Method for Producing Oxygen-Containing Compound
    1.
    发明申请
    Method for Producing Oxygen-Containing Compound 失效
    生产含氧化合物的方法

    公开(公告)号:US20120053354A1

    公开(公告)日:2012-03-01

    申请号:US13201918

    申请日:2010-02-17

    申请人: Masaaki Yoshida

    发明人: Masaaki Yoshida

    摘要: [Problem] There is provided a method for producing an oxygen-containing compound safely and with improved reaction efficiency, in which an undesired peroxide is unlikely to be produced, and efficient heat exchange of the ozonization can be achieved.[Mean for solving the Problem] The method comprises an ozonization reaction step of continuously supplying, together with an organic compound, ozone having an oxygen content of less than 10% in a dissolved state in high-pressure carbon dioxide to an ozonization reaction section having a thin tubular shape, and reacting the ozone and the organic compound under conditions that suppress generation of oxygen due to thermal decomposition of the ozone, thereby continuously producing an ozonide; and a decomposition reaction step of continuously supplying the ozonide produced in the ozonization reaction step to a decomposition reaction section having a thin tubular shape, thereby continuously producing an oxygen-containing compound, the decomposition reaction step being provided in a manner continuous with the ozonization reaction step.

    摘要翻译: [问题]提供了一种安全地生产含氧化合物的方法,并且具有改善的反应效率,其中不太可能产生不期望的过氧化物,并且可以实现臭氧化的有效的热交换。 [解决问题的意思]该方法包括臭氧化反应步骤,与臭氧化反应步骤一起,在有机化合物中将氧含量低于10%的臭氧在高压二氧化碳中的溶解状态提供给具有 细管状,并且在抑制臭氧热分解产生氧的条件下使臭氧和有机化合物反应,从而连续生产臭氧化物; 以及分解反应步骤,将在臭氧化反应步骤中生产的臭氧化物连续供给到具有薄管状分解反应段,从而连续生产含氧化合物,分解反应步骤以与臭氧化反应连续的方式提供 步。

    Process for the purification of ketones obtained from the corresponding terpenes by ozonolysis and reduction
    6.
    发明申请
    Process for the purification of ketones obtained from the corresponding terpenes by ozonolysis and reduction 失效
    通过臭氧分解和还原从相应的萜烯中纯化酮的方法

    公开(公告)号:US20020077510A1

    公开(公告)日:2002-06-20

    申请号:US10012539

    申请日:2001-12-12

    IPC分类号: C07C045/40

    摘要: Improved, safe process for the purification of ketones obtained by ozonolysis and subsequent reduction of the corresponding terpenes, in which, after the ozonolysis and reduction of acyclic mono-, bi- or tricyclic terpenes with ozonizable double bonds, converting the resulting corresponding crude ketone into a high-purity ketone by means of steam distillation at atmospheric pressure or at reduced pressure, extraction of the steam distillate and subsequent distillation.

    摘要翻译: 改进的安全方法是通过臭氧分解和随后还原相应的萜烯得到的酮的纯化,其中在臭氧分解和用可臭化双键还原无环单,双或三环萜烯之后,将所得的相应的粗酮转化成 通过在大气压或减压下蒸汽蒸馏的高纯度酮,萃取蒸馏馏分并随后进行蒸馏。