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13 条记录 (耗时 0.01 秒)

    Process for preparing primary amines from aldehydes
    3.
    发明授权
    Process for preparing primary amines from aldehydes 失效
    从醛制备伯胺的方法

    公开(公告)号：US5475141A

    公开(公告)日：1995-12-12

    申请号：US253305

    申请日：1994-06-03

    申请人： Carlo Kos ,  Friedrich Hebesberger ,  Eduard Artner ,  Engelbert Kloimstein ,  Robert Haar ,  Ernst Lust

    发明人： Carlo Kos ,  Friedrich Hebesberger ,  Eduard Artner ,  Engelbert Kloimstein ,  Robert Haar ,  Ernst Lust

    IPC分类号： C07C209/26 ,  C07D213/38 ,  C07C209/00

    CPC分类号： C07D213/38 ,  C07C209/26

    摘要： Process for preparing primary amines from aldehydes by mixing an aldehyde with a diluent, where in the case of an alcohol or of water as diluent the mixing temperature is at most 5.degree. C. to prevent the formation of the hemiacetal or the aldehyde hydrate, and bringing the mixture into contact with a mixture of ammonia, hydrogen and hydrogenation catalyst, whereby the formation of an imine is prevented, at temperatures of from 60.degree. to 180.degree. C. and pressures of from 20 to 60 bar, at least 15 mol of ammonia being used per mol of aldehyde group, and also an apparatus for carrying out the process.

    摘要翻译： 通过将醛与稀释剂混合制备伯胺的方法，其中在醇或水作为稀释剂的情况下，混合温度为至多5℃，以防止形成半缩醛或醛水合物，以及 使混合物与氨，氢气和氢化催化剂的混合物接触，从而在60℃至180℃的温度和20至60巴的压力，至少15摩尔的 每摩尔醛基使用氨，以及用于进行该方法的装置。

    Amine salts of phenyl-4-hydroxypyridazines and the preparation and herbicidal compositions thereof
    8.
    发明授权
    Amine salts of phenyl-4-hydroxypyridazines and the preparation and herbicidal compositions thereof 失效
    苯基-4-羟基哒嗪的胺盐及其制备和除草组合物

    公开(公告)号：US4058390A

    公开(公告)日：1977-11-15

    申请号：US641588

    申请日：1975-12-16

    申请人： Rupert Schonbeck ,  Engelbert Kloimstein ,  Erwin Wittmann

    发明人： Rupert Schonbeck ,  Engelbert Kloimstein ,  Erwin Wittmann

    IPC分类号： A01N43/58 ,  A01P13/00 ,  C07D237/14 ,  A01N9/24

    CPC分类号： C07D237/14

    摘要： Amine salts of 3-phenyl-6-halo-4-hydroxypyridazines of the formula: ##STR1## in which X is a chlorine or bromine atom, R.sub.1 is an alkyl group containing up to 14 carbon atoms, which group may be substituted by a hydroxy group, an alkoxy group containing up to 10 carbon atoms, cyano group, amino group or lower mono- or lower dialkylamino group, an alkenyl group containing up to 6 carbon atoms or a cycloalkyl group containing 5, 6 or 7 carbon atoms, and R.sub.2 and R.sub.3 have the same meaning as R.sub.1 or each is a hydrogen atom, or R.sub.1 and R.sub.2 together with the nitrogen atom of the amine form a 5- or 6-membered heterocyclic group which may also contain oxygen and which may be mono- or di- substituted by alkyl, and herbicidal compositions containing them.

    摘要翻译： 下式的3-苯基-6-卤代-4-羟基哒嗪的胺盐：其中X是氯或溴原子，R1是含有至多14个碳原子的烷基，该基团可以被 羟基，含有至多10个碳原子的烷氧基，氰基，氨基或低级单 - 或低级二烷基氨基，含有至多6个碳原子的链烯基或含有5,6或7个碳原子的环烷基，以及 R2和R3具有与R 1相同的含义或者各自为氢原子，或者R 1和R 2与胺的氮原子一起形成也可含有氧的5-或6-元杂环基，并且其可以是单 - 或 二烷基取代，和含有它们的除草组合物。

    Method for producing monocarbonyl compounds or biscarbonyl compounds or hydroxyl compounds
    10.
    发明授权
    Method for producing monocarbonyl compounds or biscarbonyl compounds or hydroxyl compounds 失效
    生产单羰基化合物或双羰基化合物或羟基化合物的方法

    公开(公告)号：US07169950B2

    公开(公告)日：2007-01-30

    申请号：US10469306

    申请日：2002-02-13

    申请人： Alexander Sajtos ,  Engelbert Kloimstein ,  Curt Zimmermann

    发明人： Alexander Sajtos ,  Engelbert Kloimstein ,  Curt Zimmermann

    IPC分类号： C07C69/66 ,  C07C47/00 ,  C07C45/00

    CPC分类号： C07D213/48 ,  C07B41/06 ,  C07C41/50 ,  C07C45/40 ,  C07C67/313 ,  C07C315/04 ,  C07C47/19 ,  C07C47/198 ,  C07C49/433 ,  C07C47/544 ,  C07C69/716 ,  C07C317/24 ,  C07C43/307

    摘要： The invention relates to a method for producing monocarbonyl compounds or biscarbonyl compounds or hydroxyl compounds by ozonizing, unsaturated organic carbon compounds that, per molecule, have one or more olefinic or aromatic double bonds, which can be cleaved by ozone, and by subsequently processing the ozonization products. According to the inventive method, unsaturated organic carbon compounds that, per molecule, have one or more olefinic or aromatic double bonds, which can be cleaved by ozone, are: (a) in 1 to 2 steps, continuously reacted with ozone in stoichiometric quantities or in excess while using counter educt currents and being in an organic solvent or in an aqueous solution inside a device, which consists of one to two absorption apparatuses, of devices for carrying away reaction heat, and of devices for separating the gas and liquid phases, and; (b) the peroxides resulting therefrom are, according to reaction parameters from step (a), converted into the corresponding monocarbonyl compounds or biscarbonyl compounds or hydroxyl compounds either by continuous or discontinuous hydrogenation, oxidation or heating.

    摘要翻译： 本发明涉及通过臭氧化不饱和有机碳化合物生产单羰基化合物或双羰基化合物或羟基化合物的方法，每分子具有一个或多个可被臭氧切割的烯属或芳族双键，并且随后将 臭氧化产品。 根据本发明的方法，每分子具有一个或多个可被臭氧裂解的烯属或芳族双键的不饱和有机碳化合物是：（a）以1至2个步骤与化学计量的臭氧连续反应 或者在使用反向流动电流并且在有机溶剂中或在由一至两个吸收装置组成的装置内的水溶液中用于携带反应热的装置以及用于分离气相和液相的装置 ，和 （b）根据来自步骤（a）的反应参数，由此产生的过氧化物通过连续或不连续氢化，氧化或加热转化成相应的单羰基化合物或双羰基化合物或羟基化合物。