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    SYNTHESIS OF POLYESTERS WITH PRECISELY SEQUENCED TWO OR MORE STRUCTURAL UNITS
    7.
    发明申请
    SYNTHESIS OF POLYESTERS WITH PRECISELY SEQUENCED TWO OR MORE STRUCTURAL UNITS 有权
    精密连续两个或多个结构单元的聚酯的合成

    公开(公告)号：US20110190470A1

    公开(公告)日：2011-08-04

    申请号：US12993242

    申请日：2009-05-13

    申请人： Bin Huang

    发明人： Bin Huang

    IPC分类号： C07C69/63 ,  C08G63/682 ,  C08G63/78 ,  C07C67/465 ,  C08G63/90

    CPC分类号： C08G63/912 ,  C08G63/06 ,  C08G63/6822

    摘要： The present invention related to compositions and methods of producing polyesters with two and/or more different structural units and the materials of polyesters with structure sequence exactly specified therefore produced, and various articles produced from such exactly sequenced polyesters. More particularly, homogeneous copolymers with precisely defined sequences of various hydroxyl acids and their derivatives are produced according to the present invention.

    摘要翻译： 本发明涉及生产具有两个和/或更多个不同结构单元的聚酯的组合物和方法，并且由此制备具有精确规定结构顺序的聚酯的材料，以及由这些精确测序的聚酯制备的各种制品。 更具体地，根据本发明制备具有各种羟基酸及其衍生物的精确定义的序列的均相共聚物。

    Process for oligomerization of polyunsaturated acids and esters, products obtained and use thereof
    8.
    发明授权
    Process for oligomerization of polyunsaturated acids and esters, products obtained and use thereof 失效
    多不饱和酸和酯的低聚方法，获得的产品及其用途

    公开(公告)号：US5880298A

    公开(公告)日：1999-03-09

    申请号：US186483

    申请日：1994-01-14

    申请人： Gerard Hillion ,  Robert Stern ,  Odile Le Borgne

    发明人： Gerard Hillion ,  Robert Stern ,  Odile Le Borgne

    IPC分类号： C07C67/465 ,  C09F7/00 ,  C07B35/08

    CPC分类号： C07C67/465

    摘要： For the oligomerization of a fatty ester or fatty acid containing conjugated double bonds, the reaction uses a catalyst consisting of an activated earth, e.g., montmorillonite, at a temperature of from 100.degree.-180.degree. C., preferably from 130.degree.-160.degree. C. The process can be carried out continuously or in a batch process on a fixed bed and is particularly applicable to conjugated methyl esters obtained by conjugating and transesterifying sunflower seed oil. The oligomerized products obtained are particularly useful as lubricants or polycondensation reactants.

    摘要翻译： 对于含有共轭双键的脂肪酸酯或脂肪酸的低聚反应，使用由活化土如蒙脱石组成的催化剂，温度为100-180℃，优选130-160℃。 C.该方法可以在固定床上连续进行或以间歇方式进行，特别适用于通过将向日葵籽油接合和酯交换得到的共轭甲酯。 获得的低聚产物特别可用作润滑剂或缩聚反应物。

    Process for preparing Michael addition products
    9.
    发明授权
    Process for preparing Michael addition products 失效
    迈克尔加成产物的制备方法

    公开(公告)号：US5347043A

    公开(公告)日：1994-09-13

    申请号：US169261

    申请日：1993-12-20

    申请人： Mahmood Sabahi ,  Robert G. Irwin

    发明人： Mahmood Sabahi ,  Robert G. Irwin

    IPC分类号： C07C67/343 ,  C07C69/34 ,  C07C67/00 ,  C07C67/465 ,  C07C69/38

    CPC分类号： C07C67/343

    摘要： Dialkyl malonate/alkyl acrylate Michael addition product mixtures having at least three acceptor moieties in a substantial number of the molecules can be consistently prepared without the need for long reaction times or the use of a large excess of the acceptor when the reaction is effected by gradually adding one molar proportion of a dialkyl malonate to at least three molar proportions of an alkyl acrylate which has been preheated to 60.degree.-80.degree. C. in admixture with an initiator and a phase transfer catalyst. In a preferred embodiment, the preheated mixture is maintained at 60.degree.-80.degree. C. for at least one hour before the dialkyl malonate is added in order to increase the percentage of product composed of the heavier components.

    摘要翻译： 丙二酸二烷基酯/丙烯酸烷基酯在相当数量的分子中具有至少三个受体部分的迈克尔加成产物混合物可以一致地制备，而不需要长的反应时间或当反应通过逐渐地进行反应时使用大量过量的受体 将1摩尔比例的丙二酸二烷基酯加入到至少三摩尔比例的丙烯酸烷基酯中，该丙烯酸烷基酯与引发剂和相转移催化剂混合预热至60-80℃。 在优选的实施方案中，将预热的混合物在加入丙二酸二烷基酯之前保持在60-80℃至少1小时以增加由较重组分组成的产物的百分比。