PROCESS FOR FLUORINATION USING 1,1,2,2-TETRAFLUOROETHYL-N,N-DIMETHYLAMINE
    7.
    发明申请
    PROCESS FOR FLUORINATION USING 1,1,2,2-TETRAFLUOROETHYL-N,N-DIMETHYLAMINE 审中-公开
    使用1,1,2,2-四氟乙基-N,N-二甲基胺进行氟化的方法

    公开(公告)号:US20090030246A1

    公开(公告)日:2009-01-29

    申请号:US12178873

    申请日:2008-07-24

    IPC分类号: C07C17/26

    摘要: A process for making a fluorinated product comprising contacting an alcohol with 1,1,2,2-tetrafluoroethyl-N,N-dimethylamine to produce a product mixture containing the fluorinated product and N,N-dimethyl difluoroacetamide, quenching the product mixture in water to form a first organic phase and an aqueous phase, recovering fluorinated product by separating the first organic phase from the aqueous phase, treating the aqueous phase to recover N,N-dimethyl difluoroacetamide, and converting recovered N,N-dimethyl difluoroacetamide to 1,1,2,2-tetrafluoroethyl-N,N-dimethylamine.

    摘要翻译: 一种制备氟化产物的方法,包括使醇与1,1,2,2-四氟乙基-N,N-二甲基胺接触以制备含有氟化产物和N,N-二甲基二氟乙酰胺的产物混合物,在水中淬灭产物混合物 形成第一有机相和水相,通过从水相中分离第一有机相回收氟化产物,处理水相以回收N,N-二甲基二氟乙酰胺,并将回收的N,N-二甲基二氟乙酰胺转化为1, 1,2,2-四氟乙基-N,N-二甲胺。

    Method for the application of active materials onto a surface and devices made with such methods
    8.
    发明授权
    Method for the application of active materials onto a surface and devices made with such methods 有权
    将活性物质施用到表面上的方法和用这种方法制造的装置

    公开(公告)号:US08465850B2

    公开(公告)日:2013-06-18

    申请号:US13080317

    申请日:2011-04-05

    摘要: The invention provides methods for the application of active materials onto active surfaces useful in organic electronic devices. The methods of the invention include selecting a liquid composition including an active material and a suitable liquid medium whereby when the liquid composition is deposited on the desired active surface it has no greater than about a 40° contact angle; treating the active surface to raise its surface tension before the deposition of a liquid composition containing the desired active material is deposited thereon; and combination thereof. The invention also provides organic electronic devices having at least two active layers, wherein at least one active layer comprises an active material that was deposited using at least one practice of the method of the invention.

    摘要翻译: 本发明提供了将活性材料应用于可用于有机电子器件的有源表面上的方法。 本发明的方法包括选择包括活性材料和合适液体介质的液体组合物,由此当液体组合物沉积在所需活性表面上时,其具有不大于约40°的接触角; 在沉积含有所需活性材料的液体组合物之前,处理活性表面以提高其表面张力; 及其组合。 本发明还提供了具有至少两个活性层的有机电子器件,其中至少一个活性层包含使用本发明方法的至少一种实践沉积的活性材料。