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    PROCESS FOR PREPARING ALLYL ALCOHOL ALKOXYLATES
    1.
    发明申请
    PROCESS FOR PREPARING ALLYL ALCOHOL ALKOXYLATES 有权
    制备全部醇金酸盐的方法

    公开(公告)号：US20120035381A1

    公开(公告)日：2012-02-09

    申请号：US13197336

    申请日：2011-08-03

    申请人： Markus KLUMPE ,  Thomas Ostrowski ,  Matthias Zipplies

    发明人： Markus KLUMPE ,  Thomas Ostrowski ,  Matthias Zipplies

    IPC分类号： C07C41/03

    CPC分类号： C07C41/03 ,  C08G65/2696 ,  C07C43/1785

    摘要： A process for preparing polyether alcohols by reacting one or more unsaturated starters having at least one active hydrogen atom per molecule with one or more alkylene oxides in the liquid phase in the presence of a basic catalyst in a reactor, wherein the one or more alkylene oxides are introduced into the reactor in such a way that the concentration of unreacted alkylene oxide in the liquid reaction mixture in the reactor is increased as far as possible with increasing degree of addition of the alkylene oxide onto the starter, with the proviso that the temperature at the end of a runaway reaction is at any point in time at least 100 K below the onset temperature of the decomposition reaction of the liquid reaction mixture, is proposed.

    摘要翻译： 一种制备聚醚醇的方法，其通过使反应器中碱性催化剂存在下，使每一分子中具有至少一个活性氢原子的一种或多种不饱和起始物与液相中的一种或多种烯化氧反应，其中所述一种或多种烯化氧 以使得反应器中的液体反应混合物中未反应的烯化氧的浓度尽可能地增加到起始物上的环氧烷加成程度增加的方式引入反应器，条件是温度在 失控反应的结束是在液体反应混合物的分解反应开始温度以下至少100K的任何时间点。

    Process for the preparation of polyether alcohols from unsaturated starters having active hydrogen atoms
    2.
    发明授权
    Process for the preparation of polyether alcohols from unsaturated starters having active hydrogen atoms 有权
    从具有活性氢原子的不饱和起始物制备聚醚醇的方法

    公开(公告)号：US08399608B2

    公开(公告)日：2013-03-19

    申请号：US12681789

    申请日：2007-10-25

    申请人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    发明人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    IPC分类号： C08G65/10 ,  C08G65/30 ,  C08G65/34 ,  C08F8/06 ,  C08F6/08

    CPC分类号： C08G65/2609 ,  C08G65/2648 ,  C08G65/2696

    摘要： A process for the preparation of polyether alcohols by reacting at least one alkylene oxide with at least one unsaturated starter having at least one active hydrogen atom per molecule under basic catalysis, that the alkoxylation is carried out in at least two stages, in stage (I) the alkoxylation of the starter or starters being carried out with not more than 10 mol of alkylene oxide per mole of starter with a catalyst concentration of not more than 0.0085 mol of basic catalyst per mole and in stage (II) and the optionally following stages, the alkoxylated starter or starters from stage (I) being reacted with further alkylene oxide at a catalyst concentration of at least 0.01 mol of basic catalyst per mole of starter.

    摘要翻译： 通过在碱性催化下使至少一种烯化氧与至少一种具有至少一个活性氢原子的不饱和起始物在每个分子中反应来制备聚醚醇的方法，该烷氧基化在至少两个阶段中在阶段（I ）起始物或起动器的烷氧基化作用，每摩尔起始物不超过10摩尔环氧烷烃，每摩尔催化剂浓度不大于0.0085摩尔碱性催化剂和（II）阶段和任选的后续阶段 ，来自阶段（I）的烷氧基​​化起始物或起始物与另外的烯化氧反应，每摩尔起始物的催化剂浓度为至少0.01摩尔碱性催化剂。

    Process for preparing allyl alcohol alkoxylates
    3.
    发明授权
    Process for preparing allyl alcohol alkoxylates 有权
    制备烯丙醇烷氧基化物的方法

    公开(公告)号：US09073836B2

    公开(公告)日：2015-07-07

    申请号：US13197336

    申请日：2011-08-03

    申请人： Markus Klumpe ,  Thomas Ostrowski ,  Matthias Zipplies

    发明人： Markus Klumpe ,  Thomas Ostrowski ,  Matthias Zipplies

    IPC分类号： C07C41/03 ,  C08G65/26

    CPC分类号： C07C41/03 ,  C08G65/2696 ,  C07C43/1785

    摘要： A process for preparing polyether alcohols by reacting one or more unsaturated starters having at least one active hydrogen atom per molecule with one or more alkylene oxides in the liquid phase in the presence of a basic catalyst in a reactor, wherein the one or more alkylene oxides are introduced into the reactor in such a way that the concentration of unreacted alkylene oxide in the liquid reaction mixture in the reactor is increased as far as possible with increasing degree of addition of the alkylene oxide onto the starter, with the proviso that the temperature at the end of a runaway reaction is at any point in time at least 100 K below the onset temperature of the decomposition reaction of the liquid reaction mixture, is proposed.

    摘要翻译： 一种制备聚醚醇的方法，其通过使反应器中碱性催化剂存在下，使每一分子中具有至少一个活性氢原子的一种或多种不饱和起始物与液相中的一种或多种烯化氧反应，其中所述一种或多种烯化氧 以使得反应器中的液体反应混合物中未反应的烯化氧的浓度尽可能地增加到起始物上的环氧烷加成程度增加的方式引入反应器，条件是温度在 失控反应的结束是在液体反应混合物的分解反应的起始温度以下至少100K的任何时间点。

    PROCESS FOR THE PREPARATION OF POLYETHER ALCOHOLS FROM UNSATURATED STARTERS HAVING ACTIVE HYDROGEN ATOMS
    4.
    发明申请
    PROCESS FOR THE PREPARATION OF POLYETHER ALCOHOLS FROM UNSATURATED STARTERS HAVING ACTIVE HYDROGEN ATOMS 有权
    从具有活性氢原子的不饱和起动器制备聚醚醇的方法

    公开(公告)号：US20100216968A1

    公开(公告)日：2010-08-26

    申请号：US12681789

    申请日：2007-10-25

    申请人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    发明人： Georg Heinrich Grosch ,  Matthias Zipplies ,  Thomas Ostrowski ,  Ulrich Annen ,  Markus Klumpe

    IPC分类号： C08G65/26

    CPC分类号： C08G65/2609 ,  C08G65/2648 ,  C08G65/2696

    摘要： A process for the preparation of polyether alcohols by reacting at least one alkylene oxide with at least one unsaturated starter having at least one active hydrogen atom per molecule under basic catalysis, that the alkoxylation is carried out in at least two stages, in stage (I) the alkoxylation of the starter or starters being carried out with not more than 10 mol of alkylene oxide per mole of starter with a catalyst concentration of not more than 0.0085 mol of basic catalyst per mole and in stage (II) and the optionally following stages, the alkoxylated starter or starters from stage (I) being reacted with further alkylene oxide at a catalyst concentration of at least 0.01 mol of basic catalyst per mole of starter.

    摘要翻译： 通过在碱性催化下使至少一种烯化氧与至少一种具有至少一个活性氢原子的不饱和起始物在每个分子中反应来制备聚醚醇的方法，该烷氧基化在至少两个阶段中在阶段（I ）起始物或起动器的烷氧基化作用，每摩尔起始物不超过10摩尔环氧烷烃，每摩尔催化剂浓度不大于0.0085摩尔碱性催化剂和（II）阶段和任选的后续阶段 ，来自阶段（I）的烷氧基​​化起始物或起始物与另外的烯化氧反应，每摩尔起始物的催化剂浓度为至少0.01摩尔碱性催化剂。

    METHOD FOR PRODUCING MONOHYDROXYPOLYALKYLENE OXIDES
    7.
    发明申请
    METHOD FOR PRODUCING MONOHYDROXYPOLYALKYLENE OXIDES 有权
    生产单羟基烷基亚甲基氧化物的方法

    公开(公告)号：US20120078019A1

    公开(公告)日：2012-03-29

    申请号：US13322743

    申请日：2010-06-16

    申请人： Markus Klumpe ,  Matthias Zipplies

    发明人： Markus Klumpe ,  Matthias Zipplies

    IPC分类号： C07C41/03

    CPC分类号： C08G65/2609 ,  C08G65/2612 ,  C08G65/2645

    摘要： The present invention relates to a process for the preparation of monohydroxypolyalkylene oxides (MPAO) which are substantially free of diols, comprising the reaction of at least one monoalcohol as a starter with at least one alkylene oxide in the presence of at least one basic catalyst, the catalyst being used as a solution in water or alcohol or in solvent mixtures which comprise water and/or alcohol.

    摘要翻译： 本发明涉及一种制备基本上不含二醇的单羟基聚环氧烷（MPAO）的方法，包括至少一种一元醇作为起始物与至少一种烯化氧在至少一种碱性催化剂存在下的反应， 该催化剂用作在水或醇或包含水和/或醇的溶剂混合物中的溶液。

    N,N'-disubstituted piperazines
    9.
    发明授权
    N,N'-disubstituted piperazines 失效
    N，N'-二取代哌嗪

    公开(公告)号：US4935426A

    公开(公告)日：1990-06-19

    申请号：US307525

    申请日：1989-02-08

    申请人： Matthias Zipplies ,  Hubert Sauter ,  Franz Roehl ,  Thomas Kuekenhoehner ,  Lothar Janitschke ,  Eberhard Ammermann ,  Gisela Lorenz

    发明人： Matthias Zipplies ,  Hubert Sauter ,  Franz Roehl ,  Thomas Kuekenhoehner ,  Lothar Janitschke ,  Eberhard Ammermann ,  Gisela Lorenz

    IPC分类号： C07D295/02 ,  A01N43/60 ,  C07D295/03 ,  C07D295/033 ,  C07D295/067 ,  C07D295/08

    CPC分类号： C07D295/067 ,  A01N43/60 ,  C07D295/03 ,  C07D295/033

    摘要： N,N'-disubstituted piperazines of the general formula I ##STR1## where the group is unsaturated (.dbd.) or saturated (--) and the substituents R.sup.1, R.sup.2 and A have the following meanings:A is --, --CH.dbd., --CH.sub.2 --, --CH.sub.2 --CH.sub.2 --,R.sup.1 is alkyl, alkenyl, alkynyl, cycloalkyl, cycloalkenyl, alkylcycloalkyl, cycloalkenylalkyl, alkylcycloalkenyl, bicycloalkyl, bicycloalkylalkyl or alkylbicycloalkyl, these radicals being unsubstituted or substituted by hydroxy, halogen, alkoxy or trialkylsilyl,R.sup.1 is further heterocycloalkyl with oxygen and/or sulfur, heterocycloalkylmethyl with oxygen and/or sulfur, alkyl-substituted heterocycloalkylmethyl with oxygen and/or sulfur, andR.sup.2 is alkyl, alkoxy, trimethylsilyl, cycloalkyl, alkylthio,and plant-physiologically tolerated salts thereof, and fungicides containing these compounds.

    摘要翻译： 通式I的N，N'-二取代的哌嗪（1）其中基团是不饱和的（=）或饱和的（ - ），取代基R 1，R 2和A具有以下含义：A是 - ， - CH =，-CH 2 - ， - CH 2 -CH 2 - ，R 1是烷基，烯基，炔基，环烷基，环烯基，烷基环烷基，环烯基烷基，烷基环烯基，双环烷基，双环烷基烷基或烷基双环烷基，这些基团是未取代的或被羟基，卤素，烷氧基或三烷基甲硅烷基 ，R 1为氧和/或硫的杂环烷基，与氧和/或硫的杂环烷基甲基，与氧和/或硫的烷基取代的杂环烷基甲基，R 2为烷基，烷氧基，三甲基甲硅烷基，环烷基，烷硫基和植物生理耐受盐 和含有这些化合物的杀真菌剂。

    Synergistic triazole compounds
    10.
    发明授权
    Synergistic triazole compounds 失效
    协同三唑化合物

    公开(公告)号：US4988818A

    公开(公告)日：1991-01-29

    申请号：US418225

    申请日：1989-10-06

    申请人： Manfred Lauer ,  Matthias Zipplies ,  Hubert Sauter ,  Barbara A. Moore ,  Dale R. Carlson ,  Paul S. Zorner ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Manfred Lauer ,  Matthias Zipplies ,  Hubert Sauter ,  Barbara A. Moore ,  Dale R. Carlson ,  Paul S. Zorner ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： A01N43/653 ,  A01N43/88 ,  C07D249/08 ,  C07D521/00

    CPC分类号： C07D231/12 ,  A01N43/653 ,  A01N43/88 ,  C07D233/56 ,  C07D249/08

    摘要： Triazole compounds I ##STR1## where A is C.sub.7 -C.sub.20 -alkyl or unsubstituted or substituted phenyl, naphthyl or pyridyl, and R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.6 -alkyl, C.sub.3 -C.sub.6 -alkenyl or C.sub.3 -C.sub.6 -alkynyl or is --COR.sup.x or --SO.sub.2 R.sup.x, where R.sup.x is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.8 -alkyl or phenyl, and their environmentally compatible salts, and herbicides containing one or more triazole compounds I, IA or IB ##STR2## where R.sup.1 is hydrogen, cyclopropyl or unsubstituted or substituted C.sub.1 -C.sub.6 -alkyl, C.sub.2 -C.sub.6 -alkenyl or C.sub.2 -C.sub.6 -alkynyl or is C.sub.1 -C.sub.4 -alkoxy, C.sub.2 -C.sub.4 -alkenyloxy or C.sub.2 -C.sub.4 -alkynyloxy, and R.sup.2 and R.sup.3 are each hydrogen, adamantyl or C.sub.1 -C.sub.3 -alkyl or, together with the carbon atom to which they are bonded, form unsubstituted or substituted C.sub.3 -C.sub.7 -cycloalkyl, C.sub.6 -C.sub.10 -bicycloalkyl, C.sub.6 -C.sub.10 -bicycloalkenyl, or their environmentally compatible salts and a benzothiadiazone.

    摘要翻译： 三唑化合物其中A为C 7 -C 20烷基或未取代或取代的苯基，萘基或吡啶基，R为氢或未取代或取代的C 1 -C 6 - 烷基，C 3 -C 6 - 烯基或C 3 -C 6 - 炔基 或者是-COR x或-SO 2 R x，其中R x是氢或未取代或取代的C 1 -C 8 - 烷基或苯基，以及它们的环境相容的盐和含有一种或多种三唑化合物I，IA或IB的除草剂。 其中R1是氢，环丙基或未取代的或取代的C1-C6-烷基，C2-C6-烯基或C2-C6-炔基或是C1-C4-烷氧基，C2-C4-烯氧基或C2-C4-炔氧基，R2 C 3 -C 7 - 环烷基，C 6 -C 10 - 双环烯基或它们的连接基团的碳原子一起形成未取代或取代的C 3 -C 7 - 环烷基，C 6 -C 10 - 双环烷基，C 6 -C 10 - 环境相容的盐和苯并噻二唑。