Bulk synthesis of metal and metal based dielectric nanowires
    44.
    发明授权
    Bulk synthesis of metal and metal based dielectric nanowires 失效
    金属和金属基介电纳米线的大量合成

    公开(公告)号:US07771689B2

    公开(公告)日:2010-08-10

    申请号:US10705687

    申请日:2003-11-10

    IPC分类号: C01B21/06

    摘要: A process of synthesizing metal and metal nitride nanowires, the steps comprising of: forming a catalytic metal (such as gallium, and indium) on a substrate (such as fused silica quartz, pyrolytic boron nitride, alumina, and sapphire), heating the combination in a pressure chamber, adding gaseous reactant and/or solid metal source, applying sufficient microwave energy (or current in hot filament reactor) to activate the metal of interest (such as gold, copper, tungsten, and bismuth) and continuing the process until nanowires of the desired length are formed. The substrate may be fused silica quartz, the catalytic metal a gallium or indium metal, the gaseous reactant is nitrogen and/or hydrogen and the nanowires are tungsten nitride and/or tungsten.

    摘要翻译: 合成金属和金属氮化物纳米线的方法,其步骤包括:在基底(如熔融石英石英,热解氮化硼,氧化铝和蓝宝石)上形成催化金属(如镓和铟),加热组合 在压力室中加入气体反应物和/或固体金属源,施加足够的微波能量(或热丝反应器中的电流)以激活感兴趣的金属(例如金,铜,钨和铋)并继续该过程直到 形成所需长度的纳米线。 衬底可以是熔融石英石英,催化金属是镓或铟金属,气体反应物是氮和/或氢,并且纳米线是氮化钨和/或钨。

    Synthesis of fibers of inorganic materials using low-melting metals
    45.
    发明授权
    Synthesis of fibers of inorganic materials using low-melting metals 有权
    使用低熔点金属合成无机材料的纤维

    公开(公告)号:US07713352B2

    公开(公告)日:2010-05-11

    申请号:US11521084

    申请日:2006-09-14

    IPC分类号: C30B17/00 C30B23/00

    摘要: A process is provided to produce bulk quantities of nanowires in a variety of semiconductor materials. Thin films and droplets of low-melting metals such as gallium, indium, bismuth, and aluminum are used to dissolve and to produce nanowires. The dissolution of solutes can be achieved by using a solid source of solute and low-melting metal, or using a vapor phase source of solute and low-melting metal. The resulting nanowires range in size from 1 nanometer up to 1 micron in diameter and lengths ranging from 1 nanometer to several hundred nanometers or microns. This process does not require the use of metals such as gold and iron in the form of clusters whose size determines the resulting nanowire size. In addition, the process allows for a lower growth temperature, better control over size and size distribution, and better control over the composition and purity of the nanowire produced therefrom.

    摘要翻译: 提供了一种在各种半导体材料中产生大量纳米线的方法。 使用低熔点金属如镓,铟,铋和铝的薄膜和液滴来溶解和产生纳米线。 溶质的溶解可以通过使用溶质和低熔点金属的固体源,或使用溶质和低熔点金属的气相源来实现。 所得的纳米线的尺寸范围从1纳米直到1微米的直径和长度范围从1纳米到几百纳米或微米。 该方法不需要以尺寸决定所得纳米线尺寸的簇的形式使用诸如金和铁的金属。 此外,该方法允许较低的生长温度,更好地控制尺寸和尺寸分布,以及更好地控制由其制备的纳米线的组成和纯度。

    PROCESS FOR PRETREATING ORGANIC EXTRACTANTS AND ITS PRODUCT AND APPLICATION
    46.
    发明申请
    PROCESS FOR PRETREATING ORGANIC EXTRACTANTS AND ITS PRODUCT AND APPLICATION 审中-公开
    预处理有机提取物及其产品和应用的方法

    公开(公告)号:US20100003176A1

    公开(公告)日:2010-01-07

    申请号:US12526436

    申请日:2008-02-02

    IPC分类号: C01F17/00

    摘要: A process for pretreating organic extractants and its product and application in SX separation of rare earth. The pretreating method is that extractant and rare earth solution are mixed with powder or slurry of alkaline earth metal compound containing magnesium and/or calcium to realize pre-extraction, or the organic extractant are mixed with rare earth carbonate slurry to realize pre-extraction. When rare earth ion in aqueous phase is extracted into organic phase, the exchanged hydrogen ions enter into aqueous phase and dissolve the alkaline earth metal compound or the rare earth carbonate which helps to keep the acidity equilibrium of the system. The obtained organic extractant loaded with rare earth is used for unsaponificated SX separation of rare earth.With this method, there is no need to saponificate organic extractant with liquid ammonia or alkali, and there is no ammonia-nitrogen wastewater produced. So separation cost decrease at a large scale and a lot of the cost to treat the three wastes is cut. This method is applicable to SX separation for all rare earth elements in chloride, sulphate and nitrate system and has advantages of low investment and high profit.

    摘要翻译: 一种用于预处理有机萃取剂及其产品和在稀土SX分离中的应用的方法。 预处理方法是将萃取剂和稀土溶液与含有镁和/或钙的碱土金属化合物的粉末或浆料混合以实现预萃取,或者将有机萃取剂与稀土碳酸盐浆料混合以实现预萃取。 当水相中的稀土离子萃取到有机相中时,交换的氢离子进入水相并溶解碱土金属化合物或稀土碳酸盐,有助于保持体系的酸度平衡。 将所得到的装有稀土的有机萃取剂用于稀土的未分配的SX分离。 通过这种方法,不需要用液体氨或碱对有机萃取剂进行皂化,不产生氨氮废水。 因此,分离成本大幅度地下降,处理三种废物的成本大幅度下降。 该方法适用于氯化物,硫酸盐和硝酸盐体系中所有稀土元素的SX分离,具有投资低,利润高的优点。

    ALUMINATE PHOSPHOR CONTAINING BIVALENCE METAL ELEMENTS, ITS PREPARATION AND THE LIGHT EMITTING DEVICES INCORPORATING THE SAME
    47.
    发明申请
    ALUMINATE PHOSPHOR CONTAINING BIVALENCE METAL ELEMENTS, ITS PREPARATION AND THE LIGHT EMITTING DEVICES INCORPORATING THE SAME 有权
    含有金属元素的铝酸钠,其制备方法和同时发光的发光装置

    公开(公告)号:US20090218585A1

    公开(公告)日:2009-09-03

    申请号:US12465381

    申请日:2009-05-13

    IPC分类号: H01L33/00 C09K11/85

    CPC分类号: C09K11/7774 C09K11/778

    摘要: A phosphor can be excited by UV, purple or blue light LED, its production and the light emitting devices. The general formula of the phosphor is LnaMb(O,F)12:(R3+, M′2+)x, wherein, Ln is at least one metal element selected from a group consisting of Sc, Y, La, Pr, Nd, Gd, Ho, Yb and Sm, 2.6≦a≦3.4; M is at least one element selected from a group consisting of B, Al and Ga, 4.5≦b≦5.5; R is at least one metal element selected from a group consisting of Ce and Tb; M′ is at least one metal element selected from a group consisting of Ca, Sr, Ba, Mn and Zn, 0.001≦x≦0.4. The phosphor possesses broad emitting range, high efficiency, better uniformity and stability. A light emitting device can be obtained by incorporating this phosphor into a UV, purple or blue light emitting device.

    摘要翻译: 紫外线,紫光或蓝光LED,其生产和发光器件可以激发荧光体。 荧光体的通式为LnaMb(O,F)12:(R3 +,M'2 +)x,其中,Ln为选自Sc,Y,La,Pr,Nd, Gd,Ho,Yb和Sm,2.6 <= a <= 3.4; M是选自B,Al和Ga中的至少一种元素,4.5≤b≤5.5; R是选自Ce和Tb中的至少一种金属元素; M'是选自Ca,Sr,Ba,Mn和Zn中的至少一种金属元素,0.001≤x≤0.4。 荧光粉具有广泛的发光范围,高效率,更好的均匀性和稳定性。 通过将该荧光体掺入UV,紫色或蓝色发光器件中,可以获得发光器件。

    Secured wireless communications
    49.
    发明授权

    公开(公告)号:US09641326B2

    公开(公告)日:2017-05-02

    申请号:US14402677

    申请日:2012-05-31

    摘要: The disclosure relates to secured wireless communications. A sender device emits randomly photons in a first polarization, a second polarization and a third polarization without aligning a polarization system in a plane perpendicular to the first and second polarizations with a recipient device. The recipient device is adapted for detection of events in association with six polarizations. The recipient device selects randomly polarization basis for measurement of the received photons. Information of detected events in association with three basis is communicated to the sender device. The information from the recipient device and information stored in the sender device is processed to determine events where same polarization basis was used by the sender device and the recipient device.

    SECURED WIRELESS COMMUNICATIONS
    50.
    发明申请
    SECURED WIRELESS COMMUNICATIONS 有权
    安全无线通信

    公开(公告)号:US20150172048A1

    公开(公告)日:2015-06-18

    申请号:US14402677

    申请日:2012-05-31

    IPC分类号: H04L9/08 H04L9/14

    摘要: The disclosure relates to secured wireless communications. A sender device emits randomly photons in a first polarisation, a second polarisation and a third polarisation without aligning a polarisation system in a plane perpendicular to the first and second polarisations with a recipient device. The recipient device is adapted for detection of events in association with six polarisations. The recipient device selects randomly polarisation basis for measurement of the received photons. Information of detected events in association with three basis is communicated to the sender device. The information from the recipient device and information stored in the sender device is processed to determine events where same polarisation basis was used by the sender device and the recipient device.

    摘要翻译: 本公开涉及安全的无线通信。 发送装置发射第一极化,第二极化和第三极化的随机光子,而不使偏振系统在垂直于与接收装置的第一和第二极化作用的平面内。 受体装置适于检测与六个极化相关联的事件。 受体装置选择随机的极化基准来测量接收到的光子。 与三个基础相关联的检测到的事件的信息被传送给发送者设备。 来自收件人设备的信息和存储在发送者设备中的信息被处理以确定发送者设备和接收者设备使用相同极化基础的事件。