公开(公告)号：US09771632B2

公开(公告)日：2017-09-26

申请号：US13635132

申请日：2011-10-12

申请人： Joon-Soo Kim ,  Jin-Young Lee ,  Kyeong-Woo Chung ,  Hoo-In Lee

发明人： Joon-Soo Kim ,  Jin-Young Lee ,  Kyeong-Woo Chung ,  Hoo-In Lee

IPC分类号： C22B26/00 ,  C22B26/12 ,  B01D15/02 ,  C02F1/28 ,  C22B3/24

CPC分类号： C22B26/12 ,  B01D15/02 ,  C02F1/28 ,  C22B3/24 ,  Y02P10/234

摘要： The present disclosure provides a method for adsorption/desorption of lithium ions from brine, which employs a counter current decantation process in adsorption/desorption of lithium ions, thereby achieving an adsorption rate of 65±5% and a desorption rate of 95±3%. The method includes supplying brine into one of a plurality of adsorption reactors, adsorbing lithium ions to an adsorbent by supplying the adsorbent to the adsorption reactor to which the brine is supplied and forcing the brine and the adsorbent to sequentially flow backwards inside the respective adsorption reactors, and desorbing the lithium ions from the brine by forcing the adsorbent to which the lithium ions are adsorbed to sequentially flow backwards inside a plurality of desorption reactors. Here, the brine and the adsorbent are stirred by a stirrer to maintain the adsorbent in an intermediate state instead of settling or floating inside the respective adsorption reactors.

公开(公告)号：US20130001168A1

公开(公告)日：2013-01-03

申请号：US13635132

申请日：2011-10-12

申请人： Joon-Soo Kim ,  Jin-Young Lee ,  Kyeong-Woo Chung ,  Hoo-In Lee

发明人： Joon-Soo Kim ,  Jin-Young Lee ,  Kyeong-Woo Chung ,  Hoo-In Lee

IPC分类号： B01D15/08

CPC分类号： C22B26/12 ,  B01D15/02 ,  C02F1/28 ,  C22B3/24 ,  Y02P10/234

摘要： The present disclosure provides a method for adsorption/desorption of lithium ions from brine, which employs a counter current decantation process in adsorption/desorption of lithium ions, thereby achieving an adsorption rate of 65±5% and a desorption rate of 95±3%. The method includes supplying brine into one of a plurality of adsorption reactors, adsorbing lithium ions to an adsorbent by supplying the adsorbent to the adsorption reactor to which the brine is supplied and forcing the brine and the adsorbent to sequentially flow backwards inside the respective adsorption reactors, and desorbing the lithium ions from the brine by forcing the adsorbent to which the lithium ions are adsorbed to sequentially flow backwards inside a plurality of desorption reactors. Here, the brine and the adsorbent are stirred by a stirrer to maintain the adsorbent in an intermediate state instead of settling or floating inside the respective adsorption reactors.

摘要翻译： 本公开提供了一种从盐水中吸附/解吸锂离子的方法，其采用逆流倾析方法在锂离子的吸附/脱附中实现吸附率为65±5％，解吸率为95±3％ 。 该方法包括向多个吸附反应器中的一个提供盐水，通过将吸附剂供应到供应盐水的吸附反应器中，将锂离子吸附到吸附剂中，迫使盐水和吸附剂依次在相应的吸附反应器内向后流动 ，并且通过迫使吸附有锂离子的吸附剂在多个解吸反应器内顺序地向后流动，从盐水中解吸锂离子。 这里，通过搅拌器搅拌盐水和吸附剂，以使吸附剂保持在中间状态，而不是在相应的吸附反应器内沉降或漂浮。

公开(公告)号：US20110081283A1

公开(公告)日：2011-04-07

申请号：US12621456

申请日：2009-11-18

申请人： Young-Yoon Choi ,  Sang-Bae Kim ,  Byung-Su Kim ,  Hoo-In Lee

发明人： Young-Yoon Choi ,  Sang-Bae Kim ,  Byung-Su Kim ,  Hoo-In Lee

IPC分类号： C01G21/21 ,  C22B3/00 ,  C01G9/08 ,  C01G15/00

CPC分类号： C01G21/21 ,  C01G9/08 ,  C01G15/00 ,  C01G39/06 ,  C01P2006/80

摘要： A method of removing lead sulfide contained in refined molybdenite powder concentrates (major component; MoS2) is provided. More specifically, in order to solve the problems associated with a leaching method using a leaching agent that is employed for conventional hydrometallurgical process, oxygen-free inert gas is circulated in a furnace for pyrometallurgical treatment to evaporate lead sulfide at high temperature, followed by condensing process to recover lead sulfide at low temperature. The method is characterized in that, it can reduce environmental contamination and can easily recover sulfides of valuable metals such as lead, indium, zinc and the like.

摘要翻译： 提供了一种除去精炼的辉钼矿粉末浓缩物（主要组分; MoS2）中所含的硫化铅的方法。 更具体地，为了解决与使用用于常规湿法冶金工艺的浸出剂的浸出方法相关的问题，将无氧惰性气体在用于火法冶金处理的炉中循环以在高温下蒸发硫化铅，随后冷凝 在低温下回收硫化铅的工艺。 该方法的特征在于它可以减少环境污染，并且可以容易地回收有价值的金属如铅，铟，锌等的硫化物。

公开(公告)号：US06296817B1

公开(公告)日：2001-10-02

申请号：US09404987

申请日：1999-09-22

申请人： Hyung-Kyu Park ,  Hoo-In Lee ,  Eui-Pak Yoon

发明人： Hyung-Kyu Park ,  Hoo-In Lee ,  Eui-Pak Yoon

IPC分类号： C01F700

CPC分类号： C04B33/138 ,  C01F7/0693 ,  C04B18/023 ,  C04B28/06 ,  C04B33/1328 ,  C04B35/62204 ,  C04B35/6303 ,  C04B35/66 ,  Y02P20/142 ,  Y02P40/69 ,  Y02W30/94 ,  C04B18/14

摘要： Disclosed is the recycling of aluminum dross. Aluminum dross is crushed into particles which are size-classified on the basis of 1 mm. The aluminum dross particles equal to or smaller than 1 mm in size are leached with an aqueous sodium hydroxide solution to give a leachate which contains sodium aluminate as a result of the reaction the aluminum metal of the aluminum dross particles with sodium hydroxide. The aluminum dross particles greater than 1 mm in size are remelted to recover aluminum metal. In the leachate, a small quantity of aluminum hydroxide is seeded, followed by hydrolyzing the sodium aluminate to obtain aluminum hydroxide. Meanwhile, the leachate is filtered to obtain a residue. This residue is subjected to washing, drying and roasting. The mixing of the roasted residue with aggregate and alumina cement gives alumina castable refractories. It is economically very advantageous in that aluminum dross is reused as a raw material for aluminum hydroxide and for alumina castable refractories, instead of being discarded. Also, hydrogen gas can be obtained as a by-product in the process of recycling.

摘要翻译： 披露了铝渣的回收利用。 铝渣被粉碎成基于1mm的尺寸分级的颗粒。 使用氢氧化钠水溶液浸提等于或小于1mm的铝渣渣，由于铝渣与铝氢氧化物的反应而产生含有铝酸钠的浸出液。 大于1mm的铝渣渣被重熔以回收铝金属。 在渗滤液中，接种少量氢氧化铝，然后水解铝酸钠，得到氢氧化铝。 同时，将渗滤液过滤以获得残留物。 将该残余物进行洗涤，干燥和焙烧。 焙烧的残渣与骨料和氧化铝水泥的混合产生氧化铝可浇铸的耐火材料。 在经济上非常有利的是，铝渣被用作氢氧化铝和氧化铝可浇铸耐火材料的原料，而不是被丢弃。 此外，在回收过程中可以获得作为副产物的氢气。

公开(公告)号：US08163258B2

公开(公告)日：2012-04-24

申请号：US12621456

申请日：2009-11-18

申请人： Young-Yoon Choi ,  Sang-Bae Kim ,  Byung-Su Kim ,  Hoo-In Lee

发明人： Young-Yoon Choi ,  Sang-Bae Kim ,  Byung-Su Kim ,  Hoo-In Lee

IPC分类号： C22B1/00

CPC分类号： C01G21/21 ,  C01G9/08 ,  C01G15/00 ,  C01G39/06 ,  C01P2006/80

摘要： A method of removing lead sulfide contained in refined molybdenite powder concentrates (major component; MoS2) is provided. More specifically, in order to solve the problems associated with a leaching method using a leaching agent that is employed for conventional hydrometallurgical process, oxygen-free inert gas is circulated in a furnace for pyrometallurgical treatment to evaporate lead sulfide at high temperature, followed by condensing process to recover lead sulfide at low temperature. The method is characterized in that, it can reduce environmental contamination and can easily recover sulfides of valuable metals such as lead, indium, zinc and the like.

摘要翻译： 提供了一种除去精炼的辉钼矿粉末浓缩物（主要组分; MoS2）中所含的硫化铅的方法。 更具体地，为了解决与使用用于常规湿法冶金工艺的浸出剂的浸出方法相关的问题，将无氧惰性气体在用于火法冶金处理的炉中循环以在高温下蒸发硫化铅，随后冷凝 在低温下回收硫化铅的工艺。 该方法的特征在于它可以减少环境污染，并且可以容易地回收有价值的金属如铅，铟，锌等的硫化物。