Plasticizers for Resin Compositions and Resin Compositions Including the Same
    2.
    发明申请
    Plasticizers for Resin Compositions and Resin Compositions Including the Same 审中-公开
    用于树脂组合物的增塑剂和包括其的树脂组合物

    公开(公告)号:US20130253095A1

    公开(公告)日:2013-09-26

    申请号:US13989867

    申请日:2011-11-28

    Abstract: This invention relates to a resin composition using a dicarboxylic acid diester derivative as a plasticizer, and particularly to a resin composition, which is obtained by adding the plasticizer to one or more resins selected from among aliphatic or aromatic polycarbonate resins, polyurethane resins, polyvinyl chloride resins and epoxy resins, and which has a low glass transition temperature (Tg) and can be easily processed and can impart flexibility to products. This plasticizer exhibits high plasticization efficiency, and a resin composition including the plasticizer can manifest a low glass transition temperature and good flexibility at low temperature, thus improving physical properties such as tensile strength, even when only a small amount of the plasticizer is added.

    Abstract translation: 本发明涉及一种使用二羧酸二酯衍生物作为增塑剂的树脂组合物,特别涉及一种树脂组合物,该树脂组合物是通过将增塑剂添加到一种或多种选自脂族或芳族聚碳酸酯树脂,聚氨酯树脂,聚氯乙烯 树脂和环氧树脂,并且具有低的玻璃化转变温度(Tg),并且可以容易地加工并且可以赋予产品柔性。 该增塑剂显示出高的增塑效率,并且包含该增塑剂的树脂组合物在低温下可以表现出低的玻璃化转变温度和良好的柔韧性,因此即使仅添加少量的增塑剂也能改善诸如拉伸强度的物理性能。

    PLASTICIZER AND METHOD OF PREPARING THE SAME
    3.
    发明申请
    PLASTICIZER AND METHOD OF PREPARING THE SAME 有权
    塑化剂及其制备方法

    公开(公告)号:US20130072611A1

    公开(公告)日:2013-03-21

    申请号:US13695736

    申请日:2011-02-28

    Abstract: The present invention provides an ester plasticizer for polyvinyl chloride (PVC) resin, epoxy resin or urethane resin and a method of preparing the same. More particularly, the present invention provides an ester plasticizer using triacetin and coconut oil-based biodiesel as raw materials, which can prepare a resin composition having excellent plasticizing efficiency and improved physical properties such as tensile strength and the like.When a polyvinyl chloride resin or the like is manufactured using the ester plasticizer, there are advantages in that an environment-friendly product having an excellent plasticizing efficiency and in that the physical properties such as hardness, tensile strength, etc. of the product are improved.

    Abstract translation: 本发明提供聚氯乙烯(PVC)树脂,环氧树脂或聚氨酯树脂的酯增塑剂及其制备方法。 更具体地说,本发明提供使用三醋精和椰子油类生物柴油作为原料的酯增塑剂,其可以制备具有优异的增塑效率和改善的物理性能如拉伸强度等的树脂组合物。 当使用酯增塑剂制造聚氯乙烯树脂等时,具有优异的增塑效果良好的环境友好产品,并且改善了产品的物理性能如硬度,拉伸强度等 。

    Method of preparing 10H-dibenzo[b,f][11,4]thiazepin-11-one
    4.
    发明授权
    Method of preparing 10H-dibenzo[b,f][11,4]thiazepin-11-one 有权
    制备10H-二苯并[b,f] [11,4]硫杂环庚烯-11-酮的方法

    公开(公告)号:US07214793B2

    公开(公告)日:2007-05-08

    申请号:US10533052

    申请日:2003-11-26

    CPC classification number: C07D281/16

    Abstract: Disclosed is a method of preparing 10H-dibenzo[b,f][1,4]thiazepin-11-one, including reacting dithiosalicylic acid with 1-chloro-2-nitrobenzene in a basic aqueous solution in the presence or absence of a reducing agent, to prepare 2-(2-nitrophenylsulfuryl)benzoic acid; subjecting the 2-(2-nitrophenylsulfuryl)benzoic acid to nitro group reduction in the presence of hydrogen, a solvent and a heterogeneous metal catalyst, to prepare 2-(2-aminophenylsulfuryl)benzoic acid; and directly cyclizing the 2-(2-aminophenylsulfuryl)benzoic acid in an organic solvent in the presence or absence of an acid catalyst. The method according to the present invention is economical due to the use of the inexpensive starting material, and also environmentally friendly and efficient by minimizing the use of the organic solvent and performing direct cyclization without the activation of carboxylic acid.

    Abstract translation: 公开了一种制备10H-二苯并[b,f] [1,4]硫杂吖庚因-11-酮的方法,包括在存在或不存在还原剂的情况下,将二硫代水杨酸与1-氯-2-硝基苯在碱性水溶液中反应 制备2-(2-硝基苯基硫基)苯甲酸; 在氢气,溶剂和非均相金属催化剂的存在下使2-(2-硝基苯基亚磺酰基)苯甲酸进行硝基还原,制备2-(2-氨基苯基硫基)苯甲酸; 并在酸催化剂存在或不存在下,在有机溶剂中直接环化2-(2-氨基苯基硫基)苯甲酸。 根据本发明的方法由于使用廉价的起始材料而是经济的,并且通过最小化有机溶剂的使用并且在没有羧酸活化的情况下进行直接环化,也是环境友好和有效的。

    Method for the production of serinol
    5.
    发明授权
    Method for the production of serinol 失效
    生产丝氨醇的方法

    公开(公告)号:US06509504B1

    公开(公告)日:2003-01-21

    申请号:US09936062

    申请日:2001-12-12

    CPC classification number: C07C213/02 C07C201/12 C07C215/10 C07C205/15

    Abstract: Disclosed is a method for preparing serinol (2-amino-1,3-proanediol). From nitromethane, para-formaldehyde and sodium hydroxide, 1-nitro-1,3-propanediol sodium salt is prepared as a medical intermediate. In a fixed bed, this intermediate is allowed to undergo the continuous hydrogenation of 2-nitro-1,3-propanediol sodium salt and methanol as shown in reaction (1). In addition to being simple, the method is economically favorable and affords the high yield and high purity of serinol.

    Abstract translation: 公开了一种制备丝氨醇(2-氨基-1,3-丙二醇)的方法。 由硝基甲烷,对甲醛和氢氧化钠制备1-硝基-1,3-丙二醇钠盐作为医疗中间体。 在固定床中,如反应(1)所示,使该中间体进行2-硝基-1,3-丙二醇钠盐和甲醇的连续氢化。 除了简单,该方法在经济上是有利的,并提供高产率和高纯度的丝氨醇。

    ESTER-BASED PLASTICIZER
    7.
    发明申请
    ESTER-BASED PLASTICIZER 审中-公开
    基于ESTER的塑料加工机

    公开(公告)号:US20120136101A1

    公开(公告)日:2012-05-31

    申请号:US13384799

    申请日:2010-07-13

    CPC classification number: C07C69/78 C07C67/26 C07C69/28 C08K5/103 C08L27/06

    Abstract: The present invention relates to a novel ester-based plasticizer, and, more particularly, to an ester plasticizer, which is synthesized by esterifying a polyhydric alcohol and an alkylene oxide with an aliphatic carboxylic acid or an aromatic carboxylic acid. When a polyvinylchloride resin is manufactured using the ester-based plasticizer, there are advantages in that products having a high plasticizing efficiency can be obtained and in that products having excellent physical properties, such as hardness, tensile strength, etc., can be obtained.

    Abstract translation: 本发明涉及一种新的酯类增塑剂,更具体地说,涉及通过用脂族羧酸或芳族羧酸酯化多元醇和烯化氧来合成的酯增塑剂。 当使用酯系增塑剂制造聚氯乙烯树脂时,可以获得具有高塑化效率的产品的优点,并且可以获得具有优异物理性能如硬度,拉伸强度等的产品。

    Plasticizer and method of preparing the same
    8.
    发明授权
    Plasticizer and method of preparing the same 有权
    增塑剂及其制备方法

    公开(公告)号:US09051262B2

    公开(公告)日:2015-06-09

    申请号:US13695736

    申请日:2011-02-28

    Abstract: The present invention provides an ester plasticizer for polyvinyl chloride (PVC) resin, epoxy resin or urethane resin and a method of preparing the same. More particularly, the present invention provides an ester plasticizer using triacetin and coconut oil-based biodiesel as raw materials, which can prepare a resin composition having excellent plasticizing efficiency and improved physical properties such as tensile strength and the like.When a polyvinyl chloride resin or the like is manufactured using the ester plasticizer, there are advantages in that an environment-friendly product having an excellent plasticizing efficiency and in that the physical properties such as hardness, tensile strength, etc. of the product are improved.

    Abstract translation: 本发明提供聚氯乙烯(PVC)树脂,环氧树脂或聚氨酯树脂的酯增塑剂及其制备方法。 更具体地说,本发明提供使用三醋精和椰子油类生物柴油作为原料的酯增塑剂,其可以制备具有优异的增塑效率和改善的物理性能如拉伸强度等的树脂组合物。 当使用酯增塑剂制造聚氯乙烯树脂等时,具有优异的增塑效果良好的环境友好产品,并且改善了产品的物理性能如硬度,拉伸强度等 。

    Hot Melt Composition
    9.
    发明申请
    Hot Melt Composition 审中-公开
    热熔胶组成

    公开(公告)号:US20140206835A1

    公开(公告)日:2014-07-24

    申请号:US14238988

    申请日:2012-07-27

    CPC classification number: C09J169/00 C08G64/0208 C08G64/34

    Abstract: Provided is a hot melt adhesive composition including aliphatic polycarbonate. With the hot melt adhesive composition according to the present invention, the pyrolysis temperature is low, such that the harmful gas is not generated at the time of waste treatment, resulting in providing an excellent environmentally friendly product. In addition, the hot melt adhesive composition has the low melting temperature to thereby be usable at low temperature and exhibit sufficient adhesive strength.

    Abstract translation: 提供了包含脂肪族聚碳酸酯的热熔性粘合剂组合物。 根据本发明的热熔粘合剂组合物,热解温度低,废弃处理时不产生有害气体,从而提供优良的环保产品。 此外,热熔粘合剂组合物具有低熔点温度,从而可在低温下使用并且具有足够的粘合强度。

    Method of preparing 10th-dibenzo[b,f][11,4]thiazepin-11-one
    10.
    发明申请
    Method of preparing 10th-dibenzo[b,f][11,4]thiazepin-11-one 有权
    制备10-二苯并[b,f] [11,4]硫杂环丁烷-11-酮的方法

    公开(公告)号:US20070066589A1

    公开(公告)日:2007-03-22

    申请号:US10533052

    申请日:2003-11-26

    CPC classification number: C07D281/16

    Abstract: Disclosed is a method of preparing 10H-dibenzo[b,f][1,4]thiazepin-11-one, including reacting dithiosalicylic acid with 1-chloro-2-nitrobenzene in a basic aqueous solution in the presence or absence of a reducing agent, to prepare 2-(2-nitrophenylsulfuryl)benzoic acid; subjecting the 2-(2-nitrophenylsulfuryl)benzoic acid to nitro group reduction in the presence of hydrogen, a solvent and a heterogeneous metal catalyst, to prepare 2-(2-aminophenylsulfuryl)benzoic acid; and directly cyclizing the 2-(2-aminophenylsulfuryl)benzoic acid in an organic solvent in the presence or absence of an acid catalyst. The method according to the present invention is economical due to the use of the inexpensive starting material, and also environmentally friendly and efficient by minimizing the use of the organic solvent and performing direct cyclization without the activation of carboxylic acid.

    Abstract translation: 公开了一种制备10H-二苯并[b,f] [1,4]硫杂吖庚因-11-酮的方法,包括在存在或不存在还原剂的情况下,将二硫代水杨酸与1-氯-2-硝基苯在碱性水溶液中反应 制备2-(2-硝基苯基硫基)苯甲酸; 在氢气,溶剂和非均相金属催化剂的存在下使2-(2-硝基苯基亚磺酰基)苯甲酸进行硝基还原,制备2-(2-氨基苯基硫基)苯甲酸; 并在酸催化剂存在或不存在下,在有机溶剂中直接环化2-(2-氨基苯基硫基)苯甲酸。 根据本发明的方法由于使用廉价的起始材料而是经济的,并且通过最小化有机溶剂的使用并且在没有羧酸活化的情况下进行直接环化,也是环境友好和有效的。

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