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41.发明申请公开(公告)号：US20190169102A1
公开(公告)日：2019-06-06
申请号：US16324806
申请日：2017-08-28
Applicant: Arkema France
Inventor： Dominique GARRAIT , Anne PIGAMO , Laurent WENDLINGER
IPC: C07C17/358 , B01J27/32 , B01J27/12 , B01J27/128 , B01J27/132 , B01J27/138 , B01J35/10 , B01J37/26 , B01J38/12 , C07C17/25 , C07C17/20
Abstract: The present invention relates to a process for modifying the fluorine distribution in a hydrocarbon compound in the presence of a catalyst, characterized by the use, as catalyst, of a solid composition comprising at least one component containing chromium oxyfluoride or fluoride of empirical formula CrxM(1-x)OrFs, where 2r+s is greater than or equal to 2.9 and less than 6, M is a metal chosen from columns 2 to 12 of the Periodic Table of the Elements, x has a value from 0.9 to 1, s is greater than 0 and less than or equal to 6 and r is greater than or equal to 0 and less than 3, the said solid composition having a crystallinity of less than 20% by weight. The present invention also relates to the solid composition per se.
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公开(公告)号：US20170210962A1
公开(公告)日：2017-07-27
申请号：US15481815
申请日：2017-04-07
Applicant: ARKEMA FRANCE
Inventor： Bertrand COLLIER , Dominique DEUR-BERT , Laurent WENDLINGER
CPC classification number: C09K5/08 , C07C21/18 , C09K3/00 , C09K5/044 , C09K5/045 , C09K2205/122 , C09K2205/126 , C09K2205/22 , C09K2205/32 , H01B3/56
Abstract: A composition including the compound HFO-1234yf and at least one other, additional, compound selected from HCFC-240db, HCFO-1233xf, HCFC-243db, HCFO-1233zd, HCC-40, HCFC-114a, HCFC-115, HCFC-122, HCFC-23, HCFC-124, HCFC-124a, HFC-125, HCFC-133a, HCFC-142, HCFC-143, HFC-52a, HCFC-243ab, HCFC-244eb, HFC-281ea, HCO-1110, HCFO-1111, HCFO-1113, HCFO-1223xd, and HCFO-1224xe. A composition including the compound HFO-1234yf and at least two compounds selected from HFO-1234ze, HFC-245cb, HFC-134a, HCFC-115, HFC-152a, HCC-40 and HFO-1243zf.
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公开(公告)号：US20170210960A1
公开(公告)日：2017-07-27
申请号：US15481873
申请日：2017-04-07
Applicant: ARKEMA FRANCE
Inventor： Dominique DEUR-BERT , Laurent WENDLINGER
CPC classification number: C09K5/044 , B01F17/0035 , B01F17/0085 , C09K3/00 , C09K3/30 , C09K5/04 , C09K5/045 , C09K2205/122 , C09K2205/126 , C09K2205/32 , H01B3/56
Abstract: Quasi-azeotropic or azeotropic compositions containing chloromethane and at least one or more compound(s) selected from 2,3,3,3-tetrafluoropropene, 3,3,3-trifluoropropene, 1,1,1,2-tetrafluoroethane, 1,1,1,2,2-pentafluoropropane, E/Z-1,1,3,3,3-pentafluoropropene, E/Z-1,2,3,3,3-pentafluoropropene, 1,1-difluoroethane and E-1,3,3,3-tetrafluoropropene. The composition may include either from 0.5 to 70 mol % of chloromethane and at least from 99.5 to 30 mol % of a compound selected from 2,3,3,3-tetrafluoropropene, 1,1-difluoroethane, 3,3,3-trifluoropropene and 1,1,1,2-tetrafluoroethane, or from 55 to 95 mol % of chloromethane and at least from 45 to 5 mol % of one or more compound(s) selected from 1,1,1,2,2-pentafluoropropane, E/Z-1,1,3,3,3-pentafluoropropene, E/Z-1,2,3,3,3-pentafluoropropene and E-1,3,3,3-tetrafluoropropene.
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公开(公告)号：US20160237009A1
公开(公告)日：2016-08-18
申请号：US15139662
申请日：2016-04-27
Applicant: Arkema France
Inventor： Dominique DEUR-BERT , Bertrand COLLIER , Laurent WENDLINGER
CPC classification number: C07C17/20 , C07C17/206 , C07C17/25 , C07C17/38 , C07C17/383 , F25J1/0022 , F25J3/04412 , C07C21/18
Abstract: The invention concerns a method for producing 2,3,3,3-tetrafluoropropene comprising: a fluoridation reaction of a halopropane and/or halopropene into 2,3,3,3-tetrafluoropropene by means of hydrogen fluoride; the recovery of a gas stream resulting from the reaction; the cooling and partial condensation of the gas stream resulting from the reaction into a partially condensed stream; the separation of the partially condensed stream into a gas fraction and a liquid fraction; the compression of the gas fraction into a compressed gas fraction; the compression of the liquid fraction into a compressed liquid fraction; the distillation of the compressed gas fraction and compressed liquid fraction in order to provide a stream of 2,3,3,3-tetrafluoropropene, a stream of hydrochloric acid, and a stream of unreacted hydrogen fluoride. The invention also concerns an installation suitable for implementing said method.
Abstract translation: 本发明涉及一种生产2,3,3,3-四氟丙烯的方法，包括：通过氟化氢将卤代丙烷和/或卤代丙烯氟化反应成2,3,3,3-四氟丙烯; 回收由反应产生的气流; 将由反应产生的气流冷却和部分冷凝成部分冷凝的流; 将部分冷凝的流分离成气体馏分和液体馏分; 将气体馏分压缩成压缩气体馏分; 将液体馏分压缩成压缩液体馏分; 蒸馏压缩气体馏分和压缩液体馏分以提供2,3,3,3-四氟丙烯的流，盐酸流和未反应的氟化氢气流。 本发明还涉及适于实现所述方法的安装。
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公开(公告)号：US20160176789A1
公开(公告)日：2016-06-23
申请号：US15055738
申请日：2016-02-29
Applicant: Arkema France
Inventor： Anne PIGAMO , Laurent WENDLINGER , Nicolas DOUCET
CPC classification number: C07C17/206 , B01J23/866 , B01J23/90 , B01J23/92 , B01J23/94 , B01J27/125 , B01J37/14 , B01J37/26 , B01J38/12 , C07C17/20 , C07C17/25 , Y02P20/584 , C07C21/18
Abstract: The invention relates to a fluorination process, alternately comprising reaction stages and regeneration stages, wherein the reaction stages comprise reacting a chlorinated compound with hydrogen fluoride in gas phase in the presence of a fluorination catalyst to produce a fluorinated compound, and the regeneration stages comprise contacting the fluorination catalyst with an oxidizing agent-containing gas flow.
Abstract translation: 本发明涉及氟化方法，交替包括反应阶段和再生阶段，其中反应步骤包括在氟化催化剂存在下使气相中的氯化化合物与氟化氢反应以产生氟化化合物，并且再生阶段包括接触 含有含氧化剂气体的氟化催化剂。
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Patent Agency Ranking
46.发明申请公开(公告)号：US20160023974A1
公开(公告)日：2016-01-28
申请号：US14774161
申请日：2014-02-21
Applicant: ARKEMA FRANCE
Inventor： Philippe BONNET , Bertrand COLLIER , Dominique DEUR-BERT , Laurent WENDLINGER
Abstract: An azeotropic or quasi-azeotropic composition including hydrogen fluoride, E-3,3,3-trifluoro-1-chloropropene and optionally one or more (hydro)halogen-carbon compounds including between 1 and 3 carbon atoms. Also, a preferred azeotropic or quasi-azeotropic composition including hydrogen fluoride, E-3,3,3-trifluoro-1-chloropropene, and optionally one or more compounds selected from among 1,1,1,2,2-pentafluoropropane, 2,3,3,3-tetrafluoropropene, 3,3,3-trifluoropropene, 3,3,3-trifluoro-2-chloropropene, 1,3,3,3-tetrafluoropropene, trifluoropropyne, 1,1,1,3,3-pentafluoropropane, 1,1,1,3,3-pentafluoropropane, 1,1,1,3,3-pentafluoropropene, 1,1,1,2,3-pentafluoropropene and 2-chloro,1,1,1,2-tetrafluoropropane.
Abstract translation: 共沸或准共沸组合物包括氟化氢，E-3,3,3-三氟-1-氯丙烯和任选的一种或多种（氢）卤素 - 碳化合物，包括1至3个碳原子。 此外，优选的共沸或准共沸组合物包括氟化氢，E-3,3,3-三氟-1-氯丙烯和任选的一种或多种选自1,1,1,2,2-五氟丙烷，2 ，3,3,3-四氟丙烯，3,3,3-三氟丙烯，3,3,3-三氟-2-氯丙烯，1,3,3,3-四氟丙烯，三氟丙炔，1,1,1,3,3 四氟丙烷，1,1,1,3,3-五氟丙烷，1,1,1,3,3-五氟丙烯，1,1,1,2,3-五氟丙烯和2-氯，1,1,1,2 - 四氟丙烷。
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公开(公告)号：US20160009555A1
公开(公告)日：2016-01-14
申请号：US14772950
申请日：2014-02-21
Applicant: ARKEMA FRANCE
Inventor： Philippe BONNET , Bertrandè COLLIER , Dominique DEUR-BERT , Laurent WENDLINGER
Abstract: An azeotropic or quasi-azeotropic composition including hydrogen fluoride, 2,3,3,3-tetrafluoropropene and one or more (hydro)halogen-carbon compounds including between 1 and 3 carbon atoms. Also a azeotropic or quasi-azeotropic composition including hydrogen fluoride, 2,3,3,3-tetrafluoropropene, and one or more organic compounds selected from among 1,1,1,2,2-pentafluoropropane, E-1,3,3,3-tetrafluoropropene, Z-1,3,3,3-tetrafluoropropene, 3,3,3-trifluoropropene, 3,3,3-trifluoro-2-chloropropene, E-3,3,3-trifluoro-1-chloropropene, trifluoropropyne, 1,1,1,3,3-pentafluoropropane, 1,1,1,3,3-pentafluoropropene, Z-1,1,1,2,3-pentafluoropropene and 2-chloro,1,1,1,2-tetrafluoropropane.
Abstract translation: 共沸或准共沸组合物，包括氟化氢，2,3,3,3-四氟丙烯和一种或多种（氢）卤素 - 碳化合物，包括1至3个碳原子。 还有一种共沸或准共沸组合物，包括氟化氢，2,3,3,3-四氟丙烯和一种或多种选自1,1,1,2,2-五氟丙烷，E-1,3,3 ，3-四氟丙烯，Z-1,3,3,3-四氟丙烯，3,3,3-三氟丙烯，3,3,3-三氟-2-氯丙烯，E-3,3,3-三氟-1-氯丙烯 ，三氟丙炔，1,1,1,3,3-五氟丙烷，1,1,1,3,3-五氟丙烯，Z-1,1,1,2,3-五氟丙烯和2-氯，1,1,1 ，2-四氟丙烷。
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公开(公告)号：US20240001356A1
公开(公告)日：2024-01-04
申请号：US18036438
申请日：2021-11-24
Applicant: ARKEMA FRANCE
Inventor： Laurent WENDLINGER , Dominique DEUR-BERT
CPC classification number: B01J38/04 , B01J23/866 , C07C17/206
Abstract: The present invention relates to a process for treating, in a reactor containing a catalytic bed, a solid catalyst, said process comprising the steps of: a) implementing, in said reactor, a gas-phase catalytic reaction at a catalytic bed temperature T1 in the presence of a hydrogen halide or giving rise to the formation of a hydrogen halide, b) causing an inert gas to flow through the catalytic bed at a catalytic bed temperature T2 that is lower than T1, the temperature T2 being greater than 30° C.
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公开(公告)号：US20230114828A1
公开(公告)日：2023-04-13
申请号：US17904382
申请日：2021-02-17
Applicant: ARKEMA FRANCE
Inventor： Laurent WENDLINGER
Abstract: A composition comprises at least 99.5% by weight of an iodofluorocarbon compound A and at most 0.5% by weight of a compound B selected from water, HF, HI, IF5, I2, O2, CO2, CO and nitrogen. The iodofluorocarbon compound A is of formula (I) (R1)(R2)C(I)(R3) or of formula (II) (R1)(R2)C═C(I)(R3); in which R1, R2 and R3 independently of one another are selected from the group consisting of H, F, I, a C1-C10 alkyl radical, a C3-C10 cycloalkyl radical, a C2-C10 alkenyl radical, a C3-C10 cycloalkenyl radical, and a C6-C10 aryl radical. All radicals are optionally substituted by a fluorine or iodine atom. At least one of the substituents R1, R2 or R3, is F or is a radical as defined above comprising at least one fluorine atom. The iodofluorocarbon compound A is not CF3I.
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公开(公告)号：US20230075839A1
公开(公告)日：2023-03-09
申请号：US17904379
申请日：2021-02-17
Applicant: ARKEMA FRANCE
Inventor： Laurent WENDLINGER
IPC: C07C17/087
Abstract: The present invention relates to a process for producing an iodofluoroalkane compound, comprising the steps of: a) placing a fluoroolefin in contact with hydrogen iodide to form a stream A comprising said iodofluoroalkane compound and unreacted hydrogen iodide, b) separating said stream A into a first stream Bi comprising said iodofluoroalkane compound and a stream B2 comprising unreacted hydrogen iodide, c) recycling stream B2 into step a)
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