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    Method of making polyglycerol esters
    2.
    发明授权
    Method of making polyglycerol esters 失效
    制备聚甘油酯的方法

    公开(公告)号：US08722814B2

    公开(公告)日：2014-05-13

    申请号：US12451499

    申请日：2008-05-15

    申请人： Hanamanthsa Shankarsa Bevinakatti ,  Alan Geoffrey Waite ,  Jackie Frank

    发明人： Hanamanthsa Shankarsa Bevinakatti ,  Alan Geoffrey Waite ,  Jackie Frank

    IPC分类号： C08F283/00

    CPC分类号： C11C3/025 ,  C07C67/11 ,  C07C69/33 ,  C07C69/58

    摘要： Polyglycerol carboxylic acid esters are made by reaction of a, typically C2 to C30, particularly C6 to C22, carboxylic acid with glycerol carbonate, particularly with base catalyst, and desirably at temperatures from 170° C. to 250° C. Other carbonates e.g. cyclic diol carbonates such as ethylene or propylene carbonates, may be used in combination with the glycerol carbonate to make novel mixed polymeric esters. The molar ratio of carboxylic acid group to glycerol carbonate is typically from 2 to 30, but can be up to 100. The base catalyst is desirably alkali metal hydroxide, carbonate or alkoxide. The reaction is desirably carried out in an inert atmosphere, and reducing agent such as phosphorous acid, hypophosphorous acid or borohydride and/or activated carbon, may be included to improve product color.

    摘要翻译： 聚甘油羧酸酯通过一般通常为C 2至C 30，特别是C 6至C 22羧酸与甘油碳酸酯，特别是与碱催化剂，优选在170℃至250℃的温度反应制备。 环状二醇碳酸酯如乙烯或丙烯碳酸酯可以与甘油碳酸酯组合使用以制备新的混合聚合酯。 羧酸基与碳酸甘油的摩尔比通常为2-30，但可以高达100.碱催化剂优选为碱金属氢氧化物，碳酸盐或醇盐。 反应期望在惰性气氛中进行，还可以包括还原剂如亚磷酸，次磷酸或硼氢化钠和/或活性炭，以改善产品颜色。

    Treatment of hard surfaces
    4.
    发明授权
    Treatment of hard surfaces 有权
    硬表面处理

    公开(公告)号：US08709168B2

    公开(公告)日：2014-04-29

    申请号：US13504436

    申请日：2010-10-04

    申请人： Alan Geoffrey Waite ,  Trevor Graham Blease ,  Sean Alexander Robins

    发明人： Alan Geoffrey Waite ,  Trevor Graham Blease ,  Sean Alexander Robins

    IPC分类号： B08B3/04 ,  C11D1/00 ,  C11D1/62

    CPC分类号： C08G73/0226 ,  C08G73/02 ,  C11D3/3723

    摘要： Hard surfaces can be treated to improve soil resistance, particularly resistance to oily soils, by applying a composition of a quaternised, polyamine, polypropoxylate, polyethoxylate. The polyamine can be a polyethyleneimme, desirably having a molecular weight of from 10 to 50 kDa. The average length of the polypropylenoxy chains is desirably from 10 to 100 and the polyethylenoxy chains from 5 to 50 (each per NH group in the polyamine), particularly at a molar ratio of PO:EO of about 3:1. The degree of quaternization of the nitrogen atoms in the polyamine is desirably from 70 to 100%. The polymer will usually be used in solution in water or an aqueous formulation, which may include detergent and other detergent formulation components.

    摘要翻译： 通过施用季铵化的多胺，聚丙氧基化物，聚乙氧基化物的组合物，可以处理硬表面以改善土壤抗性，特别是耐油性土壤。 多胺可以是聚乙烯亚胺，理想地具有10至50kDa的分子量。 聚丙烯氧基链的平均长度优选为10〜100，聚乙烯氧基链为5〜50（多胺中的每个NH基），特别是PO:EO的摩尔比为约3:1。 多胺中氮原子的季铵化程度优选为70〜100％。 聚合物通常用于水或水性制剂中的溶液中，其可以包括洗涤剂和其它洗涤剂配方组分。

    METHOD OF MAKING POLYGLYCEROL ESTERS
    6.
    发明申请
    METHOD OF MAKING POLYGLYCEROL ESTERS 失效
    制备聚甘油酯的方法

    公开(公告)号：US20100144978A1

    公开(公告)日：2010-06-10

    申请号：US12451499

    申请日：2008-05-18

    申请人： Hanamanthsa Shankarsa Bevinakatti ,  Alan Geoffrey Waite ,  Jackie Frank

    发明人： Hanamanthsa Shankarsa Bevinakatti ,  Alan Geoffrey Waite ,  Jackie Frank

    IPC分类号： C11C3/02 ,  C07C53/00 ,  C08G63/91

    CPC分类号： C11C3/025 ,  C07C67/11 ,  C07C69/33 ,  C07C69/58

    摘要： Polyglycerol carboxylic acid esters are made by reaction of a, typically C2 to C30, particularly C6 to C22. carboxylic acid with glycerol carbonate, particularly with base catalyst, and desirably at temperatures from 170° C. to 250° C. Other carbonates e.g. cyclic diol carbonates such as ethylene or propylene carbonates, may be used in combination with the glycerol carbonate to make novel mixed polymeric esters. The molar ratio of carboxylic acid group to glycerol carbonate is typically from 2 to 30, but can be up to 100. The base catalyst is desirably alkali metal hydroxide, carbonate or alkoxide. The reaction is desirably carried out in an inert atmosphere, and reducing agent such as phosphorous acid, hypophosphorous acid or borohydride and/or activated carbon, may be included to improve product colour.

    摘要翻译： 聚甘油羧酸酯通常通常为C 2至C 30，特别是C 6至C 22的反应制备。 羧酸与甘油碳酸酯，特别是与碱催化剂反应，并且期望在170℃至250℃的温度下进行。 环状二醇碳酸酯如乙烯或丙烯碳酸酯可以与甘油碳酸酯组合使用以制备新的混合聚合酯。 羧酸基与碳酸甘油的摩尔比通常为2-30，但可以高达100.碱催化剂优选为碱金属氢氧化物，碳酸盐或醇盐。 反应期望在惰性气氛中进行，并且可以包括还原剂如亚磷酸，次磷酸或硼氢化钠和/或活性炭，以改善产品颜色。

    Treatment of Hard Surfaces
    8.
    发明申请
    Treatment of Hard Surfaces 有权
    硬表面处理

    公开(公告)号：US20120208736A1

    公开(公告)日：2012-08-16

    申请号：US13504436

    申请日：2010-10-04

    申请人： Alan Geoffrey Waite ,  Trevor Graham Blease ,  Sean Robins

    发明人： Alan Geoffrey Waite ,  Trevor Graham Blease ,  Sean Robins

    IPC分类号： C11D3/37 ,  C07C217/42 ,  C08G73/04 ,  C09D179/02 ,  C09K3/00

    CPC分类号： C08G73/0226 ,  C08G73/02 ,  C11D3/3723

    摘要： Hard surfaces can be treated to improve soil resistance, particularly resistance to oily soils, by applying a composition of a quaternised, polyamine, polypropoxylate, polyethoxylate. The polyamine can be a polyethyleneimme, desirably having a molecular weight of from 10 to 50 kDa. The average length of the polypropylenoxy chains is desirably from 10 to 100 and the polyethylenoxy chains from 5 to 50 (each per NH group in the polyamine), particularly at a molar ratio of PO:EO of about 3:1. The degree of quaternisation of the nitrogen atoms in the polyamine is desirably from 70 to 100%. The polymer will usually be used in solution in water or an aqueous formulation, which may include detergent and other detergent formulation components.

    摘要翻译： 通过施用季铵化的多胺，聚丙氧基化物，聚乙氧基化物的组合物，可以处理硬表面以改善土壤抗性，特别是耐油性土壤。 多胺可以是聚乙烯亚胺，理想地具有10至50kDa的分子量。 聚丙烯氧基链的平均长度优选为10〜100，聚乙烯氧基链为5〜50（多胺中的每个NH基），特别是PO:EO的摩尔比为约3:1。 多胺中氮原子的季铵化程度优选为70〜100％。 聚合物通常用于水或水性制剂中的溶液中，其可以包括洗涤剂和其它洗涤剂配方组分。

    Polyglycerol Derivatives
    9.
    发明申请
    Polyglycerol Derivatives 审中-公开
    聚甘油衍生物

    公开(公告)号：US20100184871A1

    公开(公告)日：2010-07-22

    申请号：US12452951

    申请日：2008-07-30

    申请人： Hanamanthsa Shankarsa Bevinakatti ,  Alan Geoffrey Waite ,  Jackie Frank

    发明人： Hanamanthsa Shankarsa Bevinakatti ,  Alan Geoffrey Waite ,  Jackie Frank

    IPC分类号： C07D307/04 ,  A61K8/06 ,  A23D7/00 ,  C09K3/00 ,  B01F17/32 ,  C10M115/04

    CPC分类号： C07D307/20 ,  C07D309/10 ,  C08G65/34

    摘要： Polyglycerol ethers of sorbitan carboxylic acid, particularly C8 to C22 carboxylic acid, esters are new surfactant compounds, useful as emulsifiers. Desirable compounds are of the formula (I): Sor(R1)(R2)(R3)(R4) where R1, R2, R3, R4 have defined meanings such that at least one group is of the formula (II): -G2CR5, where R5 is a C7 to C21 hydrocarbyl group, and at least one is of the formula (III): -[Gly]-[AO]m-H where Gly is a glycerol residue, AO is an alkyleneoxy residue of a corresponding diol cyclic carbonate, in any order; n is an average of from 0 to 100; and m is an average of from 0 to 75; such that the total of all the indices n is at least 1.

    摘要翻译： 脱水山梨糖醇羧酸的聚甘油醚，特别是C8至C22羧酸，酯是新的表面活性剂化合物，可用作乳化剂。 希望的化合物是式（I）：Sor（R 1）（R 2）（R 3）（R 4）其中R 1，R 2，R 3，R 4具有定义的含义，使得至少一个基团为式（II）：-G 2 CR 5 其中R 5为C 7至C 21烃基，至少一个为式（III）： - [Gly] - [AO] mH其中Gly为甘油残基，AO为相应的二醇环状碳酸酯的亚烷基氧基 ，以任何顺序; n为0至100的平均值; m为0〜75的平均值。 使得所有索引n的总和至少为1。