号： C08K3/00 ,  C08G63/02 ,  C08G69/26

    CPC分类号： C08F283/06 ,  C04B24/2647 ,  C04B24/2658 ,  C04B28/02 ,  C04B28/14 ,  C04B2103/006 ,  C04B2103/32 ,  C08F290/00 ,  C08F290/142 ,  C08L51/08 ,  C04B24/18 ,  C04B24/2676 ,  C04B24/383 ,  C04B24/226 ,  C04B24/2641 ,  C04B24/32 ,  C08L2666/02

    摘要： The present invention relates to novel comb polymers which bear poly-C2-C4-alkylene ether side chains A and functional groups B which at a pH of >12 are present in the form of anionic groups on a carbon backbone and also the salts of such comb polymers. The invention also relates to the use of these comb polymers as additives in preparations comprising a mineral binder. The polyalkylene ether side chains A have the following formula: *—U—(C(O))k—X-(Alk-O)n—Y-Z  A where * indicates the point of bonding to the carbon backbone of the comb polymer, U is a chemical bond or an alkylene group having from 1 to 8 carbon atoms, X is oxygen or an NR group, k is 0 or 1, n is an integer whose average value, based on the comb polymer, is in the range from 5 to 300, Alk is C2-C4-alkylene, with the Alk radicals within the group (Alk-O)n being able to be identical or different, Y is a linear or branched alkylene group which has from 2 to 8 carbon atoms and may bear a phenyl ring, Z is a 5- to 10-membered nitrogen heterocycle which is bound via nitrogen and can have, in addition to the nitrogen atom and carbon atoms, 1, 2 or 3 additional heteroatoms selected from among oxygen, nitrogen and sulfur as ring members, with the nitrogen ring members being able to bear a group R′ and 1 or 2 carbon ring members being able to be present as carbonyl groups, R is hydrogen, C1-C4-alkyl or benzyl and R′ is hydrogen, C1-C4-alkyl or benzyl.

    摘要翻译： 本发明涉及具有聚-C2-C4-亚烷基醚侧链A和官能团B的新型梳状聚合物，其pH> 12是以碳骨架上的阴离子基团的形式存在，以及其中的盐 梳状聚合物。 本发明还涉及这些梳状聚合物作为添加剂在包含矿物粘合剂的制剂中的用途。 聚亚烷基醚侧链A具有以下公式：<？in-line-formula description =“In-line formula”end =“lead”？> * - U-（C（O））kX-（Alk-O） nYZ A <？in-line-formula description =“In-line Formulas”end =“tail”？>其中*表示与梳形聚合物的碳骨架键合的点，U是化学键或具有 1〜8个碳原子，X为氧或NR基，k为0或1，n为基于梳形聚合物的平均值为5〜300的整数，Alk为C2-C4- 亚烷基，其中基团中的Alk基团（Alk-O）n能够相同或不同，Y是具有2至8个碳原子并且可以带有苯环的直链或支链亚烷基，Z是5 至10元氮杂环，其通过氮结合并且除了氮原子和碳原子之外，还可以具有1,2或3个选自氧，氮和硫作为环成员的另外的杂原子，与氮环成员 贝宁 能够承载能够以羰基存在的基团R'和1或2个碳环成员，R是氢，C 1 -C 4 - 烷基或苄基，R'是氢，C 1 -C 4 - 烷基或苄基。

    C10 alkanolalkoxylate mixtures and use thereof as novel low-foaming wetting agents
    10.
    发明授权
    C10 alkanolalkoxylate mixtures and use thereof as novel low-foaming wetting agents 有权
    C10链烷醇烷氧基化物混合物及其作为新型低泡润湿剂的用途

    公开(公告)号：US08519196B2

    公开(公告)日：2013-08-27

    申请号：US10575760

    申请日：2004-10-14

    申请人： Markus Klumpe ,  Juergen Tropsch ,  Rolf-Dieter Kahl ,  Roland Boehn ,  Susanne Stutz ,  Ralf Noerenberg

    发明人： Markus Klumpe ,  Juergen Tropsch ,  Rolf-Dieter Kahl ,  Roland Boehn ,  Susanne Stutz ,  Ralf Noerenberg

    IPC分类号： C11D3/20

    CPC分类号： C11D3/0026 ,  C07C43/11 ,  C11D1/72 ,  C11D1/722 ,  C11D1/8255

    摘要： The alkoxylate mixtures comprise alkoxylates of the formula (I) C5H11CH(C3H7)CH2O(B)p(A)n(B)m(A)qH  (I) where A is ethyleneoxy, B, in each case independently, are C3-10-alkyleneoxy or mixtures thereof, groups A and B being present in the form of blocks in the stated sequence, p is a number from 0 to 10, n is a number greater than 0 to 20, m is a number greater than 0 to 20, q is a number greater than 0 to 10, p+n+m+q is at least 1, from 70 to 99% by weight of alkoxylates A1, in which C5H11 is n-C5H11, and from 1 to 30% by weight of alkoxylates A2, in which C5H11 is C2H5CH(CH3)CH2 and/or CH3CH(CH3)CH2CH2, being present in the mixture.

    摘要翻译： 烷氧基化物混合物包括式（I）的烷氧基​​化物：C 5 H 11 CH（C 3 H 7）CH 2 O（B）p（A）n（B）m（A）qH（I）其中A是亚乙基氧基，B各自独立地是C3- 10-亚烷基氧基或其混合物，基团A和B以所述顺序以嵌段的形式存在，p为0至10的数，n为大于0至20的数，m为大于0至 20，q是大于0至10的数，p + n + m + q至少为1，70至99重量％的烷氧基化物A1，其中C5H11为n-C5H11，1〜30％为 其中C5H11是C2H5CH（CH3）CH2和/或CH3CH（CH3）CH2CH2）的烷氧基​​化物A2的重量存在于混合物中。