METHOD AND SYSTEM FOR CONVERTING RAW COAL POWDER INTO POLYCRYSTALLINE NANO-GRAPHITE BY METAL-ASSISTED MICROWAVE TREATMENT

    公开(公告)号:US20220363547A1

    公开(公告)日:2022-11-17

    申请号:US17745643

    申请日:2022-05-16

    Inventor: TeYu Chien

    Abstract: A metal-assisted microwave treatment that converting raw coal powders into nano-graphite is presented. Specifically, four major factors are identified for successful conversion: (1) high temperature; (2) reducing environment; (3) catalyst; and (4) microwave radiation. Specifically, it is determined that the combination of the carbon sources (raw coal powders), the high temperature (microwave induced electric sparking), the reducing environment (the Ar/H2 mixture), the catalyst (Cu foil), with the microwave radiations can generate nano-graphite. This novel approach utilizes the sparking induced by the microwave radiation on the fork-shape metal foils to generate high temperature (>1000° C.) within few seconds. The small thermal load makes this method cost effective and has potential for higher temperature using metals with higher melting temperature. Refinement of this technique is possible to yield a higher quality and quantity of nano-graphite materials for a wider range of applications.

    Methods and systems for isochoric measurements using differential scanning calorimetry

    公开(公告)号:US11499928B2

    公开(公告)日:2022-11-15

    申请号:US16548898

    申请日:2019-08-23

    Abstract: In an embodiment is provided a method for measuring a vapor-liquid transition of a substance, the method including introducing a substance into a sample cell of a calorimetric block of a differential scanning calorimeter (DSC) at a first initial pressure, the system volume being constant; maintaining the substance in a vapor phase; cooling the substance at a cooling rate; and generating a thermogram. In another embodiment is provided a method for measuring a vapor-liquid transition of a substance, the method including introducing a substance into a sample cell of a calorimetric block of a DSC at a first initial pressure, the system volume being constant; maintaining the substance in a liquid phase; heating the substance at a heating rate; and generating a thermogram. In another embodiment is provided a method for measuring a vapor-liquid transition of a substance in the presence of an adsorbent.

    MODULAR REACTION CONTROL SYSTEM FOR LIVE MONITORING OF LONG-TERM AND/OR MULTI-CHANNEL REACTIONS

    公开(公告)号:US20220269233A1

    公开(公告)日:2022-08-25

    申请号:US17674700

    申请日:2022-02-17

    Abstract: A method of live monitoring of long-term and/or multi-channel reactions may include: controlling a chemical reaction apparatus via a modular control system, collecting reaction data via the digital and analog input ports, logging the reaction data via a data logging module configured to transmit the reaction data to a remote data server for data storage, periodically querying a remote interlock server for an emergency stop instruction via an emergency stop controller, inputting the emergency stop instruction into the remote interlock server via a remote user interface, executing, in response to receiving the emergency stop instruction, one or more emergency stop actions. The modular control system may include: a digital control module in electrical communication with digital input and output ports; an analog control module in electrical communication with analog input and output ports; and a pneumatic control module in pneumatic communication with pneumatic output ports.

    METHODS AND APPARATUS FOR ENHANCED OIL RECOVERY

    公开(公告)号:US20220157406A1

    公开(公告)日:2022-05-19

    申请号:US17527400

    申请日:2021-11-16

    Abstract: Embodiments of the present disclosure generally relate to methods and apparatus for enhanced oil recovery. In an embodiment, a method of enhanced oil recovery from a reservoir is provided. The method includes determining a three-dimensional molecular association between simulated oil and a simulated surface using molecular dynamics, and selecting a reservoir additive from a plurality of additives. The method further includes introducing the reservoir additive to the reservoir, and recovering oil from the reservoir using the reservoir additive. Methods of testing a candidate chemical or candidate formulation for use in enhanced oil recovery, and methods of determining an effect of a candidate chemical or formulation of candidate chemicals for use in enhanced oil recovery are also described. Oil extraction apparatus are also provided.

    HIGH VALUE PRODUCTS DERIVED FROM COAL-BASED FEEDSTOCKS

    公开(公告)号:US20220154075A1

    公开(公告)日:2022-05-19

    申请号:US17437828

    申请日:2020-03-12

    Abstract: Methods of processing a coal-based feedstock to a high value product are provided. In one embodiment a method of processing a coal-based feedstock to a high value product, the method comprises the steps of: contacting the coal-based feedstock with one or more solvents under non-pyrolytic conditions thereby generating a liquid phase; and fractionating the liquid phase to generate at least two fractions under conditions such that at least one of the fractions is the high value product. The liquid phase may comprise 5 to 25 wt % oxygen and at least 70% of the oxygen in the liquid phase may be in the form of phenolic, carboxylic and ketone functional groups of hydrocarbon-based compounds.

    QUANTUM DOT NANOFLUIDS
    80.
    发明申请

    公开(公告)号:US20210363408A1

    公开(公告)日:2021-11-25

    申请号:US17324532

    申请日:2021-05-19

    Abstract: In one embodiment, a method for recovery of an oil from a porous medium comprises contacting the porous medium with an aqueous nanofluid, solubilizing oil from the porous medium via the nanoparticles, thereby forming a dispersion comprising the oil and the aqueous nanofluid, and collecting at least some of the dispersion. The aqueous nanofluid may contain a combination of amphiphilic quantum dots and hydrophilic quantum dots, in a continuous phase. At least 90% of the quantum dot nanoparticles may have an aspect ratio of from 1:1 to 1:6. The dispersion comprising the oil and the aqueous nanofluid may be stabilized via synergistic effects resulting from the combination of amphiphilic quantum dots and hydrophilic quantum dots. In another embodiment, a method for recovery of an oil from a porous medium whereby the quantum dots are added to foaming surfactants to enhance foam lamella stability under reservoir conditions and provide conformance and mobility control in porous media and hydraulic fractures.

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