公开(公告)号：US09187848B2

公开(公告)日：2015-11-17

申请号：US14003831

申请日：2012-03-08

Applicant: Ian Graveson

Inventor： Ian Graveson

IPC: D01F1/00 ,  D01F2/24 ,  D01D1/02 ,  D01D5/40 ,  D01F6/00 ,  D01F2/00 ,  D21H13/02 ,  D21H15/00

CPC classification number: D01F6/00 ,  D01D1/02 ,  D01D5/40 ,  D01F1/00 ,  D01F2/00 ,  D01F2/24 ,  D21H13/02 ,  D21H15/00

Abstract: The present invention is directed towards a method for spinning anionically modified cellulose comprising the steps of: (a) preparing a suspension of the anionically modified cellulose in a continuous phase; (b) subjecting the suspension to high shear rate; (c) performing spinning by extruding the cellulose suspension through a spinneret into a spinbath comprising a cationic complexing agent, and (d) isolating the sun fibers from the spin bath; as well as fibers obtained based on the method of the invention and paper or board products derived from such fibers.

Abstract translation: 本发明涉及一种纺丝阴离子改性纤维素的方法，包括以下步骤：（a）制备连续相中阴离子改性纤维素的悬浮液; （b）使悬浮液经受高剪切速率; （c）通过将纤维素悬浮液通过喷丝头挤出进入包含阳离子络合剂的纺丝饼中进行纺丝，和（d）从旋转浴中分离太阳纤维; 以及基于本发明的方法获得的纤维以及衍生自这种纤维的纸或纸制品。

公开(公告)号：US20140041821A1

公开(公告)日：2014-02-13

申请号：US14003850

申请日：2012-03-08

Applicant: Ian Graveson ,  Philip Turner

Inventor： Ian Graveson ,  Philip Turner

IPC: D21C9/00

CPC classification number: D21C9/00 ,  D01D1/02 ,  D01D5/40 ,  D01F2/00 ,  D01F2/24 ,  D21H13/02 ,  D21H15/00

Abstract: The present invention is directed towards a method for spinning neutral or anionically modified cellulose comprising the steps of: (a) preparing a suspension of the neutral or anionically modified cellulose in a continuous phase; (b) subjecting the suspension to high shear rate; (c) performing spinning by extruding the cellulose suspension into an airgap region comprising at least one heated zone to obtain spun fibres, (d) subjecting the spun fibres to at least one washing stages and (e) isolating the spun fibres from the at least one washing stages; as well as fibres obtained based on the method of the invention and paper or board products derived from such fibres.

Abstract translation: 本发明涉及一种纺制中性或阴离子改性纤维素的方法，包括以下步骤：（a）制备连续相中的中性或阴离子改性纤维素的悬浮液; （b）使悬浮液经受高剪切速率; （c）通过将纤维素悬浮液挤出到包括至少一个加热区域的气隙区域中进行纺丝，以获得纺丝纤维，（d）使纺丝纤维经受至少一个洗涤阶段，和（e）至少从至少一个 一个洗涤阶段; 以及基于本发明的方法获得的纤维以及衍生自这种纤维的纸或纸制品。

公开(公告)号：US6110978A

公开(公告)日：2000-08-29

申请号：US43320

申请日：1998-06-10

Applicant: Ian Graveson ,  Kevin Philip ,  George Russell Ross ,  David Stephen Towlson

Inventor： Ian Graveson ,  Kevin Philip ,  George Russell Ross ,  David Stephen Towlson

IPC: B01F3/12 ,  B01F5/00 ,  B01F17/00 ,  D01F2/00 ,  D06M13/02 ,  D06M13/322 ,  D06M13/358 ,  D06M15/03 ,  D06M15/09 ,  D06M15/15 ,  D06M15/263 ,  D06M15/285 ,  D06M15/333 ,  D06M23/08 ,  C08L1/26 ,  D06M9/00

CPC classification number: D01F2/00 ,  B01F17/0014 ,  B01F3/1207 ,  D06M13/358 ,  D06M15/03 ,  D06M15/09 ,  D06M15/15 ,  D06M15/263 ,  D06M15/285 ,  D06M15/333 ,  D06M23/08

Abstract: A method of forming a solution of a solid includes the steps of: (1) forming a dispersion which comprises (a) a liquid, (b) the solid dispersed in powder form and (c) a polymeric binder dissolved in the liquid, and (2) mixing the dispersion with the solvent under conditions such that the powder dissolves in the solvent. If a solution prepared by this method is allowed to dry out, the polymeric binder binds the powder and thus suppresses dust formation. The method has particular application to solids which are reactive textile auxiliaries. A dispersion of a solid in powder form in an aqueous liquid contains a major proportion of a low viscosity, water-soluble cellulose ether and a minor proportion of a natural polysaccharide gum.

Abstract translation: PCT No.PCT / GB96 / 02285第 371日期：1998年6月10日 102（e）1998年6月10日PCT PCT 1996年9月18日PCT公布。 出版物WO97 / 10894 日本1997年3月27日一种形成固体溶液的方法包括以下步骤：（1）形成分散体，其包含（a）液体，（b）以粉末形式分散的固体，和（c）溶解的聚合物粘合剂 在液体中，和（2）使分散体与溶剂在使粉末溶解在溶剂中的条件下混合。 如果通过该方法制备的溶液被干燥，则聚合物粘合剂结合粉末，从而抑制粉尘形成。 该方法特别适用于作为反应性纺织助剂的固体。 粉末形式的固体在水性液体中的分散体含有主要比例的低粘度水溶性纤维素醚和少部分天然多糖胶。

公开(公告)号：US6042769A

公开(公告)日：2000-03-28

申请号：US750304

申请日：1996-12-04

Applicant: James Martin Gannon ,  Ian Graveson ,  Pamela Ann Johnson ,  Calvin Roger Woodings

Inventor： James Martin Gannon ,  Ian Graveson ,  Pamela Ann Johnson ,  Calvin Roger Woodings

IPC: D06M11/00 ,  D01F2/00 ,  D01F2/02 ,  D04H1/42 ,  D04H1/4266 ,  D04H1/44 ,  D04H1/492 ,  D06M11/30 ,  D06M101/06 ,  D21H13/02 ,  D21H13/08 ,  D01F4/00

CPC classification number: D04H1/492 ,  D01F2/00 ,  D04H1/42 ,  D04H1/4266 ,  D21H13/08

Abstract: The fibrillation tendency of solvent-spun fiber can be increased by subjecting the fiber to a treatment which reduces its degree of polymerisation by about 200 units or more. Suitable methods of treatment include severe bleaching, for example application of an aqueous liquor containing 0.1 to 10 percent by weight sodium hypochlorite (as available chlorine) to the fiber followed by steaming. Fiber may be treated in never-dried or previously-dried form. Fiber treated by the process of the invention is useful for example in the manufacture of paper and hydroentangled fabrics. Fiber of increased tendency to fibrillation can be beaten to a Canadian Standard Freeness 400 in the Disintegration Test by 30,000-150,000 disintegrator revolutions and to a Canadian Standard Freeness 200 in the same Test by 50,000-200,000 disintegrator revolutions.

Abstract translation: PCT No.PCT / GB95 / 01439 Sec。 371日期1996年12月4日第 102（e）日期1996年12月4日PCT Filed 1995年6月19日PCT公布。 第WO95 / 35399号公报 日期1995年12月28日溶剂纺纤维的原纤化倾向可以通过使纤维进行将聚合度降低约200单位或更多的处理来提高。 合适的处理方法包括严格漂白，例如将含有0.1-10重量％次氯酸钠（作为可用的氯）的含水液体施加到纤维上，然后蒸汽。 纤维可以以未干燥或预先干燥的形式进行处理。 通过本发明的方法处理的纤维例如在纸和水刺织物的制造中是有用的。 增加纤维化趋势的纤维可以在崩解试验中以30,000-150,000次崩解剂转速和加拿大标准游离度200在相同试验中以50,000-200,000次崩解器转速殴打加拿大标准游离度400。

公开(公告)号：US5725821A

公开(公告)日：1998-03-10

申请号：US750305

申请日：1996-12-04

Applicant: James Martin Gannon ,  Ian Graveson ,  Simon Ashley Mortimer

Inventor： James Martin Gannon ,  Ian Graveson ,  Simon Ashley Mortimer

IPC: D01F2/00 ,  D04H1/42 ,  D04H1/46 ,  D21H13/08 ,  D01D10/06 ,  D01F2/02

CPC classification number: D01F2/00

Abstract: A process of manufacturing lyocell fiber with an increased tendency to fibrillation which includes dissolving cellulose in a tertiary amine N-oxide solvent to form a solution. The degree of polymerization of the cellulose is not more than about 450 and the concentration of cellulose in the solution is at least 16 percent by weight. The solution is extruded through a die to form a plurality of filaments which are washed to remove the solvent, thereby forming the lyocell fiber which is then dried.

Abstract translation: PCT No.PCT / GB95 / 01440 Sec。 371日期1996年12月4日第 102（e）日期1996年12月4日PCT Filed 1995年6月19日PCT公布。 WO95 / 35400 PCT出版物 日期1995年12月28日制造具有增加的纤维颤动趋势的莱赛尔纤维的方法，其包括将纤维素溶解在叔胺N-氧化物溶剂中以形成溶液。 纤维素的聚合度不超过约450，并且溶液中纤维素的浓度至少为16重量％。 将溶液通过模具挤出以形成多个细丝，其被洗涤以除去溶剂，从而形成干燥后的溶胞酶纤维。

公开(公告)号：US09103069B2

公开(公告)日：2015-08-11

申请号：US14003850

申请日：2012-03-08

Applicant: Ian Graveson ,  Philip Turner

Inventor： Ian Graveson ,  Philip Turner

IPC: D21C9/00 ,  D01D1/02 ,  D01D5/40 ,  D01F2/00 ,  D01F2/24 ,  D21H13/02 ,  D21H15/00

CPC classification number: D21C9/00 ,  D01D1/02 ,  D01D5/40 ,  D01F2/00 ,  D01F2/24 ,  D21H13/02 ,  D21H15/00

Abstract: The present invention is directed towards a method for spinning neutral or anionically modified cellulose comprising the steps of: (a) preparing a suspension of the neutral or anionically modified cellulose in a continuous phase; (b) subjecting the suspension to high shear rate; (c) performing spinning by extruding the cellulose suspension into an airgap region comprising at least one heated zone to obtain spun fibers, (d) subjecting the spun fibers to at least one washing stages and (e) isolating the spun fibers from the at least one washing stages; as well as fibers obtained based on the method of the invention and paper or board products derived from such fibers.

Abstract translation: 本发明涉及一种纺制中性或阴离子改性纤维素的方法，包括以下步骤：（a）制备连续相中的中性或阴离子改性纤维素的悬浮液; （b）使悬浮液经受高剪切速率; （c）通过将纤维素悬浮液挤出到包括至少一个加热区域的气隙区域中进行纺丝，以获得纺丝纤维，（d）使纺丝纤维经受至少一个洗涤阶段，和（e）至少从至少一个 一个洗涤阶段; 以及基于本发明的方法获得的纤维以及衍生自这种纤维的纸或纸制品。

公开(公告)号：US20140053995A1

公开(公告)日：2014-02-27

申请号：US14003831

申请日：2012-03-08

Applicant: Ian Graveson

Inventor： Ian Graveson

IPC: D01F6/00 ,  D01F1/00

CPC classification number: D01F6/00 ,  D01D1/02 ,  D01D5/40 ,  D01F1/00 ,  D01F2/00 ,  D01F2/24 ,  D21H13/02 ,  D21H15/00

Abstract: The present invention is directed towards a method for spinning anionically modified cellulose comprising the steps of: (a) preparing a suspension of the anionically modified cellulose in a continuous phase; (b) subjecting the suspension to high shear rate; (c) performing spinning by extruding the cellulose suspension through a spinneret into a spinbath comprising a cationic complexing agent, and (d) isolating the sun fibres from the spin bath; as well as fibres obtained based on the method of the invention and paper or board products derived from such fibres.

Abstract translation: 本发明涉及一种纺丝阴离子改性纤维素的方法，包括以下步骤：（a）制备连续相中阴离子改性纤维素的悬浮液; （b）使悬浮液经受高剪切速率; （c）通过将纤维素悬浮液通过喷丝头挤出到包含阳离子络合剂的纺丝饼中进行纺丝，和（d）从旋转浴中分离太阳纤维; 以及基于本发明的方法获得的纤维以及衍生自这种纤维的纸或纸制品。

公开(公告)号：US07267744B2

公开(公告)日：2007-09-11

申请号：US10471845

申请日：2002-03-14

Applicant: Ian Graveson ,  Heinzhorst Mobius ,  Derek Andrew Weightman

Inventor： Ian Graveson ,  Heinzhorst Mobius ,  Derek Andrew Weightman

IPC: C09B9/00 ,  D21C9/00

CPC classification number: D21C9/007 ,  C08B1/00 ,  C08B9/00

Abstract: This invention provides a process for treating chemical woodpulp, or chemical cellulose including cotton linter, including the step of applying an electron processing technology (EPT) step to chemical woodpulp, or chemical cellulose, as the case may be, on an in-line basis to provide control of pulp viscosity or degree of polymerization (DP). The invention also provides a method of process control in treating the aforementioned woodpulp or cellulose, including the step of using radiation dose-viscosity relationship curve for applying an EPT step on an in-line basis. The in-line EPT step may, in one form of the invention, replace and hence eliminate a chemical DP reduction step.

Abstract translation: 本发明提供了一种用于处理化学木浆或包括棉绒的化学纤维素的方法，包括以下步骤：将化学木浆或化学纤维素（视情况而定）按照在线基础施加电子加工技术（EPT）步骤 以提供纸浆粘度或聚合度（DP）的控制。 本发明还提供了一种处理上述木浆或纤维素的方法控制方法，其中包括使用辐射剂量 - 粘度关系曲线以串联方式施加EPT步骤的步骤。 在本发明的一种形式中，在线EPT步骤可以替代并因此消除化学DP还原步骤。

公开(公告)号：US5690874A

公开(公告)日：1997-11-25

申请号：US549742

申请日：1995-11-07

Applicant: Kathryn Diana Bell ,  Ian Graveson ,  Timothy John Ollerenshaw

Inventor： Kathryn Diana Bell ,  Ian Graveson ,  Timothy John Ollerenshaw

IPC: D01F1/07 ,  D01F2/00 ,  D01F11/02 ,  D06M13/02 ,  D06M13/244 ,  D06M13/282 ,  D06M13/285 ,  D06M15/431 ,  D06M101/00 ,  D06M101/02 ,  D06M101/06

CPC classification number: D01F2/00 ,  D01F11/02 ,  D06M13/285 ,  D06M15/431 ,  D06M2101/04

Abstract: A method of forming a flame retardant cellulose fiber is disclosed which comprises the steps of producing lyocell fiber and incorporating a flame retardant chemical into the fiber while the fiber is in the never-dried condition prior to first drying.

Abstract translation: PCT No.PCT / GB94 / 00956 Sec。 371日期：1995年11月7日 102（e）日期1995年11月7日PCT 1994年5月4日PCT公布。 第WO94 / 26962号公报 日期：1994年11月24日公开了一种形成阻燃纤维素纤维的方法，其包括以下步骤：在第一次干燥之前纤维处于未干燥状态时，生产莱赛尔纤维并将阻燃化学品并入纤维中。