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公开(公告)号：US07394091B2
公开(公告)日：2008-07-01
申请号：US10521233
申请日：2003-07-16
CPC分类号： H05B33/14 , C09K11/574 , C09K11/576 , C09K11/586 , C09K11/612 , C09K11/642 , C09K11/663 , C09K11/7421 , C09K11/7703 , C09K11/7718 , C09K11/7731 , C09K11/7761 , C09K11/7786 , Y10S977/824
摘要： There is provided composite nano-particles comprising nano-crystal particles dispersed stably and individually in suspension in high concentration without mutual aggregation of the nano-particles. A determined amount of pure water or deionized water is poured into a reactor, into which is introduced nitrogen gas at rate of 300 cm3/min for a given time while agitating with a stirrer to remove dissolved oxygen in the pure water, allowing to stand in an atmosphere of nitrogen. Next, the inside of the reactor is maintained in an atmosphere of nitrogen and sodium citrate as a dispersion-stabilizing agent, an aqueous solution of MPS as a surface-modifying agent, an anion aqueous solution for co-precipitation as a nano-crystal and a cation aqueous solution are added, in that order. Then, an aqueous solution of sodium silicate is added to the reactor, which is then allowed to stand in the dark place in an atmosphere of nitrogen after agitation. At that time, a vitrification-inhibiting agent may be added in order to inhibit the growth of glass layer.
摘要翻译： 提供了包含纳米晶体颗粒的复合纳米颗粒，其以高浓度稳定地和单独地分散悬浮而没有纳米颗粒的相互聚集。 将一定量的纯水或去离子水倒入反应器中，其中以300cm 3 / min的速率将氮气引入给定时间，同时用搅拌器搅拌以除去溶解氧 纯水，允许在氮气氛中站立。 接下来，将反应器内部保持在作为分散稳定剂的氮和柠檬酸钠的气氛中，作为表面改性剂的MPS的水溶液，作为纳米晶体共沉淀的阴离子水溶液和 依次加入阳离子水溶液。 然后，向反应器中加入硅酸钠水溶液，然后在搅拌后在氮气气氛中在黑暗的位置放置。 此时，为了抑制玻璃层的生长，可以添加玻璃化抑制剂。
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2.发明授权
公开(公告)号：US5998926A
公开(公告)日：1999-12-07
申请号：US012575
申请日：1998-01-23
IPC分类号： H01L51/50 , H01L51/52 , H05B33/10 , H05B33/12 , H05B33/22 , H05B33/26 , H01J1/62 , H05B33/00
CPC分类号： H05B33/26 , H01L27/3237 , H01L51/5221 , H05B33/10 , H05B33/12 , H01L2251/5315
摘要： A fixed pattern display device of the dynamic drive type with high definition including cathodes formed into a fine pattern by conventional photolithography. The cathodes are made of a metal material having a low resistance and arranged on an insulating substrate in the form of wiring patterns for fixed display segments of each of display patterns together with the display patterns. ITO which is resistant to water is exposed in the form of anodes each acting as a common electrode, resulting in arrangement of any protective film being eliminated.
摘要翻译： 具有高清晰度的动态驱动型的固定图案显示装置，其包括通过常规光刻形成为精细图案的阴极。 阴极由具有低电阻的金属材料制成，并且以与显示图案一起的每个显示图案的固定显示段的布线图案的形式布置在绝缘基板上。 耐水性的ITO以各自作为公共电极的阳极的形式暴露，导致排除任何保护膜的布置。
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公开(公告)号：US4985225A
公开(公告)日：1991-01-15
申请号：US273761
申请日：1988-08-22
IPC分类号： C01B21/072
CPC分类号： C01B21/0726 , C01P2004/62 , C01P2006/10 , C01P2006/32
摘要： A process for producing aluminum nitride powders is disclosed, which comprises mixing a water-soluble aluminum-containing compound or an aluminum alkoxide and a water-soluble carbon-containing compound and/or a water-soluble nitrogen-containing compound, with water; drying the mixture to obtain a solid; and calcining the solid in a nitrogen-containing non-oxidative atmosphere. According to the process of the invention, high-purity uniform aluminum nitride fine powders can be obtained rapidly and inexpensively.
摘要翻译： 公开了一种制备氮化铝粉末的方法，其包括将水溶性含铝化合物或烷氧基铝与水溶性含碳化合物和/或水溶性含氮化合物与水混合; 干燥混合物得到固体; 并将固体在含氮非氧化性气氛中煅烧。 根据本发明的方法，可以快速且廉价地获得高纯度均匀的氮化铝细粉。
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公开(公告)号：US4502032A
公开(公告)日：1985-02-26
申请号：US580637
申请日：1984-02-16
申请人： Minoru Kimura , Hisamitsu Takahashi
发明人： Minoru Kimura , Hisamitsu Takahashi
摘要： An ebullition cooled transformer has a housing, a core and coil assembly disposed on the lower portion of the housing to be immersed into a condensible electrically insulating refrigerant, a cooler unit located above the core and coil assembly within the housing, and a communicating tube disposed at the top of the housing to communicate with the outside air and provided with a porous filter permitting the air to permeate it but preventing a vapor of the refrigerant from permeating it.
摘要翻译： 沸腾冷却变压器具有壳体，芯体和线圈组件，其设置在壳体的下部以便浸入可冷凝的电绝缘制冷剂中;位于壳体内部的芯和线圈组件上方的冷却器单元和布置在其中的连通管 在壳体的顶部与外部空气连通并且设置有允许空气渗入其中但防止制冷剂的蒸气渗透的多孔过滤器。
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公开(公告)号：US07871712B2
公开(公告)日：2011-01-18
申请号：US11386367
申请日：2006-03-22
CPC分类号： C07F5/003 , C08G79/00 , C08L85/00 , H01L51/5259 , Y10S428/917 , Y10T428/239
摘要： A water-capturing or drying agent placed in a hermetically sealed field light emission device for maintaining stable light emission of the light emission device not susceptible to moisture and oxygen for long period of time. The drying agent comprises a compound of polymer formed by bonding M constituting a plurality of organometallic compounds wherein M is a trivalent metal atom with an oxygen molecule. The drying agent is placed in the hermetically sealed container, thereby protecting the field light emission device from being adversely affected by damage from trace amounts of moisture permeating from outside the hermetically sealed container and/or adhered to the inner surface thereof.
摘要翻译： 放置在气密密封的场致发射装置中的捕水或干燥剂，用于长时间保持对湿气和氧气不敏感的发光装置的稳定发光。 干燥剂包括通过将M构成多个有机金属化合物而形成的聚合物的化合物，其中M是三价金属原子与氧分子。 将干燥剂置于密封容器中，从而保护场发光装置免受来自密封容器外部渗透的痕量水分的损伤和/或附着于其内表面的不良影响。
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公开(公告)号：US20060234417A1
公开(公告)日：2006-10-19
申请号：US10521233
申请日：2003-07-16
IPC分类号： H01L51/40
CPC分类号： H05B33/14 , C09K11/574 , C09K11/576 , C09K11/586 , C09K11/612 , C09K11/642 , C09K11/663 , C09K11/7421 , C09K11/7703 , C09K11/7718 , C09K11/7731 , C09K11/7761 , C09K11/7786 , Y10S977/824
摘要： There is provided composite nano-particles comprising nano-crystal particles dispersed stably and individually in suspension in high concentration without mutual aggregation of the nano-particles. A determined amount of pure water or deionized water is poured into a reactor, into which is introduced nitrogen gas at rate of 300 cm3/min for a given time while agitating with a stirrer to remove dissolved oxygen in the pure water, allowing to stand in an atmosphere of nitrogen. Next, the inside of the reactor is maintained in an atmosphere of nitrogen and sodium citrate as a dispersion-stabilizing agent, an aqueous solution of MPS as a surface-modifying agent, an anion aqueous solution for co-precipitation as a nano-crystal and a cation aqueous solution are added, in that order. Then, an aqueous solution of sodium silicate is added to the reactor, which is then allowed to stand in the dark place in an atmosphere of nitrogen after agitation. At that time, a vitrification-inhibiting agent may be added in order to inhibit the growth of glass layer.
摘要翻译： 提供了包含纳米晶体颗粒的复合纳米颗粒，其以高浓度稳定地和单独地分散悬浮而没有纳米颗粒的相互聚集。 将一定量的纯水或去离子水倒入反应器中，其中以300cm 3 / min的速率将氮气引入给定时间，同时用搅拌器搅拌以除去溶解氧 纯水，允许在氮气氛中站立。 接下来，将反应器内部保持在作为分散稳定剂的氮和柠檬酸钠的气氛中，作为表面改性剂的MPS的水溶液，作为纳米晶体共沉淀的阴离子水溶液和 依次加入阳离子水溶液。 然后，向反应器中加入硅酸钠水溶液，然后在搅拌后在氮气气氛中在黑暗的位置放置。 此时，为了抑制玻璃层的生长，可以添加玻璃化抑制剂。
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公开(公告)号：US20050227114A1
公开(公告)日：2005-10-13
申请号：US11100936
申请日：2005-04-07
IPC分类号： H05B33/04 , B01J20/22 , C07F5/06 , C08F2/44 , C08F20/28 , C09K3/00 , H01L23/26 , H01L51/50 , H01L51/52 , H05B33/14
CPC分类号： H05B33/04 , B01J20/223 , H01L23/26 , H01L51/5246 , H01L51/5259 , H01L2924/0002 , H01L2924/12044 , Y10S428/917 , Y10T428/239 , H01L2924/00
摘要： A thin-profile organic EL device with a high degree of reliability is provided. The anode, the organic layer and the light transmissible-type cathode are laminated on the substrate and the inorganic water-barrier layer are laminated thereon, and then a UV rays-curable type water-capturing agent comprising a UV rays-curing agent and a water-absorbing agent is cured to bond to the sealing substrate instead of an adhesive layer. The UV rays-curing agent comprises an acrylic monomer, initiator and accelerator. The UV rays-curable type sealing agent is placed to the outer peripheral portion of the UV rays-curable type water-capturing agent to be cured. The emission of the organic layer is transmitted upward via the cathode, UV rays-curable type water-capturing agent and the sealing substrate. The UV rays-curable type water-capturing agent can be formed in a desired thickness and pattern by applying it and irradiating with UV-rays, thereby making it possible to produce a low-profile organic EL device in large quantities with a high degree of reliability and without damaging the organic layer which is not resistant to water.
摘要翻译： 提供了具有高度可靠性的薄型有机EL器件。 将阳极，有机层和透光性阴极层压在基板上，并且将无机阻隔层层叠在其上，然后将紫外线固化型水分捕捉剂包括紫外线固化剂和 固化吸水剂以粘合到密封基材上而不是粘合剂层。 UV射线固化剂包括丙烯酸单体，引发剂和促进剂。 紫外线固化型密封剂被放置在待固化的紫外线固化型捕集剂的外周部分。 有机层的发射通过阴极，紫外线固化型水捕获剂和密封基板向上传递。 紫外线固化型水分捕捉剂可以通过涂布和照射紫外线而形成所需的厚度和图案，从而可以大量生产低等级的有机EL器件 可靠性，不损坏不耐水的有机层。
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8.发明授权Water-scavenging agent for an organic electroluminescent device and organic electroluminescent device comprising same 失效用于有机电致发光器件的清水剂和包含该有机电致发光器件的有机电致发光器件公开(公告)号：US06896980B2
公开(公告)日：2005-05-24
申请号：US10659255
申请日：2003-09-11
IPC分类号： H05B33/04 , B01D53/28 , B01J20/22 , C02F5/10 , C07F13/00 , C07F15/06 , C09K11/06 , H01L51/50 , H05B33/00 , H05B33/14
CPC分类号： C07F15/065 , C07F13/005 , Y10S428/917 , Y10T428/239
摘要： A novel water-scavenging agent of the present invention comprising a compound of formula (I) as a primary component can be dissolved in a polar solvent and coated by a screen printing method, and the inventive organic EL device comprising same can maintain stable luminescent characteristics for a prolonged time: wherein, R1, R2, R3, R4, R5 and R6 are each independently hydrogen; halogen; alkyl, aryl, cycloalkyl or hetero-ring, optionally substituted with at least one halogen atom, and M is a metal having a coordination number of 6.
摘要翻译： 包含式（I）化合物作为主要成分的本发明的新型除水剂可以溶解在极性溶剂中并通过丝网印刷法涂布，并且包含其的本发明的有机EL器件可以保持稳定的发光特性 长时间：其中R 1，R 2，R 3，R 4，R SUB > 5和R 6各自独立地为氢; 卤素; 烷基，芳基，环烷基或杂环，任选被至少一个卤素原子取代，M是配位数为6的金属。
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公开(公告)号：US06887592B2
公开(公告)日：2005-05-03
申请号：US10382905
申请日：2003-03-07
CPC分类号： H01L51/5259 , H01L51/5036 , H01L51/524 , H01L2251/5315 , Y10S428/917 , Y10T428/23 , Y10T428/239
摘要： An organic EL device having a drying medium capable of suppressing the growth of a dark spot equipped with a water-capturing medium layer for chemically capturing water placed on a water-capturing medium holding layer. The organic EL device is comprised of a sealed container having a glass substrate and a sealing cap bonded to the glass substrate. The sealed container is provided with a light emitting region formed on the substrate which is formed of organic EL material layers placed between a pair of opposite anode and cathode electrodes. The sealed container further includes a water-capturing medium holding layer provided on an inner surface of the container spaced apart from the light emitting region and a water-capturing medium holding layer.
摘要翻译： 一种具有干燥介质的有机EL装置，其具有能够抑制配置有捕获介质层的暗点的生长，用于化学捕获放置在捕获介质保持层上的水。 有机EL器件由具有玻璃基板和与玻璃基板接合的密封盖的密封容器构成。 密封容器设置有形成在基板上的发光区域，该发光区域由放置在一对相对的阳极和阴极之间的有机EL材料层形成。 密封容器还包括设置在与发光区域间隔开的容器的内表面上的水捕捉介质保持层和水捕获介质保持层。
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公开(公告)号：US06790381B2
公开(公告)日：2004-09-14
申请号：US10288665
申请日：2002-11-05
IPC分类号： C09K300
CPC分类号： C07C69/72 , C07C31/28 , C07C31/32 , C07C39/235 , C07C53/126 , C07C69/732 , C07F5/003 , C07F5/069 , C07F7/003 , C07F7/025 , C07F7/045 , H01L23/26 , H01L51/5259 , H01L2924/0002 , H01L2924/12044 , H01L2924/00
摘要： An organic EL device is disclosed in which is placed a transparent water-capturing film comprising an easy-to-use organometallic compound illustrated by the chemical formula (1): wherein, R1, R2 and R3 are selected from the group consisting of alkyl group, aryl group, cycloalkyl group, heterocyclic group and acyl group having one carbon atom and above, and M is a trivalent metallic atom.
摘要翻译： 公开了一种有机EL器件，其中放置了由化学式（1）表示的易于使用的有机金属化合物的透明捕获膜：其中R1，R2和R3选自烷基 ，芳基，环烷基，杂环基和具有一个碳原子及以上的酰基，M是三价金属原子。
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