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    COATING COMPOSITION, AND A PROCESS FOR PRODUCING THE SAME
    2.
    发明申请
    COATING COMPOSITION, AND A PROCESS FOR PRODUCING THE SAME 有权
    涂料组合物及其制造方法

    公开(公告)号：US20140024742A1

    公开(公告)日：2014-01-23

    申请号：US14009634

    申请日：2011-04-08

    申请人： Charles S. Kan ,  Rebecca S. Ortiz ,  John A. Roper, III ,  Jane Elizabeth Weier ,  Timothy J. Young ,  Gary E. Spilman ,  Ray E. Drumright

    发明人： Charles S. Kan ,  Rebecca S. Ortiz ,  John A. Roper, III ,  Jane Elizabeth Weier ,  Timothy J. Young ,  Gary E. Spilman ,  Ray E. Drumright

    IPC分类号： C09D167/00 ,  C09D163/00

    CPC分类号： C09D167/00 ,  C09D123/00 ,  C09D163/00 ,  C09D167/08 ,  C08L23/00 ,  C08L75/04 ,  C08L67/00 ,  C08L63/00

    摘要： The present invention provides a coating composition, a process for producing the same, one or more coating layers derived therefrom, and articles comprising one or more such coating layers. The coating composition according to the present invention comprises: (a) from 10 to 90 percent by weight of an aqueous, high-solid, solvent-free alkyd dispersion comprising: (i) from 40 to 70 percent by weight of one or more alkyds based on the total weight of the dispersion, wherein each said one or more alkyds has an acid value of less than 20 and a molecular weight (Mn) in the range of greater than 1000 Dalton; (ii) from less than 10 percent by weight of one or more surfactants, based on the total weight of the dispersion; and (iii) from 30 to 55 percent by weight of water, based on the total weight of the dispersion; wherein said aqueous, high-solid, solvent-free alkyd dispersion has an average particle size diameter in the range of from 0.05 to 5 μm; (b) from 10 to 90 one or more second dispersions, one or more second emulsions, or combinations thereof; wherein said coating composition has a solid content of in the range of from 25 to 65 percent by weight of solid content, based on the total weight of the coating composition, and the coating composition has a pH in the range of from 7 to 11, and wherein the coating composition has a volume average particle size in the range of from 0.03 to 5 μm, and wherein the coating composition has a viscosity in the range of from 100 to 10,000 cP.

    摘要翻译： 本发明提供一种涂料组合物，其制备方法，由其衍生的一种或多种涂层，以及包含一种或多种这样的涂层的制品。 根据本发明的涂料组合物包含：（a）10至90重量％的水性，高固体，无溶剂的醇酸树脂分散体，其包含：（i）40至70重量％的一种或多种醇酸树脂 基于分散体的总重量，其中每个所述一种或多种醇酸树脂的酸值小于20，分子量（Mn）在大于1000道尔顿范围内; （ii）基于分散体的总重量，少于10重量％的一种或多种表面活性剂; 和（iii）基于分散体的总重量的30至55重量％的水; 其中所述水性，高固体，无溶剂的醇酸树脂分散体的平均粒度直径为0.05-5μm; （b）10至90个一种或多种第二分散体，一种或多种第二乳液或其组合; 其中所述涂料组合物的固体含量为固体含量的25至65重量％，基于涂料组合物的总重量，并且涂料组合物的pH为7至11， 并且其中所述涂料组合物的体积平均粒度在0.03至5μm的范围内，并且其中所述涂料组合物具有在100至10,000cP范围内的粘度。

    ROOM TEMPERATURE CURABLE POLYMERS AND PRECURSORS THEREOF
    3.
    发明申请
    ROOM TEMPERATURE CURABLE POLYMERS AND PRECURSORS THEREOF 有权

    公开(公告)号：US20100249357A1

    公开(公告)日：2010-09-30

    申请号：US12668609

    申请日：2008-07-10

    申请人： Paul J. Popa ,  Zenon Lysenko ,  David A. Babb ,  William A. Koonce ,  Gary E. Spilman

    发明人： Paul J. Popa ,  Zenon Lysenko ,  David A. Babb ,  William A. Koonce ,  Gary E. Spilman

    IPC分类号： C08G18/42 ,  C08G63/00

    CPC分类号： C08G18/4288 ,  C08G18/4269 ,  C08G18/4277 ,  C08G18/718 ,  C08G2190/00 ,  C09J175/06

    摘要： A polyester polyol, referred to hereinafter as a MHMS polyol comprises fatty acid based mer units wherein at least about 80 weight percent of the fatty acid based mer units are from methyl 9 (10) hydroxymethylstearate, or is prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof and which has an average hydroxyl functionality of from 1.5 to 4. A reaction product, referred to herein after as MHMS alkoxysilane prepolymer, is produced from at least one such MHMS polyol and at least one isocyanate functional silane. The prepolymer is moisture cured to form a silylated MHMS polymer. The process of preparing a MHMS polyol comprises (A) reacting a fatty acid ester wherein at least about 80 weight percent of the fatty acid esters are methyl 9 (10) hydroxymethylstearate, or are prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof with an initiator having at least 2 reactive groups selected from primary hydroxyl groups, amine groups, terminal isocyanate groups, terminal carbonyl groups or a combination thereof. The process of preparing at least one MHMS alkoxysilane prepolymer comprises steps of: (a) supplying at least one MHMS polyol; (b) supplying at least one isocyanate functional silane and (c) admixing the MHMS polyol and isocyanate functional silane or combination thereof, optionally in the presence of at least one catalyst to produce at least one MHMS alkoxysilane prepolymer. A process of preparing at least one silylated MHMS polymer comprises steps of: (a) supplying at least one MHMS alkoxysilane prepolymer; and (b) exposing it to moisture under conditions such that at least one silylated MHMS polymer is formed. Articles comprising the polyol, prepolymer, or polymer include elastomers, sealants, adhesives, coatings and the like.

    Polyester coil coating formulation
    5.
    发明授权
    Polyester coil coating formulation 有权
    聚酯线圈涂料配方

    公开(公告)号：US08716429B2

    公开(公告)日：2014-05-06

    申请号：US12523333

    申请日：2008-01-29

    申请人： Gary E. Spilman ,  Scott J. Bis ,  Paul J. Popa

    发明人： Gary E. Spilman ,  Scott J. Bis ,  Paul J. Popa

    IPC分类号： C08G63/00

    CPC分类号： C09D167/00 ,  C08G63/199

    摘要： In a curable coil coating composition comprising a mixture of: (a) a curable polyester that is a liquid at room temperature, (b) a cross-linking agent; and (c) a solvent; the improvement comprising preparing the polyester from a composition comprising a mixture of 1,3- and 1,4-cyclohexane dimethanol wherein the molar ratio of the 1,3 isomer to the 1,4 isomer is from about 60:40 to about 5:95. Cured coil coatings prepared from these compositions exhibit an excellent combination of flexibility and hardness.

    摘要翻译： 一种可固化线圈涂料组合物，其包含以下混合物：（a）在室温下为液体的可固化聚酯，（b）交联剂; 和（c）溶剂; 改进包括由包含1,3-和1,4-环己烷二甲醇的混合物的组合物制备聚酯，其中1,3异构体与1,4-异构体的摩尔比为约60:40至约5： 95。 由这些组合物制备的固化线圈涂层显示出柔韧性和硬度的优异组合。

    Reducing ionic impurities content in aromatic polycarbonate resins
    6.
    发明授权
    Reducing ionic impurities content in aromatic polycarbonate resins 失效
    降低芳族聚碳酸酯树脂中的离子杂质含量

    公开(公告)号：US5907027A

    公开(公告)日：1999-05-25

    申请号：US82106

    申请日：1998-05-20

    申请人： Gary E. Spilman ,  Eric T. Gohr ,  David A. Bradley

    发明人： Gary E. Spilman ,  Eric T. Gohr ,  David A. Bradley

    IPC分类号： C08G64/40 ,  C08L69/00 ,  C08G64/00

    CPC分类号： C08G64/406 ,  C08L69/00

    摘要： An aromatic polycarbonate composition having less than 400 parts per billion each of ionic impurities, particularly sulfate, chloride and fluoride ions prepared by devolatilizing the ionic impurities from a polycarbonate composition employing an aqueous medium of about 1% by weight based on the weight of the polycarbonate composition. Preferably the devolatilizing is carried out in an extruder during compounding the polycarbonate composition and preferably under a vacuum. Also, the extruded strands of polycarbonate resin are quenched in a deionized water bath.

    摘要翻译： 一种芳族聚碳酸酯组合物，其具有小于400重量份的离子杂质，特别是硫酸盐，氯化物和氟离子，其通过使用基于聚碳酸酯的重量约1重量％的水性介质的聚碳酸酯组合物脱挥发分而制备 组成。 优选地，在组合聚碳酸酯组合物期间，优选在真空下，在挤出机中进行脱挥发分。 此外，聚碳酸酯树脂的挤出股线在去离子水浴中淬火。

    CURABLE SILYL POLYMERS
    7.
    发明申请
    CURABLE SILYL POLYMERS 审中-公开
    可固化的SILYL聚合物

    公开(公告)号：US20130096251A1

    公开(公告)日：2013-04-18

    申请号：US13700961

    申请日：2011-06-21

    申请人： Paul J. Popa ,  Gary E. Spilman ,  Zenon Lysenko ,  William A. Koonce ,  David A. Bobb ,  Martin C. Beebe ,  Thomas C. Thyne

    发明人： Paul J. Popa ,  Gary E. Spilman ,  Zenon Lysenko ,  William A. Koonce ,  David A. Bobb ,  Martin C. Beebe ,  Thomas C. Thyne

    IPC分类号： C08G18/83 ,  C08G18/12

    CPC分类号： C08G18/837 ,  C08G18/10 ,  C08G18/12 ,  C08G18/289 ,  C08G18/4891 ,  C08G18/7621 ,  C09D175/04 ,  C09J175/04

    摘要： Embodiments of the invention relate to crosslinkable silyl group-containing polymers and methods of producing them. In one embodiment a method of producing a silyl polymer is provided. The method includes reacting at least one natural oil based polyol with at least one isocyanate to form at least one prepolymer having at least one NCO group. The at least one natural oil based polyol includes the reaction product of hydroxymethylated fatty acids or esters thereof and at least one polyol initiator. The prepolymer having at least one NCO group is reacted with at least one amino functional alkoxy silane to form the silyl polymer, such that the silyl polymer includes at least one crosslinkable silyl group, at least one urethane group, and at least one urea group in each molecule.

    摘要翻译： 本发明的实施方案涉及可交联的含甲硅烷基的聚合物及其制备方法。 在一个实施方案中，提供了产生甲硅烷基聚合物的方法。 所述方法包括使至少一种天然油基多元醇与至少一种异氰酸酯反应以形成至少一种具有至少一个NCO基团的预聚物。 所述至少一种天然油基多元醇包括羟甲基化脂肪酸或其酯与至少一种多元醇引发剂的反应产物。 具有至少一个NCO基团的预聚物与至少一个氨基官能的烷氧基硅烷反应以形成甲硅烷基聚合物，使得甲硅烷基聚合物包括至少一个可交联甲硅烷基，至少一个氨基甲酸酯基和至少一个脲基 每个分子。

    COATING COMPOSITION, AND A PROCESS FOR PRODUCING THE SAME
    8.
    发明申请
    COATING COMPOSITION, AND A PROCESS FOR PRODUCING THE SAME 有权
    涂料组合物及其制造方法

    公开(公告)号：US20110207850A1

    公开(公告)日：2011-08-25

    申请号：US13083078

    申请日：2011-04-08

    申请人： Charles S. Kan ,  Rebecca S. Ortiz ,  John A. Roper, III ,  Jane E. Weier ,  Timothy J. Young ,  Gary E. Spilman ,  Ray E. Drumright

    发明人： Charles S. Kan ,  Rebecca S. Ortiz ,  John A. Roper, III ,  Jane E. Weier ,  Timothy J. Young ,  Gary E. Spilman ,  Ray E. Drumright

    IPC分类号： C09D167/00 ,  C09D163/00 ,  C09D133/08 ,  C09D131/04

    CPC分类号： C09D167/08 ,  C08J3/03 ,  C08J3/05 ,  C08J2367/08 ,  C09D5/022 ,  Y10T428/31786 ,  Y10T428/31938

    摘要： The present invention provides a coating composition, a process for producing the same, one or more coating layers derived therefrom, and articles comprising one or more such coating layers. The coating composition according to the present invention comprises: (a) from 10 to 90 percent by weight of an aqueous, high-solid, solvent-free alkyd dispersion comprising: (i) from 40 to 70 percent by weight of one or more alkyds based on the total weight of the dispersion, wherein each said one or more alkyds has an acid value of less than 20 and a molecular weight (Mn) in the range of greater than 1000 Dalton; (ii) from less than 10 percent by weight of one or more surfactants, based on the total weight of the dispersion; and (iii) from 30 to 55 percent by weight of water, based on the total weight of the dispersion; wherein said aqueous, high-solid, solvent-free alkyd dispersion has an average particle size diameter in the range of from 0.05 to 5 μm; (b) from 10 to 90 one or more second dispersions, one or more second emulsions, or combinations thereof; wherein said coating composition has a solid content of in the range of from 25 to 65 percent by weight of solid content, based on the total weight of the coating composition, and the coating composition has a pH in the range of from 7 to 11, and wherein the coating composition has a volume average particle size in the range of from 0.03 to 5 μm, and wherein the coating composition has a viscosity in the range of from 100 to 10,000 cP.

    摘要翻译： 本发明提供一种涂料组合物，其制备方法，由其衍生的一种或多种涂层，以及包含一种或多种这样的涂层的制品。 根据本发明的涂料组合物包含：（a）10至90重量％的水性，高固体，无溶剂的醇酸树脂分散体，其包含：（i）40至70重量％的一种或多种醇酸树脂 基于分散体的总重量，其中每个所述一种或多种醇酸树脂的酸值小于20，分子量（Mn）在大于1000道尔顿范围内; （ii）基于分散体的总重量，少于10重量％的一种或多种表面活性剂; 和（iii）基于分散体的总重量的30至55重量％的水; 其中所述水性，高固体，无溶剂的醇酸树脂分散体的平均粒度直径在0.05至5μm的范围内; （b）10至90个一种或多种第二分散体，一种或多种第二乳液或其组合; 其中所述涂料组合物的固体含量为固体含量的25至65重量％，基于涂料组合物的总重量，并且涂料组合物的pH为7至11， 并且其中所述涂料组合物的体积平均粒径在0.03至5μm的范围内，并且其中所述涂料组合物的粘度在100至10000cP的范围内。

    POLYESTER COIL COATING FORMULATION
    9.
    发明申请
    POLYESTER COIL COATING FORMULATION 有权
    聚酯线圈涂层配方

    公开(公告)号：US20100076154A1

    公开(公告)日：2010-03-25

    申请号：US12523333

    申请日：2008-01-29

    申请人： Gary E. Spilman ,  Scott J. Bis ,  Paul J. Popa

    发明人： Gary E. Spilman ,  Scott J. Bis ,  Paul J. Popa

    IPC分类号： C09D167/00 ,  C09D167/02

    CPC分类号： C09D167/00 ,  C08G63/199

    摘要： In a curable coil coating composition comprising a mixture of: (a) a curable polyester that is a liquid at room temperature, (b) a cross-linking agent; and (c) a solvent; the improvement comprising preparing the polyester from a composition comprising a mixture of 1,3- and 1,4-cyclohexane dimethanol wherein the molar ratio of the 1, 3 isomer to the 1, 4 isomer is from about 60:40 to about 5:95. Cured coil coatings prepared from these compositions exhibit an excellent combination of flexibility and hardness.

    摘要翻译： 一种可固化线圈涂料组合物，其包含以下混合物：（a）在室温下为液体的可固化聚酯，（b）交联剂; 和（c）溶剂; 改进包括由包含1,3-和1,4-环己烷二甲醇的混合物的组合物制备聚酯，其中1,3异构体与1,4异构体的摩尔比为约60:40至约5： 95。 由这些组合物制备的固化线圈涂层显示出柔韧性和硬度的优异组合。

    Low volatiles coatings, sealants and binders from renewable oils
    10.
    发明授权
    Low volatiles coatings, sealants and binders from renewable oils 有权
    低挥发性涂料，密封剂和可再生油的粘合剂

    公开(公告)号：US08486526B2

    公开(公告)日：2013-07-16

    申请号：US12597061

    申请日：2008-04-10

    申请人： Gary E. Spilman ,  John N. Argyropoulos ,  Debkumar Bhattacharjee ,  Paul J. Popa ,  William A. Koonce

    发明人： Gary E. Spilman ,  John N. Argyropoulos ,  Debkumar Bhattacharjee ,  Paul J. Popa ,  William A. Koonce

    IPC分类号： B32B7/12 ,  B32B27/00 ,  B32B27/40 ,  B05D3/02 ,  C08G63/08

    CPC分类号： C08G18/4288 ,  C08G18/3851 ,  C08G18/4063 ,  C08G18/6229 ,  C08G18/755 ,  C08K5/1515 ,  C08K5/29 ,  C08K5/34922 ,  C09D175/04 ,  Y10T428/2852

    摘要： A composition comprises (a) a binder component which comprises (1) 5 to 100 weight percent of at least one natural oil derived polyol having at least about 50 percent primary hydroxyl groups and (2) sufficient additional polyol different from a natural oil derived polyol to make 100 percent wherein the natural oil derived polyol has an average of from 1.5 to 3 hydroxyl groups per molecule and an equivalent weight of from 200 to 5000; and (b) a crosslinking component reactive with hydroxyl groups. Furthermore, a process for producing a coating, adhesive, binder or combination thereof on the surface of a substrate, comprises in any order: (a) admixing binder and crosslinking components of a composition to form an admixture, wherein a binder component comprises (1) 5 to 100 weight percent of at least one natural oil derived polyol having at least about 50 percent primary hydroxyl groups and (2) sufficient additional polyol different from a natural oil derived polyol to make 100 percent wherein the natural oil derived polyol has an average of from 1.5 to 3 hydroxyl groups per molecule and an equivalent weight of from 200 to 5000; and (b) applying a layer of said admixture on said surface. The invention includes coatings, adhesives, binders and combinations thereof prepared from any composition of the invention, substrates coated by the process of the invention or coated using a composition of the invention and articles, including laminates, comprising a coating, adhesive, binder or combination thereof of the invention.

    摘要翻译： 组合物包含（a）粘合剂组分，其包含（1）5至100重量％的至少一种具有至少约50％伯羟基的天然油衍生的多元醇和（2）与天然油衍生的多元醇不同的足够的另外的多元醇 以制备100％，其中天然油衍生的多元醇的平均值为每分子1.5至3个羟基，当量为200至5000; 和（b）与羟基反应的交联组分。 此外，在基材表面上制备涂料，粘合剂，粘合剂或其组合的方法包括以下任意顺序：（a）混合粘合剂和组合物的交联组分以形成混合物，其中粘合剂组分包含（1 ）5至100重量％的至少一种具有至少约50％伯羟基的天然油衍生的多元醇，和（2）与天然油衍生的多元醇不同的足够额外的多元醇以制备100％，其中天然油衍生的多元醇具有平均值 每个分子为1.5至3个羟基，当量为200至5000; 和（b）在所述表面上施加一层所述混合物。 本发明包括由本发明的任何组合物制备的涂料，粘合剂，粘合剂及其组合，通过本发明的方法涂覆的基材或使用本发明的组合物涂覆的基材和包括层压材料的制品，其包括涂料，粘合剂，粘合剂或组合 的本发明。