Abstract:
An exhaust system for an implement, especially hedge clippers, trimmers, brush cutters, chain saws and the like, driven by an internal combustion engine, comprising an exhaust pipe for receiving exhaust gas from the engine, wherein the exhaust pipe has an outlet end opening out into the atmosphere, and a circumferentially extending condensate-guiding element disposed on the internal wall of the exhaust pipe, wherein the condensate-guiding element narrows the flow cross-section of the exhaust pipe.
Abstract:
In a method for introducing a sample into a graphite tube in flameless atomic absorption spectroscopy a lamella- or crucible-like sample carrier is introduced into the graphite tube from the end face in axial direction. Drying and ashing of the sample is effected outside the graphite tube. The sample carrier may be heated indirectly by radiation or directly by electric current being passed therethrough.
Abstract:
The control apparatus controls the lowering motion of an aspirator tube into a sample vessel in an automatic sample dispenser in a manner such that the smallest possible portion of an external surface of the aspirator tube is wetted by a liquid present in the sample vessel. A servo drive lowers the aspirator tube into the sample vessel. A sensor arrangement containing a single light guide, a light transmitter and a photoelectric receiver is associated with the aspirator tube and responds to light reflections at the liquid surface upon immersion of the lower aspirator tube end into the liquid. The light guide guides the propagating light beam and a returning reflected light beam. An electronic control controls the advancement of the aspirator tube via the servo drive into a position in which a predetermined short length in the region of the lower aspirator tube end dips into the liquid. When the liquid level drops due to aspiration of liquid into the aspirator tube, the lower end of the latter follows just this drop of the liquid level so that the aspirator tube continuously remains immersed into the liquid but only with the short length at its lower end.
Abstract:
In an atomic absorption spectrometer, a burner 16 for atomizing a sample is movable between a first and a second position. In the first position, the "cloud of atoms" is formed in the area of the housing-fixed measuring light beam 14. In the second position, it is formed outside the measuring light beam. The measurement is made in the first position whereby the utilization of the energy of the measuring light beam is optimal. A drift compensation is made in the second position to take care of variations of the lamp intensity and of the detector sensitivity.
Abstract:
The present application is directed to new and improved apparatus for use in analytical instruments which includes an elongated dosing tube having a tip at one end which is constructed and arranged to move between a sample vessel, a rinsing vessel and an analytical instrument; the other end of the dosing tube being connected in fluid flow communication to a rinsing liquid supply vessel through a sample pump assembly and a rinsing liquid pump assembly; the liquid pump assembly including a pump cylinder having an inlet and an outlet; a pump piston arranged for reciprocal movement in the pump cylinder between a first end position in the discharge direction and an opposite second end position in the intake direction; a first check valve mounted on the inlet of the pump cylinder and a second check valve mounted on the outlet of the pump cylinder; a seal mounted adjacent the outlet which cooperates with the pump piston to sealingly close the outlet when the pump piston is positioned in its first end position in the discharged direction.
Abstract:
Disclosed are methods and apparatus for concentrating a looked-for element from a solution for flameless atomic absorption spectroscopy. The tip of an electrode is dipped into a sample vessel containing the solution and an electric current is passed through the electrode and solution to electrodeposit the components of the solution on the electrode. The electrode with the electrodeposition is removed from the sample vessel and inserted into the graphite tube. The tube is then heated and the sample components electrodeposited on the electrode are atomized for analysis by the measuring beam of the atomic absorption spectrometer.
Abstract:
Disclosed is an apparatus and method for using same for atomic absorption determination of volatile, thermally decomposable compounds. The test sample is converted to a gaseous sample in a reaction vessel with an inert gas atmosphere. The gaseous sample in the inert gas is then introduced into a heatable measuring cell arranged in the ray path of an atomic absorption spectrometer. To further assist decomposition, the inert gas is heated prior to entering the measuring cell.
Abstract:
A storage rack having a shelf with storage spaces, arranged over top of each other, for pallets that are horizontally removed sideways. A rack operating device moves the pallets from the spaces, and a station cart forms a lowermost space for a pallet, and can be horizontally moved from the rack on first rails. An upper cart is located above the station cart and forms another one of the spaces to receive a pallet and is horizontally movable on second rails that have a wider track than the first rails and also lead out of the rack. The upper cart has a greater clearance in an area of the station cart which is larger than a length of the pallet, and runs on the second rails, and parts of the upper cart not related to the support structure thereof can be inserted between the vertical rack supports of the rack.
Abstract:
For analyzing solid substances on mercury by measuring the atomic absorption, the substance is heated in order to expel the mercury. The generated mercury vapor is conveyed with a carrier gas flow over a body having a large surface made of an amalgam-generating material, so that the mercury vapor bonds and is accumulated as amalgam on the surface of this body. Subsequently, the body is heated in order to set the mercury accumulated as amalgam free again, and is conveyed by a carrier gas flow into a measuring vessel of an atomic absorption spectrometer. The solid substance which is to be analyzed is enclosed within a vessel having a closure which is destroyed during the heating of the solid substance. For this purpose, a cover is sealingly placed onto the vessel above the destructable closure through which cover a carrier gas flow can be supplied and be carried off. Subsequently, the heating of the solid substance takes place with the closure being destroyed, and then the generated mercury vapor being passed by the carrier gas flow over the amalgam-generating body.
Abstract:
In a device for supplying liquid to an atomization device operating with a nebulizer (22) in a spectrometer, the liquid is fed to the nebulizer (22) by a peristaltic pump (10) through a supply conduit (12). A valve (18) responding to liquid pressure is arranged closely in front of the nebulizer (22) and controls a connection between the supply conduit (12) and an outlet (30) through which excess liquid can flow off. A sensor (44) responding to the opening of the valve (18) is adapted to control the speed of the peristaltic pump (10), such that the quantity fed by the peristaltic pump (10) is slightly larger than the feeding capacity of the nebulizer (22).