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    Isolation of 1,5-dinitroanthraquinone
    3.
    发明授权
    Isolation of 1,5-dinitroanthraquinone 失效
    1,5-二硝基蒽醌的分离

    公开(公告)号：US3929841A

    公开(公告)日：1975-12-30

    申请号：US48521374

    申请日：1974-07-02

    Applicant: BASF AG

    Inventor： ACKERMANN OTTO ,  EILINGSFELD HEINZ

    IPC: C07C205/47 ,  C07C67/00 ,  C07C201/00 ,  D07B3/04 ,  C09B1/00

    CPC classification number: D07B3/04 ,  C07C201/08 ,  C07C201/16 ,  C07C2603/24 ,  C07C205/47

    Abstract: 1,5-DINITROANTHRAQUINONE IS ISOLATED FROM A NITRATION MIXTURE CONTAINING DINITROANTHRAQUINONES BY ALLOWING N-methylpyrrolidone to act on the nitroanthraquinone mixture. From 10 to 45% by weight of the nitroanthraquinone mixture remains undissolved and the undissolved material is separated from the solution. A dinitroanthraquinone is isolated which contains from 75 to 95% by weight of 1,5-dinitroanthraquinone and practically no Beta dinitroanthraquinones.

    Abstract translation: 通过允许N-甲基吡咯烷酮作用于硝基蒽醌混合物，从含有四氮杂环戊烷的硝化混合物中分离出1,5-四硝基四氢喹啉。 10至45重量％的硝基蒽醌混合物保持未溶解，并且将未溶解的材料与溶液分离。 分离出二硝基蒽醌，其含有75至95重量％的1,5-二硝基蒽醌，实际上不含β-二硝基蒽醌。

    Production of pure 1-nitroanthraquinone
    4.
    发明授权
    Production of pure 1-nitroanthraquinone 失效
    纯1-硝基四氢呋喃的生产

    公开(公告)号：US3868395A

    公开(公告)日：1975-02-25

    申请号：US37313173

    申请日：1973-06-25

    Applicant: BASF AG

    Inventor： BANTEL KARL-HEINZ ,  EILINGSFELD HEINZ

    IPC: C07C69/73 ,  C07C20060101 ,  C07C67/00 ,  C07C201/00 ,  C07C205/47 ,  C09B1/00

    Abstract: Production of pure 1-nitroanthraquinone from nitroanthraquinone mixtures by treating the mixture in an organic aprotic solvent with a primary or secondary amine or a mixture of the same. A pure 1-nitroanthraquinone in which practically no dinitroanthraquinone or other byproducts can be detected is obtained in a high yield. The 1-aminoanthraquinone obtained from this 1-nitroanthraquinone is suitable for all dye syntheses.

    Abstract translation: 通过在有机非质子溶剂中用伯或仲胺或其混合物处理混合物，从硝基蒽醌混合物中制备纯的1-硝基蒽醌。 以高产率获得实际上不能检测到二硝基蒽醌或其它副产物的纯的1-硝基蒽醌。 从该1-硝基蒽醌得到的1-氨基蒽醌适用于所有染料合成。

    Recovery of purified 1-nitroanthraquinone
    6.
    发明授权
    Recovery of purified 1-nitroanthraquinone 失效
    回收纯化的1-硝基蒽醌

    公开(公告)号：US3923845A

    公开(公告)日：1975-12-02

    申请号：US38483473

    申请日：1973-08-02

    Applicant: BASF AG

    Inventor： BANTEL KARL-HEINZ ,  EILINGSFELD HEINZ ,  STOECKELMANN GUENTER

    IPC: C07C205/47 ,  C07C20060101 ,  C07C67/00 ,  C07C201/00 ,  C07C79/37

    CPC classification number: C07C201/16 ,  C07C205/47

    Abstract: A process for the recovery of 1-nitroanthraquinone in a purified state from a nitroanthraquinone mixture containing it by treatment with a base in the presence of an initiator such as nitrite, halide, thiocyanate, alcoholate or phenolate ions in an organic solvent. A 1-nitroanthraquinone is obtained which is essentially pure or contains only small quantities of isomers and dinitroanthraquinones.

    Abstract translation: 通过在有机溶剂中在引发剂如亚硝酸盐，卤化物，硫氰酸盐，醇化物或酚盐离子存在下用碱处理，从含有它的硝基蒽醌混合物中回收纯化状态的1-硝基蒽醌的方法。 得到基本上纯的或仅含有少量异构体和二硝基蒽醌的1-硝基蒽醌。

    Production of aromatic ketones
    7.
    发明授权
    Production of aromatic ketones 失效
    生产芳香酮

    公开(公告)号：US3907837A

    公开(公告)日：1975-09-23

    申请号：US32220673

    申请日：1973-01-09

    Applicant: BASF AG

    Inventor： EFFENBERGER FRANZ ,  BANTEL KARL-HEINZ ,  EILINGSFELD HEINZ

    IPC: C07C49/76 ,  C07C205/48 ,  C07C49/68 ,  C07C49/80 ,  C07C49/84

    CPC classification number: C07C205/45 ,  C07C45/46 ,  C07C201/12 ,  C07C205/48 ,  C07C49/786 ,  C07C49/784 ,  C07C49/84

    Abstract: A method of preparing aromatic ketones by reaction of aromatic compounds with acyl chlorides or acyl anhydrides in the presence of catalytic amounts of an aromatic polynitrosulfonic acid, and new aromatic ketones derived from an aromatic compound (as the acylatable compound) having at least two nuclear substituents, at least one of said substituents being a nitro group. Both the known and the new aromatic ketones obtainable are valuable intermediates for the production of dyes and pesticides.

    Abstract translation: 在催化量的芳族多硝基磺酸存在下，通过芳族化合物与酰基氯或酰基酸酐反应制备芳族酮的方法，以及衍生自具有至少两个核取代基的芳族化合物（作为可酰化化合物）的新芳香族酮 ，所述取代基中的至少一个为硝基。 可获得的已知和新的芳族酮都可用于生产染料和农药的有价值的中间体。

    Production of pure 1-nitroanthraquinone
    8.
    发明授权
    Production of pure 1-nitroanthraquinone 失效
    纯1-硝基四氢呋喃的生产

    公开(公告)号：US3904659A

    公开(公告)日：1975-09-09

    申请号：US41036773

    申请日：1973-10-29

    Applicant: BASF AG

    Inventor： BANTEL KARL-HEINZ ,  EILINGSFELD HEINZ

    IPC: C07C205/47 ,  C07C67/00 ,  C07C201/00 ,  C07C79/37

    Abstract: A process for the production of pure 1-nitroanthraquinone from a mixture of nitroanthraquinone by treating the mixture in an organic polar aprotic solvent in the presence of an initiator such as a compound yielding nitrite, halide, thiocyanate, alcoholate or phenolate ions with a compound which has at least one -CH2- group activated by one or more carbonyl groups. 1-NITROANTHRAQUINONE WHICH IS VIRTUALLY PURE OR ONLY CONTAINS VERY SMALL AMOUNTS OF ISOMERS AND DINITROANTHRAQUINONES IS OBTAINED IN GOOD TO VERY GOOD YIELDS BY THE PROCESS OF THE INVENTION.

    Certain pyrimidine-containing dyestuffs
    9.
    发明授权
    Certain pyrimidine-containing dyestuffs 失效
    某些含嘧啶的染料

    公开(公告)号：US3862944A

    公开(公告)日：1975-01-28

    申请号：US25203172

    申请日：1972-05-10

    Applicant: BASF AG

    Inventor： EILINGSFELD HEINZ ,  SCHWANTJE GERD

    IPC: C09B5/16 ,  C07D51/46

    CPC classification number: C09B5/16

    Abstract: New dyes of the formula:

    IN WHICH TWO OF THE GROUPS X are hydroxyl and the third X is unsubstituted or substituted alkylamino, unsubstituted or substituted phenylamino, phenylthio, aliphatic, cycloaliphatic or aromatic acylamino or N''-alkylureido for dyeing synthetic material. Dyeings obtained therewith have good fastness properties. The invention relates to new dyes based on anthrapyrimidines for synthetic fibers.

    Abstract translation: 新染料的配方：

    Production of 2 4-disubstituted triazines
    10.
    发明授权
    Production of 2 4-disubstituted triazines 失效
    生产2个4分离的TRIAZINES

    公开(公告)号：US3629254A

    公开(公告)日：1971-12-21

    申请号：US3629254D

    申请日：1969-04-04

    Applicant: BASF AG

    Inventor： EILINGSFELD HEINZ ,  SCHEUERMANN HORST

    IPC: C07D55/50

    CPC classification number: C07D251/46

    Abstract: THE PRODUCTION OF 2,4-DISUBSTITUTED TRIAZINES BY REACTION OF SUBSTITUTED THIOBUIURETS WITH ESTERS OF FORMIMIDIC ACID. THE PRODUCTS OF THE PROCESS ARE VALUABLE STARTING MATERIALS FOR THE PRODUCTION OF DYES AND PESTICIDES.

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