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23 条记录 (耗时 0.021 秒)

    Process for preparing 2-amino-5-cyanobenzoic acid derivatives
    1.
    发明授权
    Process for preparing 2-amino-5-cyanobenzoic acid derivatives 有权
    制备2-氨基-5-氰基苯甲酸衍生物的方法

    公开(公告)号：US08242279B2

    公开(公告)日：2012-08-14

    申请号：US12920401

    申请日：2009-03-04

    申请人： Donald J. Dumas

    发明人： Donald J. Dumas

    IPC分类号： C07D401/00

    CPC分类号： C07C253/14 ,  C07C255/58 ,  C07D231/16

    摘要： Disclosed is a method for preparing a compound of Formula 1 comprising contacting a compound of Formula 2 with a metal cyanide reagent, a copper(I) salt reagent, an iodide salt reagent and at least one compound of Formula 3 wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; X is Br or Cl; and R5, R6, R7 and R8 are as defined in the disclosure. Also disclosed is a method for preparing a compound of Formula 4 wherein R11, R12, R13 and Z are as defined in the disclosure, using a compound of Formula 1 characterized by preparing the compound of Formula 1 by the method disclosed above or using a compound of Formula 1 prepared by the method disclosed above.

    摘要翻译： 公开了一种制备式1化合物的方法，包括使式2化合物与金属氰化物试剂，铜（I）盐试剂，碘化物盐试剂和至少一种式3化合物（其中R1是NHR3或OR4）接触 ; R2是CH3或Cl; R3是H，C1-C4烷基，环丙基，环丙基环丙基，环丙基甲基或甲基环丙基; R4是H或C1-C4烷基; X是Br或Cl; 并且R5，R6，R7和R8如本公开所定义。 还公开了制备式4化合物的方法，其中R 11，R 12，R 13和Z如本公开所定义，使用式1化合物，其特征在于通过上述方法制备式1化合物或使用化合物 通过上述方法制备。

    Herbicidal sulfonamides
    4.
    发明授权
    Herbicidal sulfonamides 失效
    除草磺酰胺

    公开(公告)号：US4718938A

    公开(公告)日：1988-01-12

    申请号：US938144

    申请日：1986-12-04

    申请人： Donald J. Dumas

    发明人： Donald J. Dumas

    IPC分类号： A01N47/36 ,  C07D521/00 ,  C07D251/46 ,  A01N43/66 ,  A01N43/70 ,  C07D401/12

    CPC分类号： C07D521/00 ,  A01N47/36

    摘要： Ortho-Hydrazinosulfonyl benzenesulfonylureas, such as 2-(2,2-dimethylhydrazinosulfonyl)-N-[(4,6-dimethoxypyrimidin-2-yl)aminocarbonyl]benzenesulfonamide, are useful as pre-emergent and post-emergent herbicides.

    摘要翻译： 正 - 肼基磺酰基苯磺酰脲如2-（2,2-二甲基肼基磺酰基）-N - [（4,6-二甲氧基嘧啶-2-基）氨基羰基]苯磺酰胺可用作芽前和芽后除草剂。

    Process for preparing benzenesulfonate salts
    5.
    发明授权
    Process for preparing benzenesulfonate salts 失效
    制备苯二甲酸盐的方法

    公开(公告)号：US5153341A

    公开(公告)日：1992-10-06

    申请号：US674400

    申请日：1991-03-25

    申请人： Bijan Amini ,  Donald J. Dumas ,  George C. Sonnichsen

    发明人： Bijan Amini ,  Donald J. Dumas ,  George C. Sonnichsen

    IPC分类号： C07C303/06 ,  C07C303/32 ,  C07C309/42

    CPC分类号： C07C303/32 ,  C07C309/42

    摘要： An improved process for preparing alkanoyloxyacetyloxybenzenesulfonate salts in which phenyl esters of alkanoyloxyacetic acids (alkanoyloxyacetyloxybenzenes) are sulfonated to yield novel alkanoyloxyacetyloxybenzenesulfonic acids which, on neutralization, yield the corresponding alkanoyloxyacetyloxybenzenesulfonate salts.

    摘要翻译： 制备烷酰氧基乙酰氧基苯磺酸盐的改进方法，其中烷酰氧基乙酸（烷酰氧基乙酰氧基苯）的苯基酯被磺化以产生新的烷酰氧基乙酰氧基苯磺酸，其在中和时产生相应的烷酰氧基乙酰氧基苯磺酸盐。

    Herbicidal orthosulfonamide benzene sulfonylureas
    6.
    发明授权
    Herbicidal orthosulfonamide benzene sulfonylureas 失效
    除草剂邻苯磺酰苯磺酰脲类

    公开(公告)号：US4956005A

    公开(公告)日：1990-09-11

    申请号：US271155

    申请日：1988-11-14

    申请人： Donald J. Dumas

    发明人： Donald J. Dumas

    IPC分类号： A01N47/36 ,  C07D521/00

    CPC分类号： C07D521/00 ,  A01N47/36

    摘要： Ortho-Sulfonamide benzenesulfonylureas, such as N-cyclopropyl-N'-[(4,6-dimethoxypyrimidin-2-yl)aminocarbonyl]-1,2-benzenedisulfonamide, are useful as pre-emergent and post-emergent herbicides.

    摘要翻译： 正 - 磺酰胺苯磺酰脲如N-环丙基-N' - [（4,6-二甲氧基嘧啶-2-基）氨基羰基] -1,2-苯并二磺酰胺可用作芽前和芽后除草剂。

    PROCESS FOR PREPARING 2-AMINO-5-CYANOBENZOIC ACID DERIVATIVES
    7.
    发明申请
    PROCESS FOR PREPARING 2-AMINO-5-CYANOBENZOIC ACID DERIVATIVES 有权
    制备2-氨基-5-氰基苯甲酸衍生物的方法

    公开(公告)号：US20100280251A1

    公开(公告)日：2010-11-04

    申请号：US12516807

    申请日：2007-12-18

    申请人： Joerg Bruening ,  Gary David Annis ,  Martin James Currie ,  Donald J. Dumas ,  Rafael Shapiro

    发明人： Joerg Bruening ,  Gary David Annis ,  Martin James Currie ,  Donald J. Dumas ,  Rafael Shapiro

    IPC分类号： C07D401/04 ,  C07C253/32 ,  C07C231/22 ,  C07D231/22 ,  C07D231/12

    CPC分类号： C07C253/14 ,  C07C231/12 ,  C07C233/65 ,  C07C255/58

    摘要： Disclosed is a method for preparing a compound of Formula 1 comprising contacting a compound of Formula 2 with a metal cyanide reagent, a copper(I) salt reagent, an iodide salt reagent and at least one compound of Formula 3 wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; Y is Br or Cl; X is NR13 or O; n is 0 or 1; and R5, R6, R7, R8, R9, R10, R11, R12 and R13 are as defined in the disclosure.Also disclosed is a method for preparing a compound of Formula 2 wherein Y is Br and R1 is NHR3 comprising introducing a gas containing bromine into a liquid containing a compound of Formula 4, and further disclosed is a method for preparing a compound of Formula 5 wherein R14, R15, R16 and Z are as defined in the disclosure using a compound of Formula 1 characterized by preparing the compound of Formula 1 by the method disclosed above.

    摘要翻译： 公开了一种制备式1化合物的方法，包括使式2化合物与金属氰化物试剂，铜（I）盐试剂，碘化物盐试剂和至少一种式3化合物（其中R1是NHR3或OR4）接触 ; R2是CH3或Cl; R3是H，C1-C4烷基，环丙基，环丙基环丙基，环丙基甲基或甲基环丙基; R4是H或C1-C4烷基; Y为Br或Cl; X为NR 13或O; n为0或1; 并且R5，R6，R7，R8，R9，R10，R11，R12和R13如本公开所定义。 还公开了制备式2化合物的方法，其中Y是Br，R 1是NHR 3，包括将含溴的气体引入含有式4化合物的液体中，并且还公开了制备式5化合物的方法，其中 R14，R15，R16和Z如本公开中所定义，使用式1的化合物，其特征在于通过上述方法制备式1的化合物。

    Processes for preparing indeno[1,2-E][1,3,4]oxadiazine-dicarboxylates
    8.
    依法登记的发明
    Processes for preparing indeno[1,2-E][1,3,4]oxadiazine-dicarboxylates 有权

    公开(公告)号：USH1950H1

    公开(公告)日：2001-03-06

    申请号：US09230987

    申请日：1999-02-03

    申请人： Donald J. Dumas

    发明人： Donald J. Dumas

    IPC分类号： C07D49800

    摘要： Oxadiazines of formula I, wherein R1 is F, Cl or fluoroalkoxy and R2 is alkyl, are prepared by reacting hydrazine derivatives of formula II with a dialkoxymethane in the presence of a protic acid catalyst in an inert solvent under conditions which allow for the prompt removal of the alcohol by-product by distillation. The reaction can be combined with the preparation of the hydrazines derivatives II from the corresponding ketones and hydrazines NH2-NHR3 in the presence of the same protic acid catalyst and an inert solvent. Oxadiazines I are useful as intermediates in the preparation of arthropodicidal agents.