Abstract:
The present invention describes a device and a method for dense and homogeneous loading of catalyst into the annular space of bayonet tubes employed in a steam reforming reactor, said device being constituted by a series of removable deflectors.
Abstract:
A device and method for automatic unloading of particles from the vertical tubes of a chemical reactor automatically feeds a fish tape into the bottom of the vertical tube to contact and dislodge the particles and automatically retracts the fish tape to allow the particles to fall out of the tube.
Abstract:
“The invention relates to a loading device having N loading heads offset by N/360° , wherein N is the number 3 or an integer multiple thereof, wherein each of the N loading heads has a connecting device for a hose arranged at the upper end, through which hose the catalyst material can be delivered from above, wherein each of the N loading heads has a deflecting cone with the tip pointing upwards beneath the connecting device and joined to the connecting device, a vertical holder is mounted on the underside of said deflecting cone, at least two circular deflector funnel elements are mounted on the vertical holder by means of horizontal braces, the deflector funnel elements open more narrowly at the top than at the bottom, gaps are provided between the deflector funnel elements and the lower deflector funnel elements have a larger diameter than the deflector funnel elements above them.”
Abstract:
A method for installing a monitoring device with the simultaneous loading of a particulate catalyst into a vertical catalyst tube includes (i) introducing a monitoring device into the tube, (ii) introducing monitoring device alignment apparatus into the tube, (iii) introducing catalyst loading apparatus into the tube, (iv) loading catalyst particles into the top of the tube whereinafter they contact said catalyst loading apparatus as they pass down the tube, forming a uniform bed of catalyst beneath said catalyst loading apparatus and alignment apparatus and around said monitoring device, and (v) simultaneously removing the catalyst loading apparatus and alignment apparatus from the catalyst tube in timed relationship to the catalyst loading. The monitoring device alignment apparatus includes a ring member and two or more spacing members affixed to the ring member such that the ring member and the monitoring device are centrally positioned within the tube.
Abstract:
A device and method for automatic unloading of particles from the vertical tubes of a chemical reactor automatically feeds a fish tape into the bottom of the vertical tube to contact and dislodge the particles and automatically retracts the fish tape to allow the particles to fall out of the tube.
Abstract:
A riser reactor system comprising a riser reactor and a catalyst feed device for fluidized catalyst, the riser reactor having a riser interior in which catalyst is flowing during normal operation, and the feed device comprising an annular trough surrounding the riser interior, the annular trough having an up-stream opening for receiving fluidized catalyst, and at least one substantially circumferential downstream opening providing fluid communication between the trough and the riser interior; and a process for the preparation of an olefinic product using a riser reactor system as claimed in any one of the preceding claims, the process comprising reacting an oxygenate feedstock in the presence of an oxygenate conversion catalyst under oxygenate-to-olefin conversion conditions in the riser reactor system, to obtain the olefinic product.
Abstract:
A device and method to load particles of catalyst on the order of cm in the principal dimension into an annular zone of reaction tubes which may reach a height of more than 10 metres, while satisfying the strict conditions of homogeneity and density of loading.
Abstract:
A process for filling a tube with granular material, which material is guided downwardly in a vertically oriented tube along a line provided with flexible elements in the shape of wires which are arranged substantially to the line, and having a radial dimension which is smaller than the inner diameter of the tube, the line being removed from the tube as the latter is filled with the granules, the line being moved during the removal movement with a non uniform speed which is related to the filling speed of the device.
Abstract:
A method for delivering a plurality of reactor monoliths into an interior of a reactor includes providing at least one tubular member having an outer wall defining an interior space adapted to allow sliding movement of reactor monolith therethrough, and providing a plurality of engagement members located within the interior space of the at least one tubular member and spaced along a length thereof, wherein each engagement member is actuable between an extended position and a retracted position. The at least one tubular member is extended into an interior of a reactor such that a first end of the at least one tubular member is located near an opening in the reactor, and a second end of the at least one tubular member is insert into the interior of the reactor. The plurality of engagement members may be controlled such that each engagement member actuates between the extended position, thereby preventing sliding movement of the monolith through the tube, and the retracted position, thereby allowing the monolith to slide past the engagement member within the tube.
Abstract:
Methods and apparatus are disclosed for filling solid particles into a vertical tube by conveying the particles downwardly into the tube along a loading tool that softens the fall of the particles and provides even filling of the tube. The loading tool includes a center member and a plurality of damper members that can be adapted in particular cases to the actual type of particles and the tube diameter. The damper members can be stiff or flexible since they do not occupy a substantial portion of the cross section of the tube at any particular axial location. In operation, the center member can be jerked during the filling operation while simultaneously being lifted up gradually as the tube fills or it can be sequentially lifted. The damper members reduce the falling velocity of the particles and divert the particles from falling in straight downward paths. This avoids bridge formation and breakage of the particles during filling.