High-temperature superconducting solid bodies and process for producing
them
    1.
    发明授权
    High-temperature superconducting solid bodies and process for producing them 失效
    高温超导固体及其制备方法

    公开(公告)号:US5830829A

    公开(公告)日:1998-11-03

    申请号:US545775

    申请日:1995-11-27

    摘要: The invention relates to a process for producing textured high-temperature superconducting solid shaped parts, which comprises solid shaped parts made of oxide-ceramic superconducting material of a phase mixture of the substance class YBCO first being molded, pressed and sintered, a zonewise thermal treatment then being carried out along their longitudinal axis. Heating is first carried out, in a first zone, to a temperature in the range of from 50 to 200 K below the peritectic melting temperature of the phase mixture initially present in the shaped part, the temperature then is raised, in a second zone having a temperature gradient in the range of from 10 to 250 K/cm, then, in a third zone, a temperature of up to 50 K above the peritectic melting temperature of the phase mixture initially present in the shaped part is maintained, cooling then being carried out, in a fourth zone having a temperature gradient in the range of from 10 to 250 K/cm. Finally, in yet a fifth zone, a temperature in the range of from 50 to 200 K below the peritectic melting temperature of the phase mixture initially present in the shaped part is maintained. According to the invention, the zones are moved along in the longitudinal direction at a speed in the range of from 1 to 10 mm/h.

    摘要翻译: PCT No.PCT / EP94 / 02206 Sec。 371日期:1995年11月27日 102(e)日期1995年11月27日PCT 1994年7月6日PCT公布。 公开号WO95 / 02717 日期1995年1月26日本发明涉及一种生产纹理高温超导固体成形部件的方法,该方法包括由氧化物 - 陶瓷超导材料制成的固体成形部件,该物质类别为YBCO的相混合物首先被模制,压制和烧结 然后沿着其纵向轴线进行了一个zonewise热处理。 首先在第一区域中进行加热,其温度在最初存在于成型部件中的相混合物的包晶熔化温度以下的温度范围内为50〜200K,然后在具有 温度梯度在10至250K / cm的范围内,则在第三区域中,保持最初存在于成型部件中的相混合物的包晶熔化温度高于50K的温度,然后冷却 在具有10至250K / cm 2的温度梯度的第四区域中进行。 最后,在第五区域中,保持最初存在于成形部件中的相混合物的包晶熔融温度以下50〜200K的范围内的温度。 根据本发明,这些区域沿着纵向方向以1至10mm / h的速度移动。

    Shaped bodies comprising textured superconducting material and a process for their production
    4.
    发明授权
    Shaped bodies comprising textured superconducting material and a process for their production 失效
    包括纹理超导材料的成形体及其生产方法

    公开(公告)号:US06221813B1

    公开(公告)日:2001-04-24

    申请号:US09424719

    申请日:1999-11-30

    IPC分类号: B28B300

    CPC分类号: H01L39/2419 H01L39/248

    摘要: The invention relates to a process for producing a shaped body, in which a mixture of oxidic starting powders or a superconducting material, which comprises at least 30% by volume of platelet-shaped primary particles and has such a composition that a high-temperature superconducting material is formed on later, suitable thermal treatment, is comminuted by milling, shearing and/or rolling in such a way that the comminuted powder has a powder particle size distribution having a d90 of ≦20 &mgr;m, and in which the powders which have been comminuted in this way are isostatically compacted by the dry bag method.

    摘要翻译: 本发明涉及一种生产成形体的方法,其中包含至少30体积%的血小板形初级颗粒的氧化起始粉末或超导材料的混合物,并且具有这样的组成:高温超导 在稍后形成材料,合适的热处理,通过研磨,剪切和/或轧制粉碎,粉碎粉末具有d90 <=20μm的粉末粒度分布,其中具有 以这种方式被粉碎,通过干袋法均匀压实。