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公开(公告)号：US08206463B2
公开(公告)日：2012-06-26
申请号：US11417720
申请日：2006-05-04
CPC分类号： C08J7/065 , B05D5/06 , B05D5/067 , B27K5/02 , B33Y40/00 , B33Y70/00 , C03C17/32 , C03C17/38 , D06P1/65118 , D06P5/00
摘要： A process for making a colored article of manufacture is disclosed. Accordingly an article of manufacture is first prepared of a material selected from the group consisting of metal, wood, glass, ceramic, masonry and polymeric materials. A polymeric coating (superstrate) is then applied to at least a portion of the surface of the article. At least a portion of the superstrate is brought into contact with a material system that contains (i) water, (ii) a carrier, (iii) a dye and (iv) a diol, under conditions calculated to bring about diffusion of said dye into said superstrate.
摘要翻译： 公开了制造彩色制品的方法。 因此，首先由选自金属，木材，玻璃，陶瓷，砖石和聚合材料的材料制备制品。 然后将聚合物涂层（覆盖层）施加到制品表面的至少一部分。 所述覆层的至少一部分与材料体系接触，所述材料体系包含（i）水，（ii）载体，（iii）染料和（iv）二醇，所述条件被计算为使所述染料 进入上层。
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2.发明授权Expansion of polymeric microspheres insitu in a rigid PUR/PIR foam formulation using a twin screw extruder 失效使用双螺杆挤出机将刚性PUR / PIR泡沫配制物中的聚合物微球膨胀
公开(公告)号：US6022912A
公开(公告)日：2000-02-08
申请号：US158209
申请日：1998-09-22
IPC分类号： B29B7/46 , B29B7/88 , B29C70/66 , B29K101/00 , B29K105/04 , C08G18/00 , C08G18/08 , C08G18/42 , C08G101/00 , C08J9/224 , C08J9/32 , B29D31/00 , B29C35/00 , C08J3/00 , C08K9/00 , C08L75/00
CPC分类号： C08J9/32 , B29C70/66 , C08G18/0876 , C08G18/4208 , C08J9/224 , C08G2101/0025 , C08J2203/14 , C08J2203/22 , C08J2375/04
摘要： The present invention relates to a process for producing a dispersion of polymeric microspheres in a polyol comprising expanding 1 to 70% by weight of polymeric beads in a polyol with a twin screw extruder to simultaneously mix and expand the beads to create a uniform dispersion of the microspheres in the polyol such that the wetting of the microspheres by the polyol is maximized.
摘要翻译： 本发明涉及在多元醇中制备聚合物微球分散体的方法，该方法包括用双螺杆挤出机在多元醇中使1-70重量％的聚合物珠膨胀，同时混合和膨胀珠粒以产生均匀的分散体 多元醇中的微球，使得多元醇对微球的润湿最大化。
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3.发明申请Apparatus and process for treating an article to impart color and/or enhance the properties of that article 有权用于处理制品以赋予颜色和/或增强该制品的性质的装置和方法公开(公告)号：US20080286478A1
公开(公告)日：2008-11-20
申请号：US11803917
申请日：2007-05-16
申请人： Edward F. Kaczkowski , Robert A. Pyles , Daniel E. Jaskiewicz , Rick L. Archey , George See , Ronald J. Rathi
发明人： Edward F. Kaczkowski , Robert A. Pyles , Daniel E. Jaskiewicz , Rick L. Archey , George See , Ronald J. Rathi
CPC分类号： B05D1/02 , B05D3/02 , B05D2201/00 , B05D2203/20 , C08J7/065 , D06M23/02 , D06M23/06 , D06P1/0016 , Y10T428/8305
摘要： A process and an apparatus for treating large articles to impart color or performance enhancing additives to the article in which a treatment system which includes: (i) a coloring solution and/or a solution containing at least one performance enhancing additive, (ii) water, and (iii) a solvent such as ethylene glycol monobutyl ether and diethylene glycol is applied to the article. The apparatus is made up of (a) a spray enclosure sized to contain the article(s) to be treated; (b) dispensing means, such as nozzles, which are configured to dispense sequentially, hot solution (i), hot solution (ii) and hot water (iii) directly onto the article surface(s); (c) means for securing and transporting the article to be treated into and out of the spray enclosure (such as a trolley system); and at least three closed vessels capable of delivering enough hot saturated coloring and/or performance enhancing solution, hot dye-free rinse solution and deionized water, respectively, with sufficient pressure to form small droplets from the spray nozzles, to thoroughly cover and rinse articles contained in the enclosure.
摘要翻译： 一种用于处理大件物品以将颜色或性能增强添加剂赋予制品的方法和设备，其中处理系统包括：（i）着色溶液和/或含有至少一种性能增强添加剂的溶液，（ii）水 ，和（iii）将溶剂如乙二醇单丁醚和二甘醇应用于制品。 该设备由（a）尺寸设计成容纳待处理物品的喷雾罩组成; （b）诸如喷嘴的分配装置，其被配置为将热溶液（i），热溶液（ii）和热水（iii）直接分配到物品表面上; （c）用于固定和运输要处理的物品进出喷雾外壳（例如手推车系统）的装置; 和至少三个密封容器，其能够分别以足够的压力输送足够的热饱和着色和/或性能增强溶液，不含热染料的漂洗溶液和去离子水，以从喷嘴形成小液滴，以彻底地覆盖和冲洗物品 包含在外壳中。
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公开(公告)号：US07175675B2
公开(公告)日：2007-02-13
申请号：US10733111
申请日：2003-12-11
IPC分类号： D06P5/00
CPC分类号： D06P1/613 , D06P1/60 , D06P1/65118 , D06P5/00
摘要： In the method of the present invention a plastic article (e.g., a molded article of thermoplastic polycarbonate) is immersed at least partially in a dye bath which includes one or more dyes, water, at least one carrier, and at least one diol. The dye bath contains: (i) at least one dye (e.g., a static and/or photochromic dye); (ii) water; (iii) at least one carrier represented by the following general formula I, R—O—(CH2)n—OHI wherein R is a radical selected from linear or branched C1–C18 alkyl, benzyl, benzoyl and phenyl, and n is 2 or 3; and (iv) a diol selected from at least one of linear or branched C2–C20 aliphatic diols, poly(C2–C4 alkylene glycol), cycloaliphatic diols having from 5 to 8 carbon atoms in the cyclic ring, monocyclic aromatic diols, bisphenols and hydrogenated bisphenols. In an embodiment of the present invention, the carrier is ethyleneglycol butyl ether, and the diol is diethylene glycol. The present invention also relates to a method of separating the dye from the water, carrier and diol components of the dye bath, by contacting the dye bath with particulate activated carbon.
摘要翻译： 在本发明的方法中，将塑料制品（例如，热塑性聚碳酸酯的模塑制品）至少部分地浸入包括一种或多种染料，水，至少一种载体和至少一种二醇的染浴中。 染浴包含：（i）至少一种染料（例如静电和/或光致变色染料）; （ii）水; （iii）由以下通式I表示的至少一种载体：<？in-line-formula description =“In-line Formulas”end =“lead”？> RO-（CH 2/2） 其中R是选自直链或支链C 1〜C的基团，其中R是选自直链或支链C 1〜 C 18 -C 18烷基，苄基，苯甲酰基和苯基，n为2或3; 和（iv）选自直链或支链C 2 -C 20脂肪族二醇中的至少一种的二醇，聚（C 2 -C 20 - 亚烷基二醇），环中具有5-8个碳原子的脂环族二醇，单环芳族二醇，双酚和氢化双酚。 在本发明的一个实施方案中，载体是乙二醇丁醚，二醇是二甘醇。 本发明还涉及通过使染料浴与颗粒活性炭接触来分离染料与染浴的水，载体和二醇组分的方法。
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公开(公告)号：US06733543B2
公开(公告)日：2004-05-11
申请号：US10106788
申请日：2002-03-26
申请人： Robert A. Pyles , Rick L. Archey
发明人： Robert A. Pyles , Rick L. Archey
IPC分类号： D06P500
摘要： A process of dyeing a molded article is disclosed. The process entails immersing at least a portion of the article in a dyeing bath, retaining the portion in the bath for a period of time sufficient to allow an amount of dye to diffuse into the article, and removing said article from the bath. The molded article comprises a polymeric resin such as (co)polyester, (co)polycarbonates, acrylonitrile-butadiene-styrene, polyamide, polyurethane, polyalkyl(meth)acrylate, allyldiglycol carbonate and styrene copolymers. The dyeing bath contains in addition to dye, water, a plasticizing agent and a leveling agent.
摘要翻译： 公开了一种染色模制品的方法。 该方法需要将至少一部分制品浸入染色浴中，将该部分保留在浴中一段足以使一定量的染料扩散到制品中的时间，以及从浴中除去所述制品。 模制品包括聚合树脂，例如（共）聚酯，（共）聚碳酸酯，丙烯腈 - 丁二烯 - 苯乙烯，聚酰胺，聚氨酯，（甲基）丙烯酸烷基酯，烯丙基二醇碳酸酯和苯乙烯共聚物。 染色浴除了染料，水，增塑剂和流平剂外还含有。
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公开(公告)号：US5399658A
公开(公告)日：1995-03-21
申请号：US146284
申请日：1993-10-29
CPC分类号： C08G64/42 , C08G64/081 , C08L69/00
摘要： A gamma radiation-resistant polycarbonate-disulfide resin is disclosed. The incorporation of disulfide linkages in the structure of polycarbonate was found to enhance the resistance of the resin to the discoloration caused by exposure to gamma radiation. Accordingly, processes for the incorporation of disulfide linkages in the molecular backbone, as end-groups or as side chains are disclosed. The polycarbonate-disulfide resin may be used as a molding resin in the context of thermoplastic molding compositions as well as a stabilizing additive in polycarbonate resin.
摘要翻译： 公开了一种耐伽马辐射的聚碳酸酯 - 二硫化物树脂。 发现在聚碳酸酯结构中引入二硫键增加了树脂对由于暴露于γ辐射引起的变色的抵抗力。 因此，公开了在分子主链中作为端基或作为侧链引入二硫键的方法。 聚碳酸酯 - 二硫化物树脂可以在热塑性模塑组合物和聚碳酸酯树脂中的稳定添加剂的情况下用作模制树脂。
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公开(公告)号：US5294729A
公开(公告)日：1994-03-15
申请号：US97743
申请日：1993-07-27
CPC分类号： C07C69/96
摘要： A process for preparing a block oligocarbonate is disclosed. The oligocarbonate conforms to ##STR1## where R denotes hydrogen or ##STR2## and where A denotes an aromatic carbonate structure conforming to ##STR3## where Ar is an aromatic radical, n is 2-6 and where B is the residue of an aliphatic polyol is disclosed. In the process a high molecular weight aromatic polycarbonate is reacted, in the melt and in the presence of a catalyst, with an aliphatic polyol. The block oligocarbonate is useful as a reactant in a process for the preparation of copolymers.
摘要翻译： 公开了制备低聚碳酸酯嵌段的方法。 低聚碳酸酯符合RABAR或者IMAGE，其中R表示氢或“IMAGE”，其中A表示符合
的芳族碳酸酯结构，其中Ar是芳族基团，n是2-6，其中B是 公开了脂族多元醇。 在此过程中，高分子量芳族聚碳酸酯在熔体和催化剂存在下与脂族多元醇反应。 在制备共聚物的方法中，低聚碳酸酯嵌段可用作反应物。 -
8.发明申请POLYCARBONATE COMPOSITIONS HAVING IMPROVED WATER RESISTANCE AND RELATED METHODS 审中-公开具有改善的耐水性和相关方法的聚碳酸酯组合物公开(公告)号：US20130090419A1
公开(公告)日：2013-04-11
申请号：US13253213
申请日：2011-10-05
摘要： The present invention relates to compositions containing a polycarbonate including a bisphenol compound and an effective amount of a bishaloformate component present in an amount sufficient to reduce the average unbound bisphenol compound level found in water after immersion in deionized water for two weeks at 40° C. of the composition to less than about 20 ppb. Also provided are methods for increasing the water resistance of a polycarbonate composition. The method involves adding an effective amount of a bishaloformate component to the polycarbonate composition such that the polycarbonate composition has an average unbound bisphenol compound level found in water after immersion in deionized water for two weeks at 40° C. of less than about 20 ppb.
摘要翻译： 本发明涉及包含双酚化合物的聚碳酸酯和有效量的双卤代甲酸酯组分的组合物，其量足以降低在40℃下浸入去离子水中2周后在水中发现的平均未结合双酚化合物水平。 的组成小于约20ppb。 还提供了增加聚碳酸酯组合物的耐水性的方法。 该方法包括向聚碳酸酯组合物中加入有效量的双卤代甲酸酯组分，使得聚碳酸酯组合物在40℃下浸入去离子水中两周后，在水中发现的平均未结合双酚化合物水平小于约20ppb。
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公开(公告)号：US06994735B2
公开(公告)日：2006-02-07
申请号：US10434242
申请日：2003-05-08
IPC分类号： D06P1/613
CPC分类号： D06P1/90 , C08J7/065 , C08J2369/00 , D06P1/65106 , D06P1/65118 , D06P1/65131
摘要： A process for tinting a molded article is disclosed. The process entails applying by spraying or by flow coating a hot, dye-solution onto at least a portion of the surface of a molded article to obtain a tinted article and washing the tinted article. In addition to the dissolved dye, the dye solution that is substantially free of particulate matter contains an aqueous solution of a carrier and an optional emulsifier. The article is one molded of a thermoplastic molding composition. In an embodiment of the invention, the dye solution is prepared by filtering a hot aqueous solution through a bag filter that contains a dye to obtain a hot, dye-solution. In a further embodiment, activated carbon is used to purify the dye solution to obtain a dye-free aqueous solution.
摘要翻译： 公开了一种着色模制品的方法。 该方法需要通过喷雾或通过将热的染料溶液流涂在模制品的表面的至少一部分上来获得有色制品并洗涤有色制品。 除了溶解的染料之外，基本上不含颗粒物质的染料溶液含有载体和任选的乳化剂的水溶液。 该制品是由热塑性模塑组合物成型的。 在本发明的一个实施方案中，通过将热水溶液通过含有染料的袋式过滤器过滤以获得热的染料溶液来制备染料溶液。 在另一个实施方案中，使用活性炭来纯化染料溶液以获得无染料的水溶液。
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公开(公告)号：US06949127B2
公开(公告)日：2005-09-27
申请号：US10796523
申请日：2004-03-09
申请人： Robert A. Pyles , Rick L. Archey
发明人： Robert A. Pyles , Rick L. Archey
IPC分类号： G02C7/02 , D06P1/16 , D06P1/613 , D06P1/651 , D06P1/92 , D06P3/00 , D06P3/54 , D06P5/00 , D06P5/20 , G02B1/04 , D06P1/60 , D06P1/64
摘要： A process of dyeing a molded article is disclosed. The process entails immersing at least a portion of the article in a dyeing bath, retaining the portion in the bath for a period of time sufficient to allow an amount of dye to diffuse into the article, and removing said article from the bath. The molded article comprises a polymeric resin such as (co)polyester, (co)polycarbonates, acrylonitrile-butadiene-styrene, polyamide, polyurethane, polyalkyl(meth)-acrylate, allyldiglycol carbonate and styrene copolymers. The dyeing bath contains in addition to dye, water, a plasticizing agent and a leveling agent.
摘要翻译： 公开了一种染色模制品的方法。 该方法需要将至少一部分制品浸入染色浴中，将该部分保留在浴中一段足以使一定量的染料扩散到制品中的时间，以及从浴中除去所述制品。 模制品包括聚合树脂，例如（共）聚酯，（共）聚碳酸酯，丙烯腈 - 丁二烯 - 苯乙烯，聚酰胺，聚氨酯，聚（甲基）丙烯酸烷基酯，烯丙基二醇碳酸酯和苯乙烯共聚物。 染色浴除了染料，水，增塑剂和流平剂外还含有。
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