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公开(公告)号:US20200180971A1
公开(公告)日:2020-06-11
申请号:US16313510
申请日:2017-06-13
Applicant: DIC Corporation
Inventor: Kiyoo Kamei , Jian-Jun Yuan , Hitoshi Sekine , Hiroshi Kinoshita
Abstract: Provided is a metal oxide production apparatus that implements a flux evaporation method. The production apparatus includes a firing furnace configured to subject a metal compound to firing in the presence of flux, a cooling pipe connected to the firing furnace and configured to convert vaporized flux resulting from the firing into powder, and a recovery means configured to recover powdered flux converted in the cooling pipe. Furthermore, provided is a metal oxide production method comprising a step (1) of subjecting a metal compound to firing in the presence of flux and obtaining a metal oxide and vaporized flux, a step (2) of converting the vaporized flux into powder by cooling the vaporized flux, and a step (3) of recovering powdered flux resulting from the converting.
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公开(公告)号:US10113096B2
公开(公告)日:2018-10-30
申请号:US15030674
申请日:2014-10-07
Applicant: DIC Corporation
Inventor: Jian-Jun Yuan , Hiroshi Kinoshita
Abstract: The present invention provides a resin composition including aluminum oxide (A) containing molybdenum having a size on the order of μm or less and a resin (B); and a resin molded body formed by molding the resin composition. Also, the present invention provides a heat-dissipating material containing the resin composition; and a heat-dissipating member containing the resin molded body. The heat-dissipating member of the present invention can be used for electronic parts such as electronic devices, electric devices, OA devices or for LED illumination.
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公开(公告)号:US11642663B2
公开(公告)日:2023-05-09
申请号:US17024779
申请日:2020-09-18
Applicant: DIC Corporation
Inventor: Masato Otsu , Jian-Jun Yuan , Minoru Tabuchi , Kaori Kawamura , Naoto Sakurai , Koichiro Matsuki , Yuichi Satokawa
CPC classification number: B01J27/051 , B01J35/004 , B01J35/0013 , B01J35/1014 , B01J37/20 , C01B3/042 , C01G39/06 , C01P2002/72 , C01P2002/80 , C01P2004/03 , C01P2004/04 , C01P2004/30 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12
Abstract: Provided is a molybdenum sulfide that is ribbon-shaped and particularly suitable for a hydrogen generation catalyst. Disclosed are a ribbon-shaped molybdenum sulfide, in which 50 particles as measured by observation with a scanning electron microscope (SEM) have a shape of, on average, 500 to 10000 nm in length, 10 to 1000 nm in width, and 3 to 200 nm in thickness; a method for producing the ribbon-shaped molybdenum sulfide, including: (1) heating a molybdenum oxide at a temperature of 200 to 1000° C. in the presence of a sulfur source; or (2) heating a molybdenum oxide at a temperature of 100 to 800° C. in the absence of a sulfur source, and then heating the molybdenum oxide at a temperature of 200 to 1000° C. in the presence of a sulfur source; and a hydrogen generation catalyst including the ribbon-shaped molybdenum sulfide.
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公开(公告)号:US20200062607A1
公开(公告)日:2020-02-27
申请号:US16611621
申请日:2018-11-11
Applicant: DIC Corporation
Inventor: Kazuo Itoya , Masaki Iida , Jian-Jun Yuan , Yasuyo Yoshimoto , Hironobu Oki , Masamichi Hayashi
Abstract: A spinel compound oxide particle includes metallic atoms, aluminum atoms, oxygen atoms, and molybdenum atoms, wherein the metallic atoms are selected from the group consisting of zinc atoms, cobalt atoms, and strontium atoms, and a crystallite size in a [111] plane is 100 nm or more. Included are a step (1) of firing a first mixture including a molybdenum compound and a metallic-atom-containing compound or a first mixture including a molybdenum compound, a metallic-atom-containing compound, and an aluminum compound to prepare an intermediate; and a step (2) of firing, at a temperature higher than a temperature selected in the step (1), a second mixture including the intermediate or a second mixture including the intermediate and an aluminum compound.
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公开(公告)号:US11926531B2
公开(公告)日:2024-03-12
申请号:US17259932
申请日:2018-07-26
Applicant: DIC Corporation
Inventor: Shingo Takada , Kazuo Itoya , Jian-Jun Yuan , Takayuki Kanematsu , Masamichi Hayashi , Fumihiko Maekawa , Yoshiyuki Sano
CPC classification number: C01F7/442 , B22F1/05 , B22F9/30 , B32B5/30 , C04B35/185 , C04B35/65 , B22F2302/253 , B22F2302/256 , B22F2304/10 , B32B2255/04
Abstract: Flaky alumina particles including mullite in a surface layer of the flaky alumina particles. A method for producing flaky alumina particles including forming a mixture by mixing together an aluminum compound that contains elemental aluminum, a molybdenum compound that contains elemental molybdenum, and silicon or a silicon compound that contains elemental silicon, the aluminum compound being in an amount greater than or equal to 50 mass %, calculated as Al2O3, the molybdenum compound being in an amount less than or equal to 40 mass %, calculated as MoO3, the silicon or the silicon compound being in an amount of 0.5 mass % or greater and less than 10 mass %, calculated as SiO2, relative to a total mass of the flaky alumina particles taken as 100 mass %; and firing the mixture.
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公开(公告)号:US20210053037A1
公开(公告)日:2021-02-25
申请号:US17024779
申请日:2020-09-18
Applicant: DIC Corporation
Inventor: Masato Otsu , Jian-Jun Yuan , Minoru Tabuchi , Kaori Kawamura , Naoto Sakurai , Koichiro Matsuki , Yuichi Satokawa
Abstract: Provided is a molybdenum sulfide that is ribbon-shaped and particularly suitable for a hydrogen generation catalyst. Disclosed are a ribbon-shaped molybdenum sulfide, in which 50 particles as measured by observation with a scanning electron microscope (SEM) have a shape of, on average, 500 to 10000 nm in length, 10 to 1000 nm in width, and 3 to 200 nm in thickness; a method for producing the ribbon-shaped molybdenum sulfide, including: (1) heating a molybdenum oxide at a temperature of 200 to 1000° C. in the presence of a sulfur source; or (2) heating a molybdenum oxide at a temperature of 100 to 800° C. in the absence of a sulfur source, and then heating the molybdenum oxide at a temperature of 200 to 1000° C. in the presence of a sulfur source; and a hydrogen generation catalyst including the ribbon-shaped molybdenum sulfide.
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公开(公告)号:US11905420B2
公开(公告)日:2024-02-20
申请号:US17265354
申请日:2019-08-09
Applicant: DIC Corporation
Inventor: Shingo Takada , Hironobu Oki , Jian-Jun Yuan , Kazuo Itoya , Yoshiyuki Sano
CPC classification number: C09C1/407 , C09C3/063 , C01P2002/85 , C01P2004/03 , C01P2004/20 , C01P2004/54 , C01P2004/61 , C01P2004/84 , C01P2006/10
Abstract: To provide plate-like alumina particles that are less likely to wear apparatuses. Plate-like alumina particles containing germanium or a germanium compound. The plate-like alumina particles preferably have a molar ratio of Ge to Al, [Ge]/[Al], of 0.08 or more as determined in an XPS analysis. The plate-like alumina particles preferably contain the germanium or germanium compound in a surface layer. The plate-like alumina particles preferably have a density of 3.7 g/cm3 or more and 4.1 g/cm3 or less. The plate-like alumina particles preferably have a molar ratio of Ge to Al, [Ge]/[Al], of 0.08 or less as determined in an XRF analysis.
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公开(公告)号:US11279830B2
公开(公告)日:2022-03-22
申请号:US16334557
申请日:2017-09-21
Applicant: DIC Corporation
Inventor: Kazuo Itoya , Atsushi Oshio , Hironobu Oki , Masaki Iida , Yasuyo Sakamoto , Masamichi Hayashi , Takayuki Kanematsu , Fumihiko Maekawa , Jian-Jun Yuan , Hiroshi Kinoshita
Abstract: Provided is a surface-treated spinel particle (B) including a spinel particle (A) including a magnesium atom, an aluminum atom, and an oxygen atom and a surface treatment layer disposed at least a portion of the surface of the spinel particle (A). The surface treatment layer includes a surface-treating agent including an organic compound or a cured product of the surface-treating agent. The spinel particle (A) further includes molybdenum. The crystallite diameter of the [111] plane of the spinel particle (A) is 220 nm or more. Also provided are a method for producing the surface-treated spinel particle (B), a resin composition including the surface-treated spinel particle (B), and a molded article.
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公开(公告)号:US20210301144A1
公开(公告)日:2021-09-30
申请号:US17265354
申请日:2019-08-09
Applicant: DIC Corporation
Inventor: Shingo Takada , Hironobu Oki , Jian-Jun Yuan , Kazuo Itoya , Yoshiyuki Sano
Abstract: To provide plate-like alumina particles that are less likely to wear apparatuses. Plate-like alumina particles containing germanium or a germanium compound. The plate-like alumina particles preferably have a molar ratio of Ge to Al, [Ge]/[Al], of 0.08 or more as determined in an XPS analysis. The plate-like alumina particles preferably contain the germanium or germanium compound in a surface layer. The plate-like alumina particles preferably have a density of 3.7 g/cm3 or more and 4.1 g/cm3 or less. The plate-like alumina particles preferably have a molar ratio of Ge to Al, [Ge]/[Al], of 0.08 or less as determined in an XRF analysis.
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10.
公开(公告)号:US20210301143A1
公开(公告)日:2021-09-30
申请号:US16334557
申请日:2017-09-21
Applicant: DIC Corporation
Inventor: Kazuo Itoya , Atsushi Oshio , Hironobu Oki , Masaki Iida , Yasuyo Sakamoto , Masamichi Hayashi , Takayuki Kanematsu , Fumihiko Maekawa , Jian-Jun Yuan , Hiroshi Kinoshita
Abstract: Provided is a surface-treated spinel particle (B) including a spinel particle (A) including a magnesium atom, an aluminum atom, and an oxygen atom and a surface treatment layer disposed at least a portion of the surface of the spinel particle (A). The surface treatment layer includes a surface-treating agent including an organic compound or a cured product of the surface-treating agent. The spinel particle (A) further includes molybdenum. The crystallite diameter of the [111] plane of the spinel particle (A) is 220 nm or more. Also provided are a method for producing the surface-treated spinel particle (B), a resin composition including the surface-treated spinel particle (B), and a molded article.
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