摘要:
The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic alkene which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B), (c) hydrogenation of the composition (B) in the presence of at least one catalyst to give a composition (C), (d) purification of the composition (C), comprising at least the steps (di) thermal treatment of the composition (C) with at least one acid or at least one catalyst comprising at least one transition metal, (dii) further purification by a method selected from the group consisting of distillation, extraction and crystallization.
摘要:
The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with at least one acid and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization, Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one acid for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with the acid.
摘要:
The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic olefin which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B).
摘要:
An electric circuit for providing a selection signal being used to select a control value of a control variable which oscillates, at steady state, about a reference value about a first control value and a second control value with a first period duration comprises a first differential circuit which provides a first current being dependent on a difference between the first control value and the reference value. The electric circuit further comprises a second differential circuit which provides a second current being dependent on a difference between the reference value and the second value and a first node at which a differential current between the first current and the second current is formed. The differential current forms the selection signal indicating if the first control value or the second value is to be selected in order to minimize a difference between the reference signal and control variable. A first current mirror circuit of the electric circuit is connected between the first differential circuit and the first node in order to pass the first current to the first node and a second current mirror circuit and a third current mirror circuit of the electric circuit are connected in series. The second and third current mirror circuits are connected between the second differential circuit and the first node in order to pass the second current to the first node.
摘要:
This invention relates to a semiconductor array having a first semiconducting layer and a second semiconducting layer made of a ferromagnetic material, which is coupled to the first semiconducting layer in such a way that a spin-polarized state of the semiconducting charge carriers is injected into the first semiconducting layer. The second semiconducting layer interacts with charge carriers made available outside of the second semiconducting layer in such a way that a high spin polarization is created in the second semiconducting layer at least 250 Kelvin.
摘要:
The method relates to a method for detecting disorders in the protein C system, and in particular for determining the activated blood coagulation factor V with increased stability with respect to decomposition by activated protein C.
摘要:
The invention relates to a unit (1) for determining the dominant light source type in electromagnetic radiation (2) incident on the unit (1) and generated from a plurality of light sources of different types. The unit comprises at least one first photodiode (10) designed to detect electromagnetic radiation in the visible spectral range and to generate a first output signal (11). The unit comprises at least one second photodiode (20) designed to detect electromagnetic radiation in the infrared spectral range and to generate a second output signal (21). The unit comprises at least one calculation unit (30) designed to derive a quotient result (23) and a frequency result (13) from the first (11) and second (21) output signals. The frequency result (13) provides information about the presence or absence of signal components in a predetermined frequency range contained in the electromagnetic radiation. The unit comprises at least one evaluation unit (40) designed to derive the dominant light source type from the quotient result (23) and the frequency result (13).
摘要:
The invention relates to a tube bundle reactor with a flat feed hood. Alternatively, the release hood may also have a flat design. The flat design reduces the heat of reaction which arises in the hood in the case of reaction types which take place not only in the tube bundle (uncatalyzed reactions and reactions with homogeneously distributed catalyst). This greatly suppresses undesired reactions which already take place in the hood owing to accumulated heat, which achieves a higher selectivity in the case of thermally sensitive reactions. In addition, the thermal distribution within the hoods can be controlled precisely.The tube bundle reactor comprises a tube bundle which has a feed end which is connected to a feed hood of the tube bundle reactor, wherein the feed hood is configured in a flat design with a cross-sectional area at the feed end and an internal volume, and the ratio of internal volume to cross-sectional area is less than 0.35 m. The invention is further implemented by means of a process for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a proportion of the reactant mixture within the tube bundle to a product. The introducing comprises: feeding the reactant mixture into an interior of a feed hood of the tube bundle reactor and passing the reactant mixture on into a feed end of the tube bundle in the form of a fluid stream. The fluid stream has a cross-sectional area on entry into the feed end, and the interior of the feed hood through which the fluid stream flows has an internal volume; where the ratio of internal volume to cross-sectional area is less than 0.35 m.
摘要:
The invention relates to a unit (1) for determining the dominant light source type in electromagnetic radiation (2) incident on the unit (1) and generated from a plurality of light sources of different types. The unit comprises at least one first photodiode (10) designed to detect electromagnetic radiation in the visible spectral range and to generate a first output signal (11). The unit comprises at least one second photodiode (20) designed to detect electromagnetic radiation in the infrared spectral range and to generate a second output signal (21). The unit comprises at least one calculation unit (30) designed to derive a quotient result (23) and a frequency result (13) from the first (11) and second (21) output signals. The frequency result (13) provides information about the presence or absence of signal components in a predetermined frequency range contained in the electromagnetic radiation. The unit comprises at least one evaluation unit (40) designed to derive the dominant light source type from the quotient result (23) and the frequency result (13).
摘要:
The invention regards a hearing aid comprising a receiver and a signal processing device, wherein the signal processing device is electrically coupled to a connection socket operable to detachably connect the receiver to the socket and whereby the signal processing device further comprise a detector operable to detect a characteristics of the receiver which is connected to the signal processing device through the connection socket. The present invention addresses the problem of identification of individual receiver properties as well as of identifying different types of receivers.