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公开(公告)号：US09631035B2
公开(公告)日：2017-04-25
申请号：US15101351
申请日：2014-12-03
发明人： Georg Groos , Erich Neumann , Michael Deuerling , Dieter Littmann
IPC分类号： C08F2/00 , C08F4/00 , C08F210/00 , B01J10/00 , B01J19/18 , C08F6/12 , C08F6/00 , C08F6/10 , C08J11/02 , C08F2/01 , C08F2/02 , C08F2/34
CPC分类号： C08F6/12 , C08F2/01 , C08F2/02 , C08F2/34 , C08F6/001 , C08F6/10 , C08J11/02 , Y02P20/582 , C08L23/04 , C08F10/02 , C08F2/00 , C08F110/02 , C08F210/16 , C08F2500/08
摘要： The present disclosure relates to a process for separating polymeric and gaseous components of a reaction mixture obtained by high-pressure polymerization of ethylenically unsaturated monomers in the presence of free-radical polymerization initiators into in a gaseous fraction and a liquid fraction, wherein the separation is carried out at a pressure of from 15 MPa to 50 MPa and a temperature of from 120° C. to 300° C. in a separation vessel which has a vertically arranged cylindrical shape with a ratio of length to diameter L/D of from 4 to 10 and which is equipped with an inlet pipe which extends vertically from the top into the separation vessel; and the ratio of the inner diameter of the inlet pipe at its lower end and the inner diameter of the separating vessel in its cylindrical part is in the range of from 0.2 to 0.4.
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2.发明申请VESSEL FOR SEPARATING COMPONENTS OF A REACTION MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS WITH INTEGRATED BURSTING DISCS 有权用于分离由具有整体冲击盘的乙烯基不饱和单体的高压聚合获得的反应混合物的组分的容器公开(公告)号：US20160319046A1
公开(公告)日：2016-11-03
申请号：US15106150
申请日：2014-12-15
发明人： Erich Neumann , Danir Khayrullin , Claudio Fibla
CPC分类号： C08F6/10 , B01D19/0036 , B01D19/0063 , B01J3/002 , B01J19/2415 , B01J2219/185 , B01J2219/1943 , B01J2219/1946 , C08F10/02 , Y02P20/582
摘要： The present disclosure relates to a vessel for separating, at a pressure of from 10 MPa to 50 MPa, a composition comprising liquid components and gaseous components into a liquid fraction and a gaseous fraction, whereinthe separation vessel has a vertically arranged cylindrical shape,has at its top a manhole, which is surrounded by a thickened part of the separation vessel wall;and bears at least one bursting disc which is held by a bursting disc holder which is installed pressure-tight within a boring in the thickened part of the separation vessel wall.
摘要翻译： 并具有至少一个爆破盘，其由爆破盘保持器保持，破裂盘保持器在分离容器壁的加厚部分的镗孔内压力安装。
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3.发明申请公开(公告)号：US20160304631A1
公开(公告)日：2016-10-20
申请号：US15101372
申请日：2014-12-03
IPC分类号： C08F6/10 , G01F23/288 , C08F6/12
CPC分类号： C08F6/10 , B01J4/002 , C08F6/001 , C08F6/12 , C08F10/02 , G01F23/2885 , C08L23/04 , C08F2/00
摘要： The present disclosure generally relates to a process for separating polymeric and gaseous components of a reaction mixture obtained by high-pressure polymerization of ethylenically unsaturated monomers in the presence of free-radical polymerization initiators into a gaseous fraction and a liquid fraction in a separation vessel, wherein the filling level of the liquid fraction in the separation vessel is measured by a radiometric level measurement system comprising at least two radioactive sources and at least three radiation detectors, and the filling level is controlled by a product discharge valve which operates based on data coming from the level measurement system.
摘要翻译： 本发明一般涉及通过烯键式不饱和单体在自由基聚合引发剂存在下高压聚合得到的反应混合物中的聚合物和气态组分分离成气态馏分和分离容器中的液体馏分的方法， 其中分离容器中的液体部分的填充水平由包括至少两个放射源和至少三个辐射检测器的辐射测量水平测量系统测量，并且填充水平由产品排放阀控制，该产品排出阀基于数据来进行操作 从水平测量系统。
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公开(公告)号：US09637568B2
公开(公告)日：2017-05-02
申请号：US15101372
申请日：2014-12-03
IPC分类号： C08F2/00 , C08F4/00 , C08F210/00 , B01J10/00 , B01J19/18 , C08F6/10 , C08F6/00 , C08F6/12 , G01F23/288 , C08F10/02 , B01J4/00
CPC分类号： C08F6/10 , B01J4/002 , C08F6/001 , C08F6/12 , C08F10/02 , G01F23/2885 , C08L23/04 , C08F2/00
摘要： The present disclosure generally relates to a process for separating polymeric and gaseous components of a reaction mixture obtained by high-pressure polymerization of ethylenically unsaturated monomers in the presence of free-radical polymerization initiators into a gaseous fraction and a liquid fraction in a separation vessel, wherein the filling level of the liquid fraction in the separation vessel is measured by a radiometric level measurement system comprising at least two radioactive sources and at least three radiation detectors, and the filling level is controlled by a product discharge valve which operates based on data coming from the level measurement system.
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5.发明授权Process for separating vinyl esters from a gas stream comprising ethylene and vinyl esters 有权从包含乙烯和乙烯基酯的气流中分离乙烯基酯的方法公开(公告)号：US09272979B2
公开(公告)日：2016-03-01
申请号：US14654100
申请日：2013-12-16
发明人： Erich Neumann , Christoph Wolf , Dieter Littmann
IPC分类号： C08F2/00 , C08F4/00 , C08F118/02 , C07C67/48 , C07C67/52 , C08F210/02
CPC分类号： C07C67/52 , C08F210/02 , Y02P20/582 , C08F2/00 , C08F218/08 , C07C69/15
摘要： A process for separating esters of vinyl alcohol from a gas stream comprising from 70 to 99.5% by weight of ethylene and from 0.5 to 30% by weight of esters of vinyl alcohol being at a pressure in the range of from 0.5 MPa to 10 MPa and a temperature in the range of from 5° C. to 50° C.; and a process for copolymerizing ethylene and esters of vinyl alcohol in the presence of free-radical polymerization initiators at pressures in the range of from 110 MPa to 500 MPa and temperatures in the range of from 100° C. to 350° C. in a continuously operated polymerization apparatus comprising such a process for separating esters of vinyl alcohol from a gas stream comprising from 70 to 99.5% by weight of ethylene and from 0.5 to 30% by weight of esters of vinyl alcohol.
摘要翻译： 一种从气流中分离乙烯醇的酯的方法，包括70至99.5重量％的乙烯和0.5至30重量％的乙烯醇的酯在0.5MPa至10MPa的压力范围内，以及 温度范围为5℃至50℃; 以及在自由基聚合引发剂的存在下，在110MPa至500MPa的压力和100℃至350℃的温度范围内，乙烯醇的乙烯和酯的共聚合方法， 连续操作的聚合装置包括这样一种从含有70-99.5％（重量）乙烯和0.5-30％（重量）乙烯醇酯的气流中分离乙烯醇酯的方法。
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6.发明申请PROCESS FOR SEPARATING VINYL ESTERS FROM A GAS STREAM COMPRISING ETHYLENE AND VINYL ESTERS 有权从包含乙烯和乙烯酯的气流分离乙烯醇的方法公开(公告)号：US20150315119A1
公开(公告)日：2015-11-05
申请号：US14654100
申请日：2013-12-16
发明人： Erich Neumann , Christoph Wolf , Dieter Littmann
IPC分类号： C07C67/52 , C08F210/02
CPC分类号： C07C67/52 , C08F210/02 , Y02P20/582 , C08F2/00 , C08F218/08 , C07C69/15
摘要： Process for separating esters of vinyl alcohol from a gas stream comprising from 70 to 99.5% by weight of ethylene and from 0.5 to 30% by weight of esters of vinyl alcohol being at a pressure in the range of from 0.5 MPa to 10 MPa and a temperature in the range of from 5° C. to 50° C. comprising the steps of a) cooling the gas stream in a first heat exchanger by means of a cooling medium to a temperature of from −5° C. to 40° C.; b) withdrawing the not condensed part of the gas stream from the first heat exchanger and transferring it to a second heat exchanger; c) cooling the gas stream in the second heat exchanger to a temperature of from −20° C. to 5° C.; d) withdrawing the not condensed part of the gas stream from the second heat exchanger, reducing the pressure of the gas stream to from 0.5 MPa to 3 MPa and transferring it to a separation vessel; e) withdrawing the not condensed part of the gas stream from the separation vessel and transferring it as cooling medium to the second heat exchanger; and f) withdrawing the cooling medium as ethylene gas stream with a reduced content of esters of vinyl alcohol from the second heat exchanger, and process for copolymerizing ethylene and esters of vinyl alcohol in the presence of free-radical polymerization initiators at pressures in the range of from 110 MPa to 500 MPa and temperatures in the range of from 100° C. to 350° C. in a continuously operated polymerization apparatus comprising such a process for separating esters of vinyl alcohol from a gas stream comprising from 70 to 99.5% by weight of ethylene and from 0.5 to 30% by weight of esters of vinyl alcohol.
摘要翻译： 从乙烯醇的70〜99.5重量％的乙烯和0.5〜30重量％的乙烯醇的酯在0.5MPa〜10MPa的压力范围内分离乙烯醇的酯的方法， 温度在5℃至50℃的范围内，包括以下步骤：a）通过冷却介质将第一热交换器中的气流冷却至-5℃至40℃的温度 。 b）从第一热交换器中取出气流的未冷凝部分并将其转移到第二热交换器; c）将第二热交换器中的气流冷却至-20℃至5℃的温度; d）从第二热交换器中取出气流的未冷凝部分，将气流的压力降至0.5MPa至3MPa并将其转移至分离容器; e）从分离容器中取出气流的未冷凝部分并将其作为冷却介质转移到第二热交换器; 以及f）将来自第二热交换器的乙烯醇酯含量降低的乙烯气流作为乙烯气流取出，以及在自由基聚合引发剂的存在下在乙烯醇的存在下共聚乙烯醇和乙烯醇酯的方法， 在连续操作的聚合装置中，从110MPa到500MPa的温度和在100℃至350℃的温度范围内，包括这样一种将乙烯醇的酯从气流中分离的方法，该气流包含70-99.5％的 乙烯重量和0.5至30％重量的乙烯醇酯。
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公开(公告)号：US12110349B2
公开(公告)日：2024-10-08
申请号：US17312288
申请日：2019-12-16
发明人： Dieter Littmann , Andre-Armand Finette , Christoph Wolf , Michael Deuerling , Juergen Mohrbutter , Danir Khayrullin , Giulia Mei , Erich Neumann
CPC分类号： C08F10/02 , B01J3/002 , B01J3/02 , B01J19/002 , B01J19/2415 , C08F2/01 , B01J2219/00033 , B01J2219/00162 , B01J2219/0027 , C08F2/02 , C08F2400/04
摘要： A process for polymerizing ethylene in a high-pressure polymerization system having a continuously operated polymerization reactor and a reactor blow down system having an emergency valve, a reactor blow down vessel containing an aqueous medium and a reactor blow down dump vessel, wherein the process includes the steps of monitoring the polymerization system for a disturbance, opening the emergency valve when a disturbance occurs to allow the content of the polymerization system to expand into the reactor blow down vessel, contacting the content of the polymerization system in the reactor blow down vessel with the aqueous medium to obtain an aqueous polymer slurry, separating the polymer slurry and gaseous components, and transferring the polymer slurry to the reactor blow down dump vessel.
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公开(公告)号：US20220106418A1
公开(公告)日：2022-04-07
申请号：US17312288
申请日：2019-12-16
发明人： Dieter Littmann , Andre-Armand Finette , Christoph Wolf , Michael Deuerling , Juergen Mohrbutter , Danir Khayrullin , Giulia Mei , Erich Neumann
摘要： A process for polymerizing ethylene in a high-pressure polymerization system having a continuously operated polymerization reactor and a reactor blow down system having an emergency valve, a reactor blow down vessel containing an aqueous medium and a reactor blow down dump vessel, wherein the process includes the steps of monitoring the polymerization system for a disturbance, opening the emergency valve when a disturbance occurs to allow the content of the polymerization system to expand into the reactor blow down vessel, contacting the content of the polymerization system in the reactor blow down vessel with the aqueous medium to obtain an aqueous polymer slurry, separating the polymer slurry and gaseous components, and transferring the polymer slurry to the reactor blow down dump vessel.
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公开(公告)号：US09637569B2
公开(公告)日：2017-05-02
申请号：US15106150
申请日：2014-12-15
发明人： Erich Neumann , Danir Khayrullin , Claudio Fibla
IPC分类号： C08F2/00 , C08F4/00 , C08F210/00 , B01J10/00 , B01J19/18 , C08F6/10 , B01J3/00 , B01D19/00 , B01J19/24 , C08F10/02
CPC分类号： C08F6/10 , B01D19/0036 , B01D19/0063 , B01J3/002 , B01J19/2415 , B01J2219/185 , B01J2219/1943 , B01J2219/1946 , C08F10/02 , Y02P20/582
摘要： The present disclosure relates to a vessel for separating, at a pressure of from 10 MPa to 50 MPa, a composition comprising liquid components and gaseous components into a liquid fraction and a gaseous fraction, wherein the separation vessel has a vertically arranged cylindrical shape, has at its top a manhole, which is surrounded by a thickened by a part of the separation vessel wall; and bears at least one bursting disc which is held by a bursting disc holder which is installed pressure-tight within a boring in the thickened part of the separation vessel wall.
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10.发明申请PROCESS FOR SEPARATING COMPONENTS OF A REACTION MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS 有权用于分离由乙烯基不饱和单体的高压聚合获得的反应混合物组分的方法公开(公告)号：US20160311939A1
公开(公告)日：2016-10-27
申请号：US15101351
申请日：2014-12-03
发明人： Georg Groos , Erich Neumann , Michael Deuerling , Dieter Littmann
CPC分类号： C08F6/12 , C08F2/01 , C08F2/02 , C08F2/34 , C08F6/001 , C08F6/10 , C08J11/02 , Y02P20/582 , C08L23/04 , C08F10/02 , C08F2/00 , C08F110/02 , C08F210/16 , C08F2500/08
摘要： The present disclosure relates to a process for separating polymeric and gaseous components of a reaction mixture obtained by high-pressure polymerization of ethylenically unsaturated monomers in the presence of free-radical polymerization initiators into in a gaseous fraction and a liquid fraction, wherein the separation is carried out at a pressure of from 15 MPa to 50 MPa and a temperature of from 120° C. to 300° C. in a separation vessel which has a vertically arranged cylindrical shape with a ratio of length to diameter L/D of from 4 to 10 and which is equipped with an inlet pipe which extends vertically from the top into the separation vessel; and the ratio of the inner diameter of the inlet pipe at its lower end and the inner diameter of the separating vessel in its cylindrical part is in the range of from 0.2 to 0.4.
摘要翻译： 本公开内容涉及通过在自由基聚合引发剂存在下将烯键式不饱和单体高压聚合得到的反应混合物中的聚合物和气态组分分离成气态馏分和液体馏分的方法，其中分离 在具有垂直排列的圆柱形状的分离容器中，在15MPa至50MPa的压力和120℃至300℃的温度下进行，长度与直径L / D的比率为4 至10，并且其具有从顶部垂直延伸到分离容器中的入口管; 并且其下端的入口管的内径与其圆柱形部分中的分离容器的内径的比率在0.2至0.4的范围内。
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