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    Process for producing 2,3,5-trichloropyridine
    2.
    发明授权
    Process for producing 2,3,5-trichloropyridine 失效
    制备2,3,5-三氯吡啶的方法

    公开(公告)号：US4258194A

    公开(公告)日：1981-03-24

    申请号：US74216

    申请日：1979-09-10

    Applicant: Claus D. Weis ,  Peter Sutter

    Inventor： Claus D. Weis ,  Peter Sutter

    IPC: C07D213/61 ,  C07F9/40 ,  C07D213/02

    CPC classification number: C07D213/61 ,  C07F9/4075

    Abstract: A novel process for producing 2,3,5-trichloropyridine is described. In this process, 2,3,4,5-tetrachloropyridine is reacted, in an alkanephosphonic acid dialkyl ester (dialkyl alkane phosphonate) having 1 to 4 carbon atoms in each of the alkyl groups or in a phosphoric acid trialkyl ester (trialkyl phosphate) having 1 to 4 carbon atoms in each of the alkyl groups as the solvent, at 60.degree. to 120.degree. C., in the presence of 1.4 to 2.8 mols, per mol of 2,3,4,5-tetrachloropyridine, of an ammonium salt of an inorganic or organic acid, with 1.2 to 1.6 gram atoms of zinc per mol of 2,3,4,5-tetrachloropyridine, the 2,3,4,5-tetrachloropyridine being selectively dechlorinated in the 4-position.2,3,5-Trichloropyridine is a valuable intermediate for producing herbicidally effective .alpha.-[4-(3',5'-dichloropyrid-2-yloxy)-phenoxy-]-alkanecarboxylic acids and derivatives thereof.There are also described novel ammonium salts of methanephosphonic acid monomethyl ester, in the presence of which salts the selective dechlorination of 2,3,4,5-tetrachloropyridine in the 4-position is advantageously performed.

    Abstract translation: 描述了一种制备2,3,5-三氯吡啶的新方法。 在该方法中，2,3,4,5-四氯吡啶在各烷基中的烷基膦酸二烷基酯（具有1至4个碳原子的二烷基烷烃膦酸酯）或磷酸三烷基酯（磷酸三烷基酯）中反应， 在每个烷基中作为溶剂具有1至4个碳原子，在60至120℃下，在1.4至2.8摩尔存在下，每摩尔2,3,4,5-四氯吡啶，铵 无机或有机酸的盐，每摩尔2,3,4,5-四氯吡啶为1.2-1.6克原子锌，2,3,4,5-四氯吡啶在4位选择性脱氯。 2,3,5-三氯吡啶是产生除草有效的α-[4-（3'，5'-二氯吡啶-2-基氧基） - 苯氧基] - 烷羧酸及其衍生物的有价值的中间体。 还描述了甲基膦酸单甲酯的新型铵盐，在其存在下，有利地进行4位的2,3,4,5-四氯吡啶的选择性脱氯。

    Process for the preparation of alkali metal salts of phosphonic acid monoalkyl esters
    3.
    发明授权
    Process for the preparation of alkali metal salts of phosphonic acid monoalkyl esters 失效
    制备膦酸单烷基酯的碱金属盐的方法

    公开(公告)号：US4950819A

    公开(公告)日：1990-08-21

    申请号：US245489

    申请日：1988-09-19

    Applicant: Claus D. Weis ,  Peter Sutter

    Inventor： Claus D. Weis ,  Peter Sutter

    IPC: C07F9/40

    CPC classification number: C07F9/4075

    Abstract: A process for the preparation of alkali metal salts of phosphonic acid monoalkyl esters of formula ##STR1## by reacting 1 mole of a phosphonic acid ester of formula ##STR2## with 1 mole of a finely particulate alkali metal halide of formula XY. In these formulae, R is straight chain or branched C.sub.1 -C.sub.20 alkyl, R.sub.1 is C.sub.1 -C.sub.4 alkyl, X is an alkali metal cation and Y is a halogen anion.

    Abstract translation: 通过使1摩尔式（IMAGE）（2）的膦酸酯与1摩尔的细颗粒的碱金属卤化物反应制备式（1）的膦酸单烷基酯的碱金属盐的方法， 公式XY。 在这些式中，R是直链或支链C 1 -C 20烷基，R 1是C 1 -C 4烷基，X是碱金属阳离子，Y是卤素阴离子。

    Benzanthrone lactones
    5.
    发明授权
    Benzanthrone lactones 失效
    苯甲酮内酯

    公开(公告)号：US4740604A

    公开(公告)日：1988-04-26

    申请号：US49915

    申请日：1987-05-15

    Applicant: Claus D. Weis ,  Peter Sutter

    Inventor： Claus D. Weis ,  Peter Sutter

    IPC: C09B3/06 ,  C07C59/84 ,  C07C59/88 ,  C07C59/90 ,  C07D307/77 ,  C09B29/36

    CPC classification number: C07D307/77 ,  C07C59/84 ,  C07C59/88 ,  C07C59/90 ,  C09B29/36

    Abstract: There are disclosed benzanthrone lactones of formula ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are as defined in claim 1. The benzanthrone lactones of formula (1) are important intermediates for the synthesis of novel dyes which are obtained by coupling suitable diazo components to said compounds of formula (1).

    Abstract translation: 公开了式（1）所示的苯酮酮内酯，其中R 1，R 2和R 3如权利要求1中所定义。式（1）的苯醌酮内酯是合成新染料的重要中间体，其通过偶合合适的重氮 所述式（1）化合物的组分。

    Preparation of dyed plastics or polymeric dye particles
    6.
    发明授权
    Preparation of dyed plastics or polymeric dye particles 失效
    染色塑料或聚合染料颗粒的制备

    公开(公告)号：US06923836B2

    公开(公告)日：2005-08-02

    申请号：US10451172

    申请日：2001-12-13

    Applicant: Rainer Hildebrand ,  Peter Sutter

    Inventor： Rainer Hildebrand ,  Peter Sutter

    IPC: C07D221/18 ,  C08J3/20 ,  C08K5/3437 ,  C08K5/36 ,  C08L101/00 ,  C09B5/34

    CPC classification number: C09B5/347 ,  C08K5/3437

    Abstract: The present application relates to a process for preparing dyed plastics or polymeric dye particles characterized in that it comprises mixing a high molecular weight organic material with a coloristically effective amount of at least one dye of the formula where R1 is hydrogen, hydroxyl or a radical —NHCO—R6, where R6 is C1-C6alkyl or unsubstituted or C1-C4alkyl- or halogen-substituted phenyl, R2 is hydrogen, hydroxyl or a radical W—R7, where W is —NHCO— or —S— and R7 is C1-C6alkyl or unsubstituted or C1-C4alkyl- or halogen-substituted phenyl, R3 is hydrogen, R4 is hydrogen or hydroxyl, R5 is hydrogen, or R3 and R4 combine to form the radical of the formula, where the rings A and B may independently bear further substituents.

    Abstract translation: 本发明涉及一种制备染色塑料或聚合染料颗粒的方法，其特征在于其包括将高分子量有机材料与有色度有效量的至少一种下式的染料混合：其中R 1， 是氢，羟基或基团-NHCO-R 6，其中R 6是C 1 -C 6 - 烷基或未取代的或C 1 -C 4烷基或卤素取代的苯基，R 2是氢，羟基或基团WR

    Fast-writable and precision-writable high-capacity optical storage media
    8.
    发明授权
    Fast-writable and precision-writable high-capacity optical storage media 失效
    快速写入和精确写入的大容量光存储介质

    公开(公告)号：US06849315B2

    公开(公告)日：2005-02-01

    申请号：US10483130

    申请日：2002-07-04

    Applicant: Urs Lehmann ,  Peter Aeschlimann ,  Peter Sutter ,  Beat Schmidhalter ,  Jean-Luc Budry ,  Heinz Spahni

    Inventor： Urs Lehmann ,  Peter Aeschlimann ,  Peter Sutter ,  Beat Schmidhalter ,  Jean-Luc Budry ,  Heinz Spahni

    IPC: B41M5/26 ,  C09B11/00 ,  C09B11/02 ,  C09B11/20 ,  C09B11/28 ,  C09B45/14 ,  C09B45/20 ,  C09B55/00 ,  C09B69/02 ,  G11B7/004 ,  G11B7/24 ,  G11B7/244 ,  G11B7/246 ,  G11B7/2467 ,  G11B7/249 ,  G11B7/253 ,  G11B7/254 ,  G11B7/2542 ,  G11B7/258 ,  G11B7/259 ,  G11B7/26 ,  B32B3/02

    CPC classification number: G11B7/244 ,  C09B11/28 ,  G11B7/2467 ,  G11B7/249 ,  G11B7/253 ,  G11B7/2542 ,  G11B7/259 ,  Y10T428/21

    Abstract: The invention relates to an optical recording medium, comprising a substrate and a recording layer, wherein the recording layer comprises a compound of formula (I), wherein R1, R2, R3, R4, R5, R6, R7, R8, R9, R10, R11, R12 and R13 are each independently of the others hydrogen, G1 or C1-C24alkyl, C2-C24alkenyl, C2-C24alkynyl, C3-C24cycloalkyl, C3-C24cycloalkenyl, C7-C24aralkyl, C6-C24aryl, C4-C12heteroaryl or C1-C12heterocycloalkyl, each unsubstituted or substituted by one or more identical or different substituents G1, wherein R1 and R2, R1 and R13, R2 and R3, R3 and R4, R4 and R5, R5 and R6, R6 and R7, R7 and R8, R8 and R9, R9 and R10, R10 and R11, R11 and R12 and/or R12 and R13 can independently of one another be bonded to one another in pairs separately or, when they contain substitutable sites, via a direct bond or via a —CH2—, —O—, —S—, —NH— or —NC1-C24alkyl-bridge in such a manner that, together with the atoms and bonds indicated in formula (I), five- or six-membered, saturated, unsaturated or aromatic, unsubstituted or G1-substituted rings are formed, G1 is any desired substituent,? xm- is an inorganic, organic organometallic anion, Yn+ is a proton or a metal, ammonium or phosphonium cation, and m and n are each independently of the other a number from 1 to 5, and p and q are each independently of the other O or a number from 0.2 to 6, the ratio of p and q to one another, depending upon m and n and, as applicable, the number of charged G1, being such that in formula (I) there is no excess positive or negative charge. Generally the optical recording medium according to the invention additionally comprises a reflecting layer. The recording media according to the invention exhibit high sensitivity and good playback characteristics, especially at high recording and playback speeds. The light stability is also excellent.

    Abstract translation: 本发明涉及一种光记录介质，包括基片和记录层，其中记录层包括式（I）化合物，其中R1，R2，R3，R4，R5，R6，R7，R8，R9，R10 ，R11，R12和R13各自独立地为氢，G1或C1-C24烷基，C2-C24链烯基，C2-C24炔基，C3-C24环烷基，C3-C24环烯基，C7-C24芳烷基，C6-C24芳基，C4-C12杂芳基或C1- C 1 -C 6杂环烷基，每个未取代或被一个或多个相同或不同的取代基G1取代，其中R1和R2，R1和R13，R2和R3，R3和R4，R4和R5，R5和R6，R6和R7，R7和R8，R8 并且R 9，R 9和R 10，R 10和R 11，R 11和R 12和/或R 12和R 13可以彼此独立地彼此相互键合，或者当它们含有可取代的位置时，经由直接键或通过-CH 2 - ，-O - ， - S - ， - NH-或-NCl-C24烷基 - 桥，其与式（I）中所示的原子和键一起为五或六元饱和， 形成不饱和或芳族，未取代或者G1取代的环，G1是a

    Azo dyes, processes for their preparation and their use
    9.
    发明授权
    Azo dyes, processes for their preparation and their use 失效
    偶氮染料，其制备方法及其用途

    公开(公告)号：US5650497A

    公开(公告)日：1997-07-22

    申请号：US679841

    申请日：1996-07-15

    Applicant: Jean-Marie Adam ,  Peter Sutter

    Inventor： Jean-Marie Adam ,  Peter Sutter

    IPC: C09B31/065 ,  C09B43/18 ,  C09B43/28 ,  C09B31/047 ,  D06P1/39 ,  D06P3/24

    CPC classification number: C09B31/065 ,  C09B43/18 ,  C09B43/28 ,  Y10S8/924

    Abstract: Azo dyes of the formula ##STR1## in which R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 independently of one another are hydrogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy or halogen,R.sub.6 is hydrogen or C.sub.1 -C.sub.4 Alkyl,X is --C.sub.1 -C.sub.4 alkylene-O--C.sub.1 -C.sub.4 alkyl andY is hydrogen; unsubstituted or hydroxy- or C.sub.1 -C.sub.4 alkoxy-substituted C.sub.1 -C.sub.8 alkyl, C.sub.2 -C.sub.4 -alkonoyl or C.sub.1 -C.sub.4 alkoxycarbonyl; a radical of the formula --CH.sub.2 --CH.dbd.CH.sub.2 ;C.sub.1 -C.sub.4 alkylsulfonyl; or unsubstituted or C.sub.1 -C.sub.4 alkyl-, C.sub.1 -C.sub.4 alkoxy- or halogen-substituted phenylsulfonyl, produce dyeings with good fastness properties on fibre materials containing nitrogen or containing hydroxyl groups.

    Abstract translation: 其中R 1，R 2，R 3，R 4和R 5彼此独立地是氢，C 1 -C 4烷基，C 1 -C 4烷氧基或卤素，R 6是氢或C 1 -C 4烷基， C1-C4亚烷基-O-C1-C4烷基，Y是氢; 未取代的或羟基或C 1 -C 4烷氧基取代的C 1 -C 8烷基，C 2 -C 4 - 烷酰基或C 1 -C 4烷氧基羰基; 式-CH 2 -CH = CH 2的基团; C 1 -C 4烷基磺酰基; 或未取代的或C 1 -C 4烷基 - ，C 1 -C 4烷氧基或卤素取代的苯基磺酰基，在含氮或含羟基的纤维材料上产生具有良好牢度性能的染色。

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