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    Non-aqueous electrolyte solution and non-aqueous electrolyte solution secondary battery using the same
    1.
    发明授权
    Non-aqueous electrolyte solution and non-aqueous electrolyte solution secondary battery using the same 有权
    非水电解液和非水电解液二次电池使用相同

    公开(公告)号：US07144660B2

    公开(公告)日：2006-12-05

    申请号：US10397320

    申请日：2003-03-27

    Applicant: Kunihisa Shima ,  Kenji Shizuka ,  Makoto Ue

    Inventor： Kunihisa Shima ,  Kenji Shizuka ,  Makoto Ue

    IPC: H01M10/40

    CPC classification number: H01M10/0567 ,  H01M4/525 ,  H01M4/587 ,  H01M10/0525 ,  H01M10/0587 ,  H01M10/4235 ,  H01M10/446 ,  H01M2004/021 ,  H01M2300/0037

    Abstract: A non-aqueous electrolyte solution that contains an organic solvent, and a lithium salt and an electrolyte, that is useful for the preparation of a secondary battery that is equipped with a negative electrode and a positive electrode, each of which is capable of storing and releasing lithium, wherein the non-aqueous electrolyte solution contains partially hydrogenated terphenyl that is a mixture of two or more compounds of which one is diphenylcyclohexane that is present in an amount ranging from 10 to 65 wt % of the partially hydrogenated terphenyl and the partially hydrogenated terphenyl has a solubility of not less than 0.5 wt % in the electrolyte solution at room temperature.

    Abstract translation: 含有有机溶剂的非水电解质溶液，以及锂盐和电解质，其可用于制备具有负极和正极的二次电池，每个二次电池能够储存和 释放锂，其中所述非水电解质溶液包含部分氢化的三联苯，其是两种或更多种其中一种是二苯基环己烷的化合物的混合物，其以部分氢化的三联苯的10至65重量％的量存在，并且部分氢化 三联苯在室温下在电解液中的溶解度不小于0.5重量％。

    Layered lithium-nickel-based compound oxide powder and its production process
    2.
    发明申请
    Layered lithium-nickel-based compound oxide powder and its production process 有权
    分层锂镍复合氧化物粉及其制作工艺

    公开(公告)号：US20050158546A1

    公开(公告)日：2005-07-21

    申请号：US11032113

    申请日：2005-01-11

    Applicant: Kenji Shizuka

    Inventor： Kenji Shizuka

    IPC: C01G53/00 ,  H01M4/02 ,  H01M4/04 ,  H01M4/131 ,  H01M4/50 ,  H01M4/505 ,  H01M4/52 ,  H01M4/525 ,  H01M4/58 ,  H01M4/587 ,  H01M10/0525 ,  H01M10/0568 ,  H01M10/36

    CPC classification number: C01G45/1228 ,  C01G51/50 ,  C01G53/50 ,  C01P2002/22 ,  C01P2002/52 ,  C01P2002/54 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/22 ,  C01P2006/40 ,  H01M4/0404 ,  H01M4/0419 ,  H01M4/0471 ,  H01M4/131 ,  H01M4/505 ,  H01M4/525 ,  H01M4/587 ,  H01M10/0525 ,  H01M10/0568 ,  H01M2004/028 ,  Y10T428/2982

    Abstract: A layered lithium-nickel-based compound oxide powder for a positive electrode material for a high density lithium secondary cell, capable of providing a lithium secondary cell having a high capacity and excellent in the rate characteristics also, is provided. A layered lithium-nickel-based compound oxide powder for a positive electrode material for a lithium secondary cell, characterized in that the bulk density is at least 2.0 g/cc, the average primary particle size B is from 0.1 to 1 μm, the median diameter A of the secondary particles is from 9 to 20 μm, and the ratio A/B of the median diameter A of the secondary particles to the average primary particle size B, is within a range of from 10 to 200. In production of a layered lithium-nickel-based compound oxide powder, which comprises spray drying a slurry having a nickel compound and a transition metal element compound capable of substituting lithium other than nickel, dispersed in a liquid medium, followed by mixing with a lithium compound, and firing the mixture, the spray drying is carried out under conditions of 0.4≦G/S≦4 and G/S≦0.0012 V, when the slurry viscosity at the time of the spray drying is represented by V (cp), the slurry supply amount is represented by S (g/min) and the gas supply amount is represented by G (L/min).

    Abstract translation: 提供了一种用于高密度锂二次电池用正极材料的层状锂镍复合氧化物粉末，其能够提供具有高容量和优异率的锂二次电池。 一种用于锂二次电池用正极材料的层状锂镍系复合氧化物粉末，其特征在于，堆积密度为2.0g / cc以上，平均一次粒径B为0.1〜1μm，中值 二次粒子的直径A为9〜20μm，二次粒子的中值粒径A与平均一次粒径B的比A / B在10〜200的范围内。在 分层的锂镍复合氧化物粉末，其包括喷雾干燥分散在液体介质中的具有镍化合物和能够取代镍以外的锂的过渡金属元素化合物的浆料，然后与锂化合物混合， 混合物中，喷雾干燥在0.4≤G/S≤4和G / S = 0.0012V的条件下进行，当喷雾干燥时的浆料粘度由V（cp）表示时， 浆料供给量用S（g / min）表示 气体供给量由G（L / min）表示。

    Layered lithium-nickel-based compound oxide powder and its production process
    7.
    发明授权
    Layered lithium-nickel-based compound oxide powder and its production process 有权
    分层锂镍复合氧化物粉及其制作工艺

    公开(公告)号：US07309543B2

    公开(公告)日：2007-12-18

    申请号：US11032113

    申请日：2005-01-11

    Applicant: Kenji Shizuka

    Inventor： Kenji Shizuka

    IPC: H01M4/00

    CPC classification number: C01G45/1228 ,  C01G51/50 ,  C01G53/50 ,  C01P2002/22 ,  C01P2002/52 ,  C01P2002/54 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/22 ,  C01P2006/40 ,  H01M4/0404 ,  H01M4/0419 ,  H01M4/0471 ,  H01M4/131 ,  H01M4/505 ,  H01M4/525 ,  H01M4/587 ,  H01M10/0525 ,  H01M10/0568 ,  H01M2004/028 ,  Y10T428/2982

    Abstract: A layered lithium-nickel-based compound oxide powder for a positive electrode material for a high density lithium secondary cell, capable of providing a lithium secondary cell having a high capacity and excellent in the rate characteristics also, is provided.A layered lithium-nickel-based compound oxide powder for a positive electrode material for a lithium secondary cell, characterized in that the bulk density is at least 2.0 g/cc, the average primary particle size B is from 0.1 to 1 μm, the median diameter A of the secondary particles is from 9 to 20 μm, and the ratio A/B of the median diameter A of the secondary particles to the average primary particle size B, is within a range of from 10 to 200. In production of a layered lithium-nickel-based compound oxide powder, which comprises spray drying a slurry having a nickel compound and a transition metal element compound capable of substituting lithium other than nickel, dispersed in a liquid medium, followed by mixing with a lithium compound, and firing the mixture, the spray drying is carried out under conditions of 0.4≦G/S≦4 and G/S≦0.0012V, when the slurry viscosity at the time of the spray drying is represented by V (cp), the slurry supply amount is represented by S (g/min) and the gas supply amount is represented by G (L/min).

    Abstract translation: 提供了一种用于高密度锂二次电池用正极材料的层状锂镍复合氧化物粉末，其能够提供具有高容量和优异率的锂二次电池。 一种用于锂二次电池用正极材料的层状锂镍系复合氧化物粉末，其特征在于，堆积密度为2.0g / cc以上，平均一次粒径B为0.1〜1μm，中值 二次粒子的直径A为9〜20μm，二次粒子的中值粒径A与平均一次粒径B的比A / B在10〜200的范围内。在 分层的锂镍复合氧化物粉末，其包括喷雾干燥分散在液体介质中的具有镍化合物和能够取代镍以外的锂的过渡金属元素化合物的浆料，然后与锂化合物混合， 混合物中，喷雾干燥在0.4≤G/S≤4和G /S≤0.0012V的条件下进行，当喷雾干燥时的浆料粘度由V（cp）表示时， 浆料供给量由S（g / min）和t表示 他的供气量由G（L / min）表示。

    Layered Lithium Nickel Manganese Cobalt Composite Oxide Powder For Material Of Positive Electrode Of Lithium Secondary Battery, Process For Producing The Same, Positive Electrode Of Lithium Secondary Battery Therefrom, And Lithium Secondary Battery
    8.
    发明申请
    Layered Lithium Nickel Manganese Cobalt Composite Oxide Powder For Material Of Positive Electrode Of Lithium Secondary Battery, Process For Producing The Same, Positive Electrode Of Lithium Secondary Battery Therefrom, And Lithium Secondary Battery 有权
    锂二次电池正极材料的层状锂锰锰复合氧化物粉末，其制造方法，锂二次电池正极和锂二次电池

    公开(公告)号：US20070202405A1

    公开(公告)日：2007-08-30

    申请号：US10591911

    申请日：2005-04-27

    Applicant: Kenji Shizuka ,  Kenji Okahara

    Inventor： Kenji Shizuka ,  Kenji Okahara

    IPC: H01M4/52 ,  H01M4/50 ,  C01G45/12 ,  C01G53/04 ,  C01G51/04

    CPC classification number: H01M4/505 ,  C01G45/1228 ,  C01G51/50 ,  C01G53/50 ,  C01P2002/54 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2006/10 ,  C01P2006/12 ,  C01P2006/40 ,  H01M4/131 ,  H01M4/133 ,  H01M4/525 ,  H01M4/587 ,  H01M10/0525 ,  H01M2004/021 ,  H01M2300/004

    Abstract: A powder of a layered lithium-nickel-manganese-cobalt composite oxide for use as a positive-electrode material for lithium secondary battery is provided which, when used as a positive-electrode material for lithium secondary battery, enables a cost reduction and higher safety to be reconciled with improved battery performances. The powder of a layered lithium-nickel-manganese-cobalt composite oxide for use as a positive-electrode material for lithium secondary battery is composed of secondary particles formed by the aggregation of primary particles. It has a composition represented by the following formula (I), has a volume resistivity of 5×105 Ω·cm or lower in the state of being compacted at a pressure of 40 MPa, and has a value of C/S, wherein C is the concentration of carbon contained therein (% by weight) and S is the BET specific surface area thereof (m2/g), of 0.025 or smaller. The powder has been regulated so as to have a volume resistivity not higher than the specified value and a considerably reduced carbon content while having a composition in a limited range, whereby a cost reduction and higher safety can be reconciled with improved battery performances. Li1+zNixMnyCo1−x−yOδ  (I) (0

    Abstract translation: 提供了用作锂二次电池的正极材料的分层锂镍锰钴复合氧化物粉末，其用作锂二次电池的正极材料时，能够降低成本并提高安全性 与电池性能提高相协调。 用作锂二次电池正极材料的层状锂镍锰钴复合氧化物粉末由通过一次粒子聚集而形成的二次粒子构成。 其具有由下式（I）表示的组成，在40MPa的压力下被压实的状态下的体积电阻率为5×10 5Ω·cm以下，并且具有 C / S，其中C是其中所含的碳的浓度（重量％），S是其BET比表面积（m 2 SUP / g），为0.025或更小。 该粉末被调节成具有不高于规定值的体积电阻率并且具有显着降低的碳含量，同时具有在有限范围内的组成，由此可以与改进的电池性能相一致地降低成本和更高的安全性。 <？in-line-formula description =“In-line Formulas”end =“lead”？> Li 1 + z （I）<？in-line-formula description =“In-line Formulas”end =“tail”？>（0

    Nonaqueous electrolyte secondary cell
    9.
    发明授权
    Nonaqueous electrolyte secondary cell 失效
    非水电解质二次电池

    公开(公告)号：US5866279A

    公开(公告)日：1999-02-02

    申请号：US819708

    申请日：1997-03-18

    Applicant: Hiroshi Wada ,  Kenji Shizuka

    Inventor： Hiroshi Wada ,  Kenji Shizuka

    IPC: C01G45/00 ,  H01M2/16 ,  H01M4/131 ,  H01M4/1391 ,  H01M4/50 ,  H01M4/505 ,  H01M10/052 ,  H01M10/36

    CPC classification number: H01M4/505 ,  C01G45/1242 ,  C01P2002/32 ,  C01P2006/40 ,  H01M10/052 ,  H01M2/1653 ,  H01M4/131 ,  H01M4/1391

    Abstract: A nonaqueous electrolyte secondary cell, wherein a lithium-containing metal oxide capable of binding and releasing lithium is used as a positive electrode, and a nonaqueous electrolyte containing a lithium salt is used as an electrolyte, in which a spinel type lithium manganese oxide which satisfies the formula:Li�Mn.sub.2-x Li.sub.x !O.sub.4-.delta.wherein 0.ltoreq.x.ltoreq.0.05, and -0.025.ltoreq..delta..ltoreq.0.050, and wherein the average valency of Mn is within a range of from 3.501 to 3.535, is used as the lithium-containing metal oxide.

    Abstract translation: 使用能够结合和释放锂的含锂金属氧化物的非水电解质二次电池用作正极，并且使用含有锂盐的非水电解质作为电解质，其中满足以下条件的尖晶石型锂锰氧化物 式：Li [Mn2-xLix] O4-δ其中0≤x≤0.05，和-0.025≤δ≤0.050，其中Mn的平均化合价在3.501〜 3.535用作含锂金属氧化物。

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