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    1-Phenyl-cyclooctadiene (1,5)
    3.
    发明授权
    1-Phenyl-cyclooctadiene (1,5) 失效
    1-苯基 - 环辛二烯（1,5）

    公开(公告)号：US4070406A

    公开(公告)日：1978-01-24

    申请号：US737765

    申请日：1976-11-01

    Applicant: Gunther Wilke ,  Paul Heimbach

    Inventor： Gunther Wilke ,  Paul Heimbach

    IPC: C07C2/02 ,  C07C2/42 ,  C07C13/00 ,  C07C13/20 ,  C07C13/263 ,  C07C13/271 ,  C07C13/277 ,  C07C13/28 ,  C07C13/32 ,  C07C13/605 ,  C07C43/188 ,  C07C15/00 ,  C07C3/035

    CPC classification number: C07C43/188 ,  C07C13/00 ,  C07C13/20 ,  C07C13/263 ,  C07C13/271 ,  C07C13/277 ,  C07C13/28 ,  C07C13/32 ,  C07C13/605 ,  C07C2/02 ,  C07C2/42 ,  C07C2101/14 ,  C07C2101/16 ,  C07C2101/18 ,  C07C2101/20 ,  C07C2103/84

    Abstract: A series of mono, bi and tricarbocyclic compounds, most of which have olefinic unsaturation in the ring, which may or may not have substituents thereon. While the bi and tricyclic rings may be unsubstituted, these compounds which have olefinic unsaturation, particularly multiple olefinic unsaturation, are polymerizable and copolymerizable in known polymerization systems. They are particularly good crosslinking agents. These compounds are further useful in the sense that they can be cleaved oxidatively, to corresponding carboxylic acids, aldehydes and/or alcohols which have known utility in the plasticizer and detergent arts. The compounds which do not have olefinic unsaturation can also be oxidatively cleaved to produce oxygenated, e.g., acid, alcohol or aldehyde, compounds having known utility.

    Abstract translation: 一系列单环，双和三环化合物，其中大多数在环中具有烯属不饱和键，其可以具有或不具有取代基。 虽然双环和三环可以是未取代的，但是具有烯属不饱和键，特别是多个烯属不饱和键的这些化合物在已知的聚合体系中是可聚合的和可共聚的。 它们是特别好的交联剂。 这些化合物在它们可以被氧化裂解的意义上可进一步用于在增塑剂和洗涤剂领域已知有用的相应的羧酸，醛和/或醇。 不具有烯属不饱和键的化合物也可被氧化裂解以产生氧化的，例如酸，醇或醛，已知有用的化合物。

    Ethyl 3,7-cyclodecadiene-1-carboxylate
    4.
    发明授权
    Ethyl 3,7-cyclodecadiene-1-carboxylate 失效
    3,7-环癸二烯-1-羧酸乙酯

    公开(公告)号：US4056552A

    公开(公告)日：1977-11-01

    申请号：US565282

    申请日：1975-04-04

    Applicant: Gunther Wilke ,  Paul Heimbach

    Inventor： Gunther Wilke ,  Paul Heimbach

    IPC: C07C69/74

    CPC classification number: C07C2102/32 ,  C07C2103/84

    Abstract: A series of mono, bi and tricarbocyclic compounds, most of which have olefinic unsaturation in the ring, which may or may not have substituents thereon. While the bi and tricyclic rings may be unsubstituted, these compounds which have olefinic unsaturation, particularly multiple olefinic unsaturation, are polymerizable and copolymerizable in known polymerization systems. They are particularly good crosslinking agents. These compounds are further useful in the sense that they can be cleaved oxidatively, to corresponding carboxylic acids, aldehydes and/or alcohols which have known utility in the plasticizer and detergent arts. The compounds which do not have olefinic unsaturation can also be oxidatively cleaved to produce oxygenated, e.g., acid, alcohol or aldehyde, compounds having known utility.

    Abstract translation: 一系列单环，双和三环化合物，其中大多数在环中具有烯属不饱和键，其可以具有或不具有取代基。 虽然双环和三环可以是未取代的，但是具有烯属不饱和键，特别是多个烯属不饱和键的这些化合物在已知的聚合体系中是可聚合的和可共聚的。 它们是特别好的交联剂。 这些化合物在它们可以被氧化裂解的意义上可进一步用于在增塑剂和洗涤剂领域已知有用的相应的羧酸，醛和/或醇。 不具有烯属不饱和键的化合物也可被氧化裂解以产生氧化的，例如酸，醇或醛，已知有用的化合物。

    Process for the electrochemical synthesis of organic metal compounds
    6.
    发明授权
    Process for the electrochemical synthesis of organic metal compounds 失效
    电化学合成有机金属化合物的方法

    公开(公告)号：US3964983A

    公开(公告)日：1976-06-22

    申请号：US403239

    申请日：1973-10-03

    Applicant: Wilhelm Eisenbach ,  Herbert Lehmkuhl ,  Gunther Wilke

    Inventor： Wilhelm Eisenbach ,  Herbert Lehmkuhl ,  Gunther Wilke

    IPC: C25B3/12 ,  C25B3/00 ,  B01K3/00

    CPC classification number: C25B3/12 ,  C25B3/00

    Abstract: Process for reacting an H-acidic organic compound, in which the acidic H-atom is bonded to the organic radical by an oxygen or a sulphur atom, e.g. an alcohol, with a metal having a standard potential which is more positive than -1.66 volts and which at most reacts with the H-acidic compound under current-free conditions, e.g. Ni, Co, Fe, Mn, Sb, Cu, or Au. The H-acidic compound or a solution thereof is a polar solvent is made conducting by addition of a soluble salt of chlorine, bromine or iodine, and is electrolysed at a temperature of up to 150.degree.C, using said metal as the anode, for production of the alcoholate.

    Abstract translation: 使酸性H原子通过氧或硫原子键合到有机基团上的H酸性有机化合物反应的方法，例如 醇，其具有比-1.66伏特更正的标准电位的金属，并且其在无电流条件下至多与H-酸性化合物反应，例如在无电流条件下。 Ni，Co，Fe，Mn，Sb，Cu或Au。 通过加入氯，溴或碘的可溶性盐使H酸性化合物或其溶液是极性溶剂进行导电，并使用所述金属作为阳极，在高达150℃的温度下电解，得到 生产醇酸盐。

    Process for catalytic dimerization of acrylic acid derivatives
    8.
    发明授权
    Process for catalytic dimerization of acrylic acid derivatives 失效
    丙烯酸衍生物的催化二聚方法

    公开(公告)号：US4594447A

    公开(公告)日：1986-06-10

    申请号：US657292

    申请日：1984-10-03

    Applicant: Gunther Wilke ,  Karin Sperling ,  Ludwig Stehling

    Inventor： Gunther Wilke ,  Karin Sperling ,  Ludwig Stehling

    IPC: B01J31/00 ,  B01J31/24 ,  C07B61/00 ,  C07C67/347 ,  C07C67/465 ,  C07C69/593 ,  C07C67/343

    CPC classification number: C07C67/347

    Abstract: The invention relates to a process for the dimerization of derivatives of acrylic acid in the homogeneous phase which process is characterized in that a compound having the general formula H.sub.2 C.dbd.CR.sup.1 -COOR.sup.2, wherein R.sup.1 represents H or a linear alkyl group having from 1 to 3 carbon atoms and R.sup.2 represents a linear alkyl group having from 1 to 3 carbon atoms, is reacted in a solvent at a temperature of from -50.degree. C. to +50.degree. C. in the presence of nickel compounds as catalysts which contain complex anions X in a molar ratio Ni:X=1:1 and organic or hydride ligands and are modifed with phosphanes having the general formula PR.sub.2 R', wherein R and R' may be same or different and represent alkyl residues having from 1 to 8 carbon atoms or phenyl residues, as well as the use of the dimers formed in the dimerization.

    Abstract translation: 本发明涉及在均相中使丙烯酸衍生物二聚的方法，该方法的特征在于具有通式H 2 C = CR 1 -COOR 2的化合物，其中R 1表示H或具有1至3个直链烷基 碳原子和R 2表示具有1至3个碳原子的直链烷基，在溶剂中在-50℃至+ 50℃的温度下在镍化合物作为催化剂存在下反应，所述催化剂含有复合阴离子 X与Ni：X = 1：1的摩尔比和有机或氢化物配体，并用具有通式PR2R'的磷烷改性，其中R和R'可以相同或不同，代表具有1至8个碳原子的烷基 或苯基残基，以及二聚体中形成的二聚体的用途。

    3-Methoxycyclooctadiene-(1,5)
    10.
    发明授权
    3-Methoxycyclooctadiene-(1,5) 失效
    3-甲氧基环辛二烯 - （1,5）

    公开(公告)号：US4076757A

    公开(公告)日：1978-02-28

    申请号：US737766

    申请日：1976-11-01

    Applicant: Gunther Wilke ,  Paul Heimbach

    Inventor： Gunther Wilke ,  Paul Heimbach

    IPC: C07C2/02 ,  C07C2/42 ,  C07C13/00 ,  C07C13/20 ,  C07C13/263 ,  C07C13/271 ,  C07C13/277 ,  C07C13/28 ,  C07C13/32 ,  C07C13/605 ,  C07C43/188 ,  C07C43/18

    CPC classification number: C07C43/188 ,  C07C13/00 ,  C07C13/20 ,  C07C13/263 ,  C07C13/271 ,  C07C13/277 ,  C07C13/28 ,  C07C13/32 ,  C07C13/605 ,  C07C2/02 ,  C07C2/42 ,  C07C2101/14 ,  C07C2101/16 ,  C07C2101/18 ,  C07C2101/20 ,  C07C2103/84

    Abstract: A series of mono, bi and tricarbocyclic compounds, most of which have olefinic unsaturation in the ring, which may or may not have substituents thereon. While the bi and tricyclic rings may be unsubstituted, these compounds which have olefinic unsaturation, particularly multiple olefinic unsaturation, are polymerizable and copolymerizable in known polymerization systems. They are particularly good crosslinking agents. These compounds are further useful in the sense that they can be cleaved oxidatively, to corresponding carboxylic acids, aldehydes and/or alcohols which have known utility in the plasticizer and detergent arts. The compounds which do not have olefinic unsaturation can also be oxidatively cleaved to produce oxygenated, e.g., acid, alcohol or aldehyde, compounds having known utility.

    Abstract translation: 一系列单环，双和三环化合物，其中大多数在环中具有烯属不饱和键，其可以具有或不具有取代基。 虽然双环和三环可以是未取代的，但是具有烯属不饱和键，特别是多个烯属不饱和键的这些化合物在已知的聚合体系中是可聚合的和可共聚的。 它们是特别好的交联剂。 这些化合物在它们可以被氧化裂解的意义上可进一步用于在增塑剂和洗涤剂领域已知有用的相应的羧酸，醛和/或醇。 不具有烯属不饱和键的化合物也可被氧化裂解以产生氧化的，例如酸，醇或醛，已知有用的化合物。

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