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公开(公告)号：US20230312367A1
公开(公告)日：2023-10-05
申请号：US18041254
申请日：2021-08-03
Applicant: BASF SE
Inventor： Benjamin Johannes Herbert BERGNER , Thorsten BEIERLING
CPC classification number: C01G53/006 , C01G53/04 , C01P2002/72 , C01P2002/60 , C01P2004/50 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/40
Abstract: Disclosed herein is a process for precipitating a mixed hydroxide of TM where TM includes Ni, at least one of Co and Mn, and, optionally, one of Al, Mg, Zr or Ti from an aqueous solution of salts of such transition metals or of Al or of Mg. The process is carried out in a stirred vessel and includes the step of introducing a 10 to 40% by weight aqueous solution of ammonia and an aqueous solution of transition metal salts through at least two inlets into the stirred vessel. An aqueous solution of alkali metal hydroxide is added separately from the at least two inlets.
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公开(公告)号：US20250042769A1
公开(公告)日：2025-02-06
申请号：US18719035
申请日：2023-01-06
Applicant: BASF SE
Inventor： Thorsten BEIERLING , Simon SCHROEDLE , Thomas Michael RYLL
Abstract: Disclosed herein is a method for making a particulate (oxy)hydroxide of TM, where TM is a combination of nickel and at least one metal selected from Co and Mn, the process including: (a) providing an aqueous solution (α) containing water-soluble salts of Ni and of at least one transition metal selected from Co and Mn, (b) combining a solution (α) and a solution (β) and, if applicable, a solution (γ) at a pH value in a range of from 12.0 to 13.0 determined at 23° C. in a continuous stirred tank reactor, thereby creating a slurry of solid particles of a hydroxide containing nickel, and (c) transferring slurry from step (b) into a batch-wise operated stirred tank reactor where a solution (α) and a solution (β) and optionally a solution (γ) are combined with the slurry at a pH value in a range of from 11.0 to 12.0 determined at 23° C.
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公开(公告)号：US20240132372A1
公开(公告)日：2024-04-25
申请号：US18548011
申请日：2022-03-04
Applicant: BASF SE
Inventor： Thorsten BEIERLING , Rafael Benjamin BERK , Lukas Karl METZGER
IPC: C01G53/00
CPC classification number: C01G53/42 , C01P2004/03 , C01P2006/12 , C01P2006/82
Abstract: Disclosed herein is a process for making a particulate (oxy)hydroxide, carbonate, or oxide of TM which includes nickel and at least one metal selected from the group consisting of cobalt, manganese, and aluminum. The process includes providing an aqueous solution (α1) containing a water-soluble salt of Ni, one of an aqueous solution (α2) containing a water-soluble salt of Co, an aqueous solution (α3) containing a water-soluble salt of Mn, or an aqueous solution (α4) containing a water-soluble compound of Al, an aqueous solution (β) containing an alkali metal hydroxide or carbonate and, optionally, an aqueous solution (γ) containing ammonia or an organic acid or its alkali metal salt, combining solution (α1) and solution (β) and at least one of solutions (α2), (α3), (α4), and, if applicable, solution (γ), in different locations of a continuous reactor, and removing the particles from the liquid by a solid-liquid separation method.
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公开(公告)号：US20240228323A9
公开(公告)日：2024-07-11
申请号：US18548011
申请日：2022-03-04
Applicant: BASF SE
Inventor： Thorsten BEIERLING , Rafael Benjamin BERK , Lukas Karl METZGER
IPC: C01G53/00
CPC classification number: C01G53/42 , C01P2004/03 , C01P2006/12 , C01P2006/82
Abstract: Disclosed herein is a process for making a particulate (oxy)hydroxide, carbonate, or oxide of TM which includes nickel and at least one metal selected from the group consisting of cobalt, manganese, and aluminum. The process includes providing an aqueous solution (α1) containing a water-soluble salt of Ni, one of an aqueous solution (α2) containing a water-soluble salt of Co, an aqueous solution (α3) containing a water-soluble salt of Mn, or an aqueous solution (α4) containing a water-soluble compound of Al, an aqueous solution (β) containing an alkali metal hydroxide or carbonate and, optionally, an aqueous solution (γ) containing ammonia or an organic acid or its alkali metal salt, combining solution (α1) and solution (β) and at least one of solutions (α2), (α3), (α4), and, if applicable, solution (γ), in different locations of a continuous reactor, and removing the particles from the liquid by a solid-liquid separation method.
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公开(公告)号：US20230212028A1
公开(公告)日：2023-07-06
申请号：US17999057
申请日：2021-05-28
Applicant: BASF SE
Inventor： Benjamin Johannes Herbert BERGNER , Thorsten BEIERLING
IPC: C01G53/00
CPC classification number: C01G53/40 , C01P2002/52 , C01P2004/61 , C01P2004/84 , C01P2006/40 , C01P2004/03
Abstract: Process for making a particulate (oxy)hydroxide of TM wherein TM comprises nickel and where-in said process comprises the steps of: (a) Providing an aqueous solution (α) containing water-soluble salts of Ni and of at least one transition metal selected from Co and Mn, and, optionally, at least one further metal sel-ected from Ti, Zr, Mo, W, Al, Mg, Nb, and Ta, and an aqueous solution (β) containing an alkali metal hydroxide and, optionally, an aqueous solution (γ) containing ammonia, (b) combining a solution (α) and a solution (β) and, if applicable, a solution (γ) at a pH value in the range of from 12.0 to 13.0 in a stirred tank reactor, thereby creating solid particles of a hydroxide containing nickel, said solid particles being slurried, (c) transferring said slurry into another stirred tank reactor and combining it with a solution (α) and a solution (β) and, if applicable, a solution (γ) at a pH value in the range of from 11.0 to 12.7 and at conditions wherein the solubility of nickel is higher than in step (b), wherein the stirring speed is reduced in the course of step (c).
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Patent Agency Ranking
公开(公告)号：US20210024371A1
公开(公告)日：2021-01-28
申请号：US17041789
申请日：2019-03-21
Applicant: BASF SE
Inventor： Christian RIEMANN , Thorsten BEIERLING , Matthias RAULS
Abstract: Process for precipitating a carbonate or (oxy)hydroxide comprising nickel from an aqueous solution of a nickel salt wherein such process is carried out in a vessel comprising (A) a vessel body, (B) one or more elements that control the hydraulic flow of the slurry formed during the precipitation and that induce a loop-type circulation flow, and (C) a stirrer whose stirrer element is in the vessel but located separately from the element(s) (B).
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公开(公告)号：US20240425385A1
公开(公告)日：2024-12-26
申请号：US18570726
申请日：2022-07-12
Applicant: BASF SE
Inventor： Thorsten BEIERLING , Sabine FRISCHHUT , Matthias RAULS , Lukas Karl METZGER , Sabine WEIGUNY , Michael LENNARTZ , Rafael Benjamin BERK
IPC: C01G53/00
Abstract: Disclosed herein is a process for making a particulate (oxy)hydroxide of TM, where TM represents a combination of metals and includes nickel and at least one metal selected from cobalt and aluminum and manganese. The process includes: (a) combining an aqueous slurry of metallic nickel and at least one metal selected from aluminum and transition metals other than nickel with an oxidant selected from oxygen and nitrate in a first reaction vessel or in a first group of reaction vessels at a temperature of from 5° to 40° C., (b) transferring aqueous reaction medium from the first reaction vessel to a second reaction vessel, where the second reaction vessel contains a slurry of a hydroxide of TM, (c) removing the particles from step (b) from the liquid by a solid-liquid separation method, and drying the particles, and (d) returning liquid phase obtained in step (c) to the first reaction vessel.
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公开(公告)号：US20240351912A1
公开(公告)日：2024-10-24
申请号：US18683954
申请日：2022-09-12
Applicant: BASF SE
Inventor： Sabine FRISCHHUT , Thorsten BEIERLING , Lukas Karl METZGER , Matthias RAULS , Marc DUCHARDT
CPC classification number: C01G53/42 , C01G53/04 , C01G53/40 , H01M4/525 , C01P2002/52 , C01P2006/40 , H01M2004/028
Abstract: Disclosed herein is a process for making a particulate (oxy)hydroxide of TM, where TM represents metals and includes nickel and at least one metal selected from cobalt and aluminum and manganese. The process includes the steps of:
(a) combining an aqueous slurry of metallic nickel and at least one metal selected from cobalt and manganese and aluminum with an oxidant selected from nitrate and peroxide in a reaction vessel under an atmosphere with less than 100 ppm O2, thereby obtaining an aqueous reaction medium with a pH value in the range of from 7.5 to 12 containing particles,
(b) removing the particles from step (a) from the liquid by a solid-liquid separation method, and drying the particles, and
(c) returning mother liquor obtained in step (b) to the reaction vessel.-
公开(公告)号：US20240110747A1
公开(公告)日：2024-04-04
申请号：US18256081
申请日：2021-12-10
Applicant: BASF SE
Inventor： Timo HENSLER , Andreas Michael KERN , Raquel FIZ GONZALEZ , Thorsten BEIERLING
Abstract: Disclosed herein is a process for removing water from a particulate material selected from (oxy)hydroxides and carbonates containing at least one of nickel cobalt, and at least one metal other than nickel. The process includes the step of introducing at least one particulate material with a water content in the range of from 1 to 30% by weight, referring to said particulate material, into a rotary kiln with external heating elements and moving it through the rotary kiln together with a flow of a gas. The residual moisture of the resultant product is in the range of from 50 ppm to 1.5% by weight.
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公开(公告)号：US20240166532A1
公开(公告)日：2024-05-23
申请号：US18550378
申请日：2022-03-21
Applicant: BASF SE
IPC: C01G53/00 , H01M4/505 , H01M4/525 , H01M10/0525
CPC classification number: C01G53/44 , C01G53/006 , C01G53/66 , H01M4/505 , H01M4/525 , H01M10/0525 , C01P2002/60 , C01P2004/53 , C01P2006/12 , C01P2006/40
Abstract: Disclosed herein is a process for making a particulate oxyhydroxide or oxide of TM with a bimodal particles diameter distribution where TM represents metals, and where TM includes nickel and at least one metal is selected from the group consisting of cobalt and manganese.
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