公开(公告)号：US20110299072A1

公开(公告)日：2011-12-08

申请号：US12674354

申请日：2008-08-19

申请人： Yasuyuki Yamada ,  Munehiro Hoshino

发明人： Yasuyuki Yamada ,  Munehiro Hoshino

IPC分类号： G01J3/42 ,  G01N25/00

CPC分类号： G01N33/2835 ,  G01N1/4044 ,  G01N1/405 ,  G01N21/6404 ,  G01N2021/3107

摘要： To provide a mercury measuring apparatus of a closed system capable of performing automatically a process ranging from collection to injection of the sample composed mainly of hydrocarbon, which is effective to accomplish a highly reliable measurement. The mercury measuring apparatus 100 includes a column 1 filled with a first adsorbent 11 and a reducing agent 13, an injecting unit 3 for injecting a sample into the column 1, a first heating unit 12, a second heating unit, a mercury collecting tube 18 filled with a second adsorbent 17, a third heating unit 19, a mercury measuring unit 2, gas flow passages FP1, FP2 and FP4, flow switching valves V1 to V3, V5 and V6 for selecting one of the gas flow passages FP1, FP2 and FP4, and a control unit 4.

摘要翻译： 提供一种封闭式系统的水银测量装置，其能够自动执行从主要由烃组成的样品的收集到注入的过程，其有效地实现高度可靠的测量。 汞测量装置100包括填充有第一吸附剂11和还原剂13的柱1，用于将样品注入柱1的注入单元3，第一加热单元12，第二加热单元，汞收集管18 填充有第二吸附剂17，第三加热单元19，汞测量单元2，气体流路FP1，FP2和FP4，用于选择气体流路FP1，FP2中的一个的流量切换阀V1〜V3，V5，V6， FP4和控制单元4。

公开(公告)号：US20110294222A1

公开(公告)日：2011-12-01

申请号：US13139364

申请日：2009-12-08

申请人： Jacques Delaire ,  Isabelle Leray ,  Jean-Pierre Lefevre ,  Liyun Zhao ,  Ting Wu

发明人： Jacques Delaire ,  Isabelle Leray ,  Jean-Pierre Lefevre ,  Liyun Zhao ,  Ting Wu

IPC分类号： G01N21/64

CPC分类号： G01N21/643 ,  B01F5/061 ,  B01F13/0059 ,  B01F2005/0621 ,  B01F2005/0636 ,  B01L2200/027 ,  B01L2200/10 ,  B01L2300/0654 ,  B01L2300/0816 ,  B01L2300/0867 ,  B01L2400/086 ,  G01N1/4044 ,  G01N1/405 ,  G01N21/645 ,  G01N31/22 ,  G01N33/1813 ,  G01N2021/7786

摘要： Process for metering lead in a sample of original water, in which is placed a sample of the water of which at least a substantial portion of the colloidal and organic material is passed in solution (sample of pretreated water), having: a first stage, starting from a sample of pretreated water with an adjusted pH, the lead is concentrated and the other parasitic ions are at least partially eliminated to obtain a sample of water that is concentrated with lead and substantially lacking in other parasitic ions (sample of lead-concentrated water); and a second stage in which, starting from the sample of lead-concentrated water, the sample of lead-concentrated water is mixed with a selective, lead-sensitive fluorescent probe whose fluorescence intensity/lead metering function is known; then, the thus produced water/fluorescent probe mixture is excited by the light, and the fluorescence intensity of the thus excited water/fluorescent probe mixture is collected optically; finally, starting from the thus detected fluorescence intensity, the lead metering of the sample to be metered is determined based on the fluorescence intensity/lead metering function.

摘要翻译： 在原水的样品中计量铅的方法，其中放置有至少大部分胶态和有机材料的水通过溶液（预处理水样品）的水样品，其具有：第一阶段， 从调整pH值的预处理水样品开始，铅被浓缩，其他寄生离子至少部分地被去除，以获得用铅浓缩并基本上不含其他寄生离子的水样品（铅浓缩样品 水）; 第二阶段，从铅浓缩水样品开始，铅浓缩水样品与已知荧光强度/铅计量功能的选择性铅敏感荧光探针混合; 然后，将由此产生的水/荧光探针混合物用光激发，并且由此激发的水/荧光探针混合物的荧光强度被光学收集; 最后，从这样检测到的荧光强度开始，基于荧光强度/铅计量功能确定要计量的样品的铅计量。

公开(公告)号：US07888265B2

公开(公告)日：2011-02-15

申请号：US11708770

申请日：2007-02-20

申请人： Katsuya Hirano ,  Mohammad B. Shabani

发明人： Katsuya Hirano ,  Mohammad B. Shabani

IPC分类号： H01L21/302 ,  H01L21/461

CPC分类号： G01N1/32 ,  G01N1/4044 ,  H01L21/3221

摘要： This method for assaying copper in silicon wafers includes the steps of: forming a polysilicon layer on the surface of a p-type silicon wafer having the same characteristics as the silicon wafers being assayed; heat treating the p-type silicon wafer after it has been polished; dissolving the polysilicon layer on the heat-treated p-type silicon wafer with a mixed acid composed of at least hydrofluoric acid and nitric acid; and quantitatively determining the copper components within the mixed acid following dissolution of the polysilicon layer.

摘要翻译： 这种用于测定硅晶片中的铜的方法包括以下步骤：在具有与被测定的硅晶片相同的特性的p型硅晶片的表面上形成多晶硅层; 在抛光p型硅晶片之后对其进行热处理; 用由至少氢氟酸和硝酸组成的混合酸将多晶硅层溶解在经热处理的p型硅晶片上; 并定量测定多晶硅层溶解后混合酸中的铜成分。

公开(公告)号：US20110033943A1

公开(公告)日：2011-02-10

申请号：US12988771

申请日：2009-04-20

申请人： Daniel Dessort ,  Robert Le Van Loï ,  Nadine Loubere

发明人： Daniel Dessort ,  Robert Le Van Loï ,  Nadine Loubere

IPC分类号： G01N33/00 ,  G01N33/52

CPC分类号： G01N33/225 ,  C01B17/20 ,  C01G11/00 ,  C01G11/02 ,  G01N1/00 ,  G01N1/22 ,  G01N1/4044 ,  G01N21/643 ,  G01N21/78 ,  G01N21/783 ,  G01N31/22 ,  G01N31/224 ,  G01N33/0044

摘要： The invention relates to a method for sampling a sulphur-containing solid product including supplying a gas flow comprising hydrogen sulphide, bringing the gas flow into contact with a solid reagent and reacting the solid reagent with the hydrogen sulphide contained in the gas flow, the reaction fixing the sulphur of the hydrogen sulphide by forming a sulphur-containing solid product which is different in colour from the solid reagent, and recovering the sulphur-containing solid product. The invention also relates to a device suitable for the implementation of this method.

摘要翻译： 本发明涉及一种用于对含硫固体产物进行取样的方法，包括供应包含硫化氢的气流，使气流与固体试剂接触并使固体试剂与气流中所含的硫化氢反应，反应 通过形成与固体试剂不同颜色的含硫固体产物并回收含硫固体产物来固定硫化氢的硫。 本发明还涉及适用于实施该方法的装置。

公开(公告)号：US20110011155A1

公开(公告)日：2011-01-20

申请号：US12889534

申请日：2010-09-24

申请人： Satoshi HIKIMA ,  Satoshi Fujita

发明人： Satoshi HIKIMA ,  Satoshi Fujita

IPC分类号： G01N30/02 ,  B01D59/44 ,  G01N30/00

CPC分类号： G01N33/36 ,  G01N1/4044

摘要： To provide a process, whereby a low molecular weight organic compound having at most 20 carbon atoms present in a trace amount in a cloth made of chemical fibers treated with a water and oil repellent agent, can be accurately analyzed.A process for analyzing a low molecular weight organic compound having at most 20 carbon atoms in a cloth made of chemical fibers treated with a water and oil repellent agent, which comprises (a) a step of dissolving the cloth made of chemical fibers treated with a water and oil repellent agent in a solvent capable of dissolving a resin constituting the cloth, to obtain a solution, (b) a step of mixing the solution with a solvent capable of agglomerating the resin to agglomerate the resin, to obtain a liquid containing a resin agglomerate, (c) a step of subjecting the liquid containing a resin agglomerate to solid-liquid separation to obtain a liquid phase, and (d) a step of measuring the concentration of a low molecular weight compound having at most 20 carbon atoms in the liquid phase by means of a liquid chromatograph-mass spectrometer, a liquid chromatograph-tandem mass spectrometer, a gas chromatograph-mass spectrometer or a gas chromatograph-tandem mass spectrometer.

摘要翻译： 为了提供一种方法，由此可以精确地分析在由防水拒油剂处理的化学纤维制成的布中存在痕量的至多20个碳原子的低分子量有机化合物。 一种用于分析在由防水拒油剂处理的化学纤维制成的布中具有至多20个碳原子的低分子量有机化合物的方法，其包括（a）将由化学纤维制成的布 在能够溶解构成布的树脂的溶剂中的防水防油剂，以获得溶液，（b）将溶液与能够凝聚树脂的溶剂混合以使树脂聚结的步骤，得到含有 树脂凝聚体，（c）对含有树脂凝聚体的液体进行固液分离以获得液相的步骤，（d）测定在液相中含有最多20个碳原子的低分子化合物的浓度的步骤 通过液相色谱 - 质谱仪，液相色谱 - 串联质谱仪，气相色谱 - 质谱仪或气相色谱 - 串联质谱仪进行液相。

公开(公告)号：US20090277875A1

公开(公告)日：2009-11-12

申请号：US12086515

申请日：2006-12-12

申请人： Karl-Heinz Wiedemann ,  Juergen Weber

发明人： Karl-Heinz Wiedemann ,  Juergen Weber

IPC分类号： B44C1/22

CPC分类号： G01N1/32 ,  G01N1/4044

摘要： A method known in prior art for determining the occupation of the surface of a silica glass component with impurities comprises taking a sample, a process in which at least some of the surface of the silica glass component is brought in contact with an acidic desorption solution, and surface impurities that are to be analyzed are accumulated therein and are subjected to an element-specific analysis. The aim of the invention is to create a method which is based on said method, allows the occupation of the surface of silica glass components to be determined accurately and reproducibly, and is suited for determining small amounts of impurities within the order of magnitude of 1010 atoms/cm2 also directly in situ. Said aim is achieved by the fact that taking the sample encompasses contacting the component surface with an acidic desorption solution containing water, nitric acid, and hydrofluoric acid, the nitric acid concentration in the desorption solution amounting to 1.5 to 5 times the hydrofluoric acid concentration (in percent by volume), provided that the contact time and the contact temperature are adjusted such that a maximum of 0.5 ?m of the component surface are removed.

摘要翻译： 现有技术中已知的用于确定具有杂质的二氧化硅玻璃组分的表面占有率的方法包括：取样品，其中至少部分二氧化硅玻璃组分的表面与酸性解吸溶液接触的方法， 并且将要分析的表面杂质积聚在其中并进行元素特异性分析。 本发明的目的是创建一种基于所述方法的方法，允许准确可重复地确定二氧化硅玻璃组分的表面的占用，并且适合于确定在数量级范围内的少量杂质 原子/ cm2也直接原位。 所述目的通过以下事实实现：取样包括使组分表面与含有水，硝酸和氢氟酸的酸性解吸溶液接触，解吸溶液中的硝酸浓度为氢氟酸浓度的1.5至5倍（ 以体积计），只要调整接触时间和接触温度，从而去除组分表面的最大值为0.5μm。

公开(公告)号：US20090168059A1

公开(公告)日：2009-07-02

申请号：US12322158

申请日：2009-01-29

申请人： Stuart Farquharson ,  Paul Maksymiuk ,  Chetan S. Shende

发明人： Stuart Farquharson ,  Paul Maksymiuk ,  Chetan S. Shende

IPC分类号： G01J3/44 ,  G01N30/00

CPC分类号： G01N30/74 ,  B01L3/0275 ,  G01N1/40 ,  G01N1/4044 ,  G01N21/658 ,  G01N30/6082 ,  G01N30/78 ,  G01N2030/746 ,  G01N21/63

摘要： A stationary medium is employed both to separate chemicals from a sample solution and also to generate surface-enhanced Raman scattering, so that spectral analysis of the separated analyte chemical can be performed. Applied driving force causes the sample to flow into the stationary medium and to distribute therethrough, thereby causing rapid separation of the analyte chemical, and surface-enhanced Raman scattered radiation is quickly detected, at a plurality of locations along a flow path defined by the stationary medium, for ultimate analysis.

摘要翻译： 既采用固定介质将样品溶液中的化学物质分开，也可产生表面增强的拉曼散射，从而可以进行分离的分析物化学品的光谱分析。 施加的驱动力使得样品流入固定介质并分布在其中，从而导致分析物化学物质的快速分离，并且在沿着由静止物定义的流动路径的多个位置处快速检测到表面增强的拉曼散射辐射 中等，用于最终分析。

公开(公告)号：US20080176320A1

公开(公告)日：2008-07-24

申请号：US12015414

申请日：2008-01-16

申请人： Yingjie Liu

发明人： Yingjie Liu

IPC分类号： C12N5/06

CPC分类号： C12Q1/6806 ,  G01N1/4044 ,  C12Q2527/125

摘要： The teaching provides a method for selectively lysing sperm cells in a mixed cell sample, particularly in the field of forensic sciences. Reagents and kits for carrying out the methods are also provided.

摘要翻译： 该教学提供了选择性裂解混合细胞样品中精子细胞的方法，特别是在法医科学领域。 还提供了用于执行方法的试剂和试剂盒。

公开(公告)号：US20070275479A1

公开(公告)日：2007-11-29

申请号：US11438880

申请日：2006-05-23

申请人： Dileep Chintaman Joshi

发明人： Dileep Chintaman Joshi

IPC分类号： G01N1/18

CPC分类号： G01N1/34 ,  G01N1/4044 ,  Y10T436/255

摘要： The accelerated testing of articles for the leachability of metals into a fluid stream is accomplished by contacting the article with an extraction solution, ultrasonically agitating the solution with optional heating, and analyzing the solution for the presence of extracted metals. A particular extraction solution for assessing the extractability of metals into drinking water includes bicarbonate and a free halogen.

摘要翻译： 通过将制品与提取溶液接触，可以通过任选加热超声波搅拌溶液，并分析溶液中萃取的金属的存在，来实现金属进入流体物流的物品的可加速测试。 用于评估金属到饮用水中的提取性的特定提取溶液包括碳酸氢盐和游离卤素。

公开(公告)号：US20070202607A1

公开(公告)日：2007-08-30

申请号：US11361653

申请日：2006-02-24

申请人： Robert Revesz

发明人： Robert Revesz

IPC分类号： G01N1/00

CPC分类号： G01N1/40 ,  B01L3/50255 ,  B01L2300/0803 ,  B01L2300/1866 ,  B01L2400/0478 ,  G01N1/4044 ,  G01N1/44 ,  G01N22/00 ,  Y10T436/25

摘要： A method and apparatus are disclosed that are useful in bench top sample preparation and filtration techniques, including those related to microwave assisted extraction and partial digestion. In one aspect the method includes the steps of positioning a microwave-transparent matrix removal tool in a microwave transparent reaction vessel adding a matrix-based composition to the microwave reaction vessel containing the removal tool, applying microwave radiation to the reaction vessel, the matrix-based composition, and the matrix removal tool, and removing the matrix based composition from the reaction vessel using the matrix removal tool. In another aspect the method includes the steps of positioning a matrix based composition that includes at least some liquid in a filter vessel, and applying a moderate over-pressure to the composition upstream of the filter to accelerate the movement of liquid through the filter.

摘要翻译： 公开了一种在台式样品制备和过滤技术中有用的方法和装置，包括与微波辅助提取和部分消化有关的方法和装置。 在一个方面，该方法包括以下步骤：将微波透明基质去除工具放置在微波透明反应容器中，将含有基质的组合物加入含有去除工具的微波反应容器中，向反应容器施加微波辐射， 基体去除工具，以及使用基质去除工具从反应容器中除去基于基质的组合物。 在另一方面，该方法包括以下步骤：将基于基质的组合物定位在过滤器容器中，其包括至少一些液体，以及在过滤器上游对组合物施加适度的过压，以加速液体通过过滤器的运动。