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公开(公告)号：US06926868B2
公开(公告)日：2005-08-09
申请号：US09992590
申请日：2001-11-06
IPC分类号： B01D3/06 , B01J8/00 , B01J8/20 , B01J8/38 , B01J19/00 , B01J19/18 , B01J19/24 , C08F2/00 , C08F6/00 , C08F10/00 , C08F210/16 , B01J8/08
CPC分类号： B01D3/06 , B01J8/003 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/0053 , B01J19/1837 , B01J2208/0007 , B01J2208/00539 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00033 , B01J2219/00103 , B01J2219/00114 , B01J2219/00162 , B01J2219/00164 , B01J2219/00191 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00236 , B01J2219/0024 , C08F2/00 , C08F6/003 , C08F10/00 , C08F210/16 , C08F2/14 , C08F210/14
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent of a slurry loop reactor containing a flow of slurry therein, comprising a discharge conduit extending a distance into the loop reactor; the conduit having a longitudinal axis and an opening inside the loop reactor; at least a portion of the conduit being curved along its longitudinal axis inside the loop reactor; and the opening substantially facing the flow of the slurry, wherein the discharge conduit is located within a lower leg of the loop reactor such that a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank wherein volatile inert diluent and unreacted monomers are removed and the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
摘要翻译： 公开了一种用于连续分离包含稀释剂和未反应单体的液体介质的流体/设备，所述液体介质包含其中含有浆料流的淤浆环流反应器的聚合流出物，所述淤浆环流反应器包括延伸一段距离进入环管反应器的排放管道; 导管具有纵向轴线和环形反应器内部的开口; 导管的至少一部分沿其纵向轴线在环形反应器内弯曲; 并且所述开口基本上面向所述浆料的流动，其中所述排出导管位于所述环管反应器的小腿内，使得将来自浆料反应器的聚合流出物通过排出阀和输送管道连续排放到第一中间压力 闪蒸罐，其中挥发性惰性稀释剂和未反应单体被除去，而在将约50至100％的惰性稀释剂从其中移除到第二闪蒸罐中的较低压力下保留的聚合物固体。
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公开(公告)号：US06800698B2
公开(公告)日：2004-10-05
申请号：US10260011
申请日：2003-03-11
IPC分类号： C08F200
CPC分类号： B01D3/06 , B01J8/003 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/20 , B01J8/382 , B01J19/0053 , B01J19/1837 , B01J2208/0007 , B01J2208/00539 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00033 , B01J2219/00103 , B01J2219/00114 , B01J2219/00162 , B01J2219/00164 , B01J2219/00191 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00236 , B01J2219/0024 , C08F2/00 , C08F6/003 , C08F10/00 , C08F210/16 , C08F2/14 , C08F210/14
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent comprising diluent, unreacted monomers and polymer solids, comprising a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank with a conical bottom defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the slurry/polymer solids and an exit seal chamber of such diameter (d) and length (l) as to maintain a desired volume of concentrated polymer solids/slurry in the exit seal chamber such as to form a pressure seal while continuously discharging a plug flow of concentrated polymer solids/slurry bottom product of the first flash tank from the exit seal chamber through a seal chamber exit reducer with inclined sides defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
摘要翻译： 公开了一种用于从包含稀释剂，未反应单体和聚合物固体的聚合流出物连续分离包含稀释剂和未反应单体的液体介质的方法/装置，其包括通过排放阀将淤浆反应器的聚合流出物连续排出并将传输导管 具有锥形底部的第一中间压力闪蒸罐，该锥形底部由基本上直的侧面倾斜的水平面倾斜，该水平面等于或大于浆料/聚合物固体的滑动角度以及直径（d）的出口密封室， 长度（l）以在出口密封室中保持所需体积的浓缩聚合物固体/浆料，以形成压力密封，同时连续地将第一闪蒸罐的浓缩聚合物固体/浆料底部产物的塞流从出口 密封室通过密封室出口减速器，斜面大致直线形成 以等于或大于在较低压力下将约50至100％的惰性稀释剂从其中除去至第二闪蒸罐后残留的聚合物固体的滑动角度等于或大于水平的角度。
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公开(公告)号：US07575724B2
公开(公告)日：2009-08-18
申请号：US11832156
申请日：2007-08-01
CPC分类号： B01J8/003 , B01D3/06 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/0053 , B01J19/1837 , B01J2208/0007 , B01J2208/00539 , B01J2208/00548 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00033 , B01J2219/00103 , B01J2219/00114 , B01J2219/00162 , B01J2219/00164 , B01J2219/00191 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00236 , B01J2219/0024 , C08F2/00 , C08F6/003 , C08F10/00 , C08F210/16 , Y10S526/943 , Y10T29/49345 , Y10T29/49826 , Y10T29/53 , C08F2/01 , C08F2/14 , C08F210/14
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent comprising diluent, unreacted monomers and polymer solids, comprising a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank with a conical bottom defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the slurry/polymer solids and an exit seal chamber of such diameter (d) and length (l) as to maintain a desired volume of concentrated polymer solids/slurry in the exit seal chamber such as to form a pressure seal while continuously discharging a plug flow of concentrated polymer solids/slurry bottom product of the first flash tank from the exit seal chamber through a seal chamber exit reducer with inclined sides defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
摘要翻译： 公开了一种用于从包含稀释剂，未反应单体和聚合物固体的聚合流出物连续分离包含稀释剂和未反应单体的液体介质的方法/装置，其包括通过排放阀将淤浆反应器的聚合流出物连续排出并将传输导管 具有锥形底部的第一中间压力闪蒸罐，该锥形底部由基本上直的侧面倾斜的水平面倾斜，该水平面等于或大于浆料/聚合物固体的滑动角度以及直径（d）的出口密封室， 长度（l）以在出口密封室中保持所需体积的浓缩聚合物固体/浆料，以形成压力密封，同时连续地将第一闪蒸罐的浓缩聚合物固体/浆料底部产物的塞流从出口 密封室通过密封室出口减速器，斜面大致直线形成 以等于或大于在较低压力下将约50至100％的惰性稀释剂从其中除去至第二闪蒸罐后残留的聚合物固体的滑动角度等于或大于水平的角度。
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公开(公告)号：US06380325B1
公开(公告)日：2002-04-30
申请号：US09654799
申请日：2000-09-05
IPC分类号： C08F606
CPC分类号： B01D3/06 , B01J8/003 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/1837 , B01J2208/00539 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00103 , B01J2219/00114 , C08F6/003
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent comprising diluent, unreacted monomers and polymer solids, comprising a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank with a conical bottom defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the slurry/polymer solids and an exit seal chamber of such diameter (d) and length (l) as to maintain a desired volume of concentrated polymer solids/slurry in the exit seal chamber such as to form a pressure seal while continuously discharging a plug flow of concentrated polymer solids/slurry bottom product of said first flash tank from the exit seal chamber through a seal chamber exit reducer with inclined sides defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
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公开(公告)号：US06281300B1
公开(公告)日：2001-08-28
申请号：US09081392
申请日：1998-05-18
IPC分类号： C08F612
CPC分类号： B01D3/06 , B01J8/003 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/1837 , B01J2208/00539 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00103 , B01J2219/00114 , C08F6/003
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent comprising diluent, unreacted monomers and polymer solids, comprising a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank with a conical bottom defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the slurry/polymer solids and an exit seal chamber of such diameter (d) and length (l) as to maintain a desired volume of concentrated polymer solids/slurry in the exit seal chamber such as to form a pressure seal while continuously discharging a plug flow of concentrated polymer solids/slurry bottom product of said first flash tank from the exit seal chamber through a seal chamber exit reducer with inclined sides defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
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公开(公告)号：US07381777B1
公开(公告)日：2008-06-03
申请号：US11711453
申请日：2007-02-26
CPC分类号： C08F10/02 , C08F210/16 , C08F2400/02 , C08F2/40 , C08F2/005 , C08F2/14 , C08F210/14 , C08F2500/12
摘要： The present invention relates to methods for controlling fouling in the reaction zone of slurry-type olefin polymerization reactors by measuring a process operating parameter and by responding to said process operating parameter, e.g., by introducing a gaseous poison for the polymerization catalyst in response to a comparison between said measured parameter and a fouling parameter limit for said measured parameter.
摘要翻译： 本发明涉及通过测量工艺操作参数和响应所述工艺操作参数来控制浆料型烯烃聚合反应器的反应区域中的结垢的方法，例如通过引入用于聚合催化剂的气体毒物以响应于 所述测量参数与所述测量参数的污垢参数极限之间的比较。
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公开(公告)号：US06833415B2
公开(公告)日：2004-12-21
申请号：US10079226
申请日：2002-02-19
IPC分类号： C08F200
CPC分类号： B01D3/06 , B01J8/003 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/0053 , B01J19/1837 , B01J2208/0007 , B01J2208/00539 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00033 , B01J2219/00103 , B01J2219/00114 , B01J2219/00162 , B01J2219/00164 , B01J2219/00191 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00236 , B01J2219/0024 , C08F2/00 , C08F6/003 , C08F10/00 , C08F210/16 , C08F2/14 , C08F210/14
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent comprising diluent, unreacted monomers and polymer solids, comprising a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank with a conical bottom defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the slurry/polymer solids and an exit seal chamber of such diameter (d) and length (l) as to maintain a desired volume of concentrated polymer solids/slurry in the exit seal chamber such as to form a pressure seal while continuously discharging a plug flow of concentrated polymer solids/slurry bottom product of the first flash tank from the exit seal chamber through a seal chamber exit reducer with inclined sides defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
摘要翻译： 公开了一种用于从包含稀释剂，未反应单体和聚合物固体的聚合流出物连续分离包含稀释剂和未反应单体的液体介质的方法/装置，其包括通过排放阀将淤浆反应器的聚合流出物连续排出并将传输导管 具有锥形底部的第一中间压力闪蒸罐，该锥形底部由基本上直的侧面倾斜的水平面倾斜，该水平面等于或大于浆料/聚合物固体的滑动角度以及直径（d）的出口密封室， 长度（l）以在出口密封室中保持所需体积的浓缩聚合物固体/浆料，以形成压力密封，同时连续地将第一闪蒸罐的浓缩聚合物固体/浆料底部产物的塞流从出口 密封室通过密封室出口减速器，斜面大致直线形成 以等于或大于在较低压力下将约50至100％的惰性稀释剂从其中除去至第二闪蒸罐后残留的聚合物固体的滑动角度等于或大于水平的角度。
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公开(公告)号：US07268194B2
公开(公告)日：2007-09-11
申请号：US10085809
申请日：2002-02-28
CPC分类号： B01J8/003 , B01D3/06 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/0053 , B01J19/1837 , B01J2208/0007 , B01J2208/00539 , B01J2208/00548 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00033 , B01J2219/00103 , B01J2219/00114 , B01J2219/00162 , B01J2219/00164 , B01J2219/00191 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00236 , B01J2219/0024 , C08F2/00 , C08F6/003 , C08F10/00 , C08F210/16 , Y10S526/943 , Y10T29/49345 , Y10T29/49826 , Y10T29/53 , C08F2/01 , C08F2/14 , C08F210/14
摘要： A process of converting a loop reactor into multiple loop reactors comprising starting with a loop reactor comprising at least 8 vertical legs, at least two non-vertical conversion runs, each non-vertical run connected in fluid flow communication with two vertical legs; at least two feed inlets; and at least two continuous discharge conduits; disconnecting at least one connection of each conversion run; and reconnecting each conversion run in fluid flow communication with a different vertical leg in such a manner to form multiple loop reactors each having at least one feed inlet and at least one continuous discharge conduit.
摘要翻译： 将环管反应器转化为多个环流反应器的方法，包括从包括至少8个垂直支管的环流反应器开始，至少两个非垂直转换运行，每个非垂直运行与两个垂直支路流体连通地连接; 至少两个进料口; 和至少两个连续排出管道; 断开每个转换运行的至少一个连接; 并且以这样的方式将流体流动连通中的每个转换运行重新连接成形成多个环路反应器，每个回路反应器具有至少一个进料入口和至少一个连续的排出管道。
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公开(公告)号：US07034090B2
公开(公告)日：2006-04-25
申请号：US10023677
申请日：2002-02-14
IPC分类号： C08F2/00
CPC分类号： B01D3/06 , B01J8/003 , B01J8/005 , B01J8/0055 , B01J8/007 , B01J8/382 , B01J19/1837 , B01J2208/00539 , B01J2208/00761 , B01J2208/00769 , B01J2208/00867 , B01J2219/00006 , B01J2219/00103 , B01J2219/00114 , C08F6/003
摘要： A process/apparatus is disclosed for continuously separating a liquid medium comprising diluent and unreacted monomers from a polymerization effluent comprising diluent, unreacted monomers and polymer solids, comprising a continuous discharge of the polymerization effluent from a slurry reactor through a discharge valve and transfer conduit into a first intermediate pressure flash tank with a conical bottom defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the slurry/polymer solids and an exit seal chamber of such diameter (d) and length (l) as to maintain a desired volume of concentrated polymer solids/slurry in the exit seal chamber such as to form a pressure seal while continuously discharging a plug flow of concentrated polymer solids/slurry bottom product of said first flash tank from the exit seal chamber through a seal chamber exit reducer with inclined sides defined by substantially straight sides inclined at an angle to that of horizontal equal to or greater than the angle of slide of the polymer solids which remain after removal of about 50 to 100% of the inert diluent therefrom to a second flash tank at a lower pressure.
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