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    Process for making a carbon nanotubes/ultra-high molar mass polyethylene composite fibre
    1.
    发明授权
    Process for making a carbon nanotubes/ultra-high molar mass polyethylene composite fibre 有权
    制造碳纳米管/超高摩尔质量聚乙烯复合纤维的方法

    公开(公告)号：US07780888B2

    公开(公告)日：2010-08-24

    申请号：US11658155

    申请日：2005-07-14

    申请人： Harm van der Werff ,  Shilun Ruan ,  Tongxi Yu ,  Ping Gao ,  Roelef Marissen

    发明人： Harm van der Werff ,  Shilun Ruan ,  Tongxi Yu ,  Ping Gao ,  Roelef Marissen

    IPC分类号： D01F6/00 ,  C08K3/02

    CPC分类号： B82Y30/00 ,  D01F1/10 ,  D01F6/04

    摘要： The invention relates to a process for making a carbon nanotubes/ultra-high molar mass polyethylene (CNTs/UHPE) composite fiber comprising the steps of a) pre-treating CNTs with an acidic aqueous solution; b) making a composition containing pre-treated CNTs dispersed in a solution of UHPE in a spin solvent; and c) spinning the composition obtained into fibers; wherein step b) comprises making a dispersion of pre-treated CNTs in an alcohol, and mixing this dispersion with a mixture of UHPE and spin solvent. With this process CNTs/UHPE composite fibers showing improved tensile properties are obtained at relatively low CNTs content. A further advantage is that no or hardly any additional components, like dispersion aids, need to be added to make a stable dispersion of CNTs in the spin composition. The invention also relates to a CNTs/UHPE composite fiber obtainable by the process according to the invention, and to semi-finished or end-use articles containing said composite fiber.

    摘要翻译： 本发明涉及一种制备碳纳米管/超高摩尔质量聚乙烯（CNTs / UHPE）复合纤维的方法，包括以下步骤：a）用酸性水溶液预处理CNT; b）制备含有预处理的CNT分散在UHPE在旋转溶剂中的溶液中的组合物; 和c）将得到的组合物纺丝成纤维; 其中步骤b）包括将预处理的CNT分散在醇中，并将该分散体与UHPE和旋转溶剂的混合物混合。 通过这种方法，CNTs / UHPE复合纤维在较低的CNTs含量下得到显示出改善的拉伸性能。 另一个优点是不需要或几乎没有任何附加的组分，如分散助剂，以便使CNT在纺丝组合物中的稳定分散。 本发明还涉及通过本发明的方法获得的CNTs / UHPE复合纤维，以及含有所述复合纤维的半成品或最终用途制品。

    Process For Making a Carbon Nanotubes/Ultra-High Molar Mass Polyethylene Composite Fibre
    2.
    发明申请
    Process For Making a Carbon Nanotubes/Ultra-High Molar Mass Polyethylene Composite Fibre 有权
    制备碳纳米管/超高摩尔质量聚乙烯复合纤维的方法

    公开(公告)号：US20080145301A1

    公开(公告)日：2008-06-19

    申请号：US11658155

    申请日：2005-07-14

    申请人： Harm Van Der Werff ,  Shilun Ruan ,  Tongxi Yu ,  Ping Gao ,  Roelef Marissen

    发明人： Harm Van Der Werff ,  Shilun Ruan ,  Tongxi Yu ,  Ping Gao ,  Roelef Marissen

    IPC分类号： D01F9/12 ,  B28B11/00

    CPC分类号： B82Y30/00 ,  D01F1/10 ,  D01F6/04

    摘要： The invention relates to a process for making a carbon nanotubes/ultra-high molar mass polyethylene (CNTs/UHPE) composite fibre comprising the steps of a) pre-treating CNTs with an acidic aqueous solution; b) making a composition containing pre-treated CNTs dispersed in a solution of UHPE in a spin solvent; and c) spinning the composition obtained into fibres; wherein step b) comprises making a dispersion of pre-treated CNTs in an alcohol, and mixing this dispersion with a mixture of UHPE and spin solvent. With this process CNTs/UHPE composite fibres showing improved tensile properties are obtained at relatively low CNTs content. A further advantage is that no or hardly any additional components, like dispersion aids, need to be added to make a stable dispersion of CNTs in the spin composition. The invention also relates to a CNTs/UHPE composite fibre obtainable by the process according to the invention, and to semi-finished or end-use articles containing said composite fibre.

    摘要翻译： 本发明涉及一种制备碳纳米管/超高摩尔质量聚乙烯（CNTs / UHPE）复合纤维的方法，包括以下步骤：a）用酸性水溶液预处理CNT; b）制备含有预处理的CNT分散在UHPE在旋转溶剂中的溶液中的组合物; 和c）将得到的组合物纺丝成纤维; 其中步骤b）包括将预处理的CNT分散在醇中，并将该分散体与UHPE和旋转溶剂的混合物混合。 通过这种方法，CNTs / UHPE复合纤维在较低的CNTs含量下得到显示出改善的拉伸性能。 另一个优点是不需要或几乎没有任何附加的组分，如分散助剂，以便使CNT在纺丝组合物中的稳定分散。 本发明还涉及通过本发明的方法获得的CNTs / UHPE复合纤维，以及含有所述复合纤维的半成品或最终用途制品。