摘要:
The invention provides a process for producing an aqueous dispersion of particles of rutile titanium oxide, which comprises: a first step in which after a chloride ion concentration of an aqueous solution of titanium tetrachloride is adjusted to 0.5 mole/L or more and less than 4.4 mole/L, the aqueous solution of titanium tetrachloride is heated at a temperature in a range of from 25° C. to 75° C. to hydrolyze the titanium tetrachloride, thereby obtaining a slurry containing the thus precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a fifth step in which an acid is added to the slurry obtained in the fourth step to deflocculate the slurry, and the resulting slurry is subjected to wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.
摘要:
The invention provides a dispersion of particles of rutile titanium oxide wherein the particles of rutile titanium oxide have a D50 in a range of 1 to 15 nm and a D90 of 40 nm or less in particle size distribution as determined by a dynamic light scattering method; a specific surface area in a range of 120 to 180 m2/g as determined by a BET method; and a rate of weight loss of 5% or less as obtained by heating the particles of rutile titanium oxide from 105° C. to 900° C.Such a dispersion of particles of rutile titanium oxide is obtained by a process according to the invention, which comprises: a first step in which an aqueous titanium tetrachloride solution is heated and hydrolyzed to obtain a slurry containing the precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water; a fifth step in which an acid is added to the slurry obtained in the fourth step, and the resulting mixture is subjected to a wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.
摘要:
The invention provides a dispersion of particles of rutile titanium oxide wherein the particles of rutile titanium oxide have a D50 in a range of 1 to 15 nm and a D90 of 40 nm or less in particle size distribution as determined by a dynamic light scattering method; a specific surface area in a range of 120 to 180 m2/g as determined by a BET method; and a rate of weight loss of 5% or less as obtained by heating the particles of rutile titanium oxide from 105° C. to 900° C.Such a dispersion of particles of rutile titanium oxide is obtained by a process according to the invention, which comprises: a first step in which an aqueous titanium tetrachloride solution is heated and hydrolyzed to obtain a slurry containing the precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water; a fifth step in which an acid is added to the slurry obtained in the fourth step, and the resulting mixture is subjected to a wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.
摘要:
The invention provides a process for producing an aqueous dispersion of particles of rutile titanium oxide, which comprises: a first step in which after a chloride ion concentration of an aqueous solution of titanium tetrachloride is adjusted to 0.5 mole/L or more and less than 4.4 mole/L, the aqueous solution of titanium tetrachloride is heated at a temperature in a range of from 25° C. to 75° C. to hydrolyze the titanium tetrachloride, thereby obtaining a slurry containing the thus precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a fifth step in which an acid is added to the slurry obtained in the fourth step to deflocculate the slurry, and the resulting slurry is subjected to wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.
摘要:
An internal combustion engine includes: a cylinder block having a block cooling water passage that supplies cooling water to a plurality of cylinder bores, and an inter-bore cooling water passage provided between cylinder bores that supplies cooling water between the cylinder bores; a cylinder head having a first cooling water passage to which cooling water is supplied from the block cooling water passage, and a second cooling water passage, which is provided independently from the first cooling water passage, and to which cooling water is supplied from the inter-bore cooling water passage; a heat exchanger; a first cooling water introducing part that leads cooling water, which is flown out from the first cooling water passage, to the heat exchanger; and a second cooling water introducing part that leads cooling water, which is flown out from the second cooling water passage, to a downstream side of the heat exchanger.
摘要:
A rod locking apparatus with a simple structure and outstanding operability for facilitating rod locking and a camera stand with such a rod locking apparatus. The rod locking apparatus comprises an insertion hole formed in the main body, through which the rod is inserted, a space formed in the main body in such a manner that it intersects with the insertion hole, with a communicating hole that communicates with the insertion hole, an eccentrically rotating shaft inserted in the space with an external locking hand grip provided thereon and an elastic member provided on the external circumference of the eccentrically rotating shaft. This allows the rod to be easily locked and released. Also a camera stand comprising a slide track, a slider device mounted on the slide track in such a manner that it can freely slide a rod on which the slider device is mounted and a camera mounting platform mounted on the rod further provided with the rod locking apparatus described above wherein the position of the camera mounted on the camera mounting platform can be easily adjusted and locked into place.
摘要:
An internal combustion engine includes: a cylinder block having a block cooling water passage that supplies cooling water to a plurality of cylinder bores, and an inter-bore cooling water passage provided between cylinder bores that supplies cooling water between the cylinder bores; a cylinder head having a first cooling water passage to which cooling water is supplied from the block cooling water passage, and a second cooling water passage, which is provided independently from the first cooling water passage, and to which cooling water is supplied from the inter-bore cooling water passage; a heat exchanger; a first cooling water introducing part that leads cooling water, which is flown out from the first cooling water passage, to the heat exchanger; and a second cooling water introducing part that leads cooling water, which is flown out from the second cooling water passage, to a downstream side of the heat exchanger.
摘要:
An automatic answering telephone set comprises a voice synthesizing unit and a voice detector for reproducing a recorded message in response to a remote control performed by using a predetermined password number. A plurality of decoy numerals are inserted immediately before each of numerals constituting the preestablished password number to thereby form a pseudo-password number including the decoy numerals. A calling party is inquired of with the pseudo-password number. An input password number is then formed in accordance with replies of the calling party as detected by the voice detector. Only when coincidence is found between the predetermined password number and the input numerical password, the remote control is accepted.