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公开(公告)号：US07459138B2
公开(公告)日：2008-12-02
申请号：US10976216
申请日：2004-10-28
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B01J8/0055 , B01J8/388 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/843
摘要： A process and apparatus for catalytic production of single walled carbon nanotubes. Catalytic particles are exposed to different process conditions at successive stages wherein the catalytic particles do not come in contact with reactive (catalytic) gases until preferred process conditions have been attained, thereby controlling the quantity and form of carbon nanotubes produced. The reaction gas is preferably provided at a high space velocity to minimize CO2 build-up. The process also contemplates processes and apparatus which recycle and reuse the gases and catalytic particulate materials, thereby maximizing cost efficiency, reducing wastes, reducing the need for additional raw materials, and producing the carbon nanotubes, especially SWNTs, in greater quantities and for lower costs.
摘要翻译： 用于催化生产单壁碳纳米管的方法和装置。 催化颗粒在连续阶段暴露于不同的工艺条件，其中催化剂颗粒不与反应（催化）气体接触，直到获得优选的工艺条件，从而控制产生的碳纳米管的数量和形式。 优选以高空间速度提供反应气体以最小化CO 2积聚。 该方法还考虑了再循环和再利用气体和催化颗粒材料的方法和设备，从而最大限度地提高成本效率，减少废物，减少对额外原材料的需求，以及大量生产碳纳米管，特别是SWNT，并降低成本 。
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公开(公告)号：US06919064B2
公开(公告)日：2005-07-19
申请号：US09996142
申请日：2001-11-28
CPC分类号： B82Y30/00 , B01J8/0055 , B01J8/388 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/843
摘要： A process and apparatus for catalytic production of single walled carbon nanotubes. Catalytic particles are exposed to different process conditions at successive stages wherein the catalytic particles do not come in contact with reactive (catalytic) gases until preferred process conditions have been attained, thereby controlling the quantity and form of carbon nanotubes produced. The reaction gas is preferably provided at a high space velocity to minimize CO2 build-up. The process also contemplates processes and apparatus which recycle and reuse the gases and catalytic particulate materials, thereby maximizing cost efficiency, reducing wastes, reducing the need for additional raw materials, and producing the carbon nanotubes, especially SWNTs, in greater quantities and for lower costs.
摘要翻译： 用于催化生产单壁碳纳米管的方法和装置。 催化颗粒在连续阶段暴露于不同的工艺条件，其中催化剂颗粒不与反应（催化）气体接触，直到获得优选的工艺条件，从而控制产生的碳纳米管的数量和形式。 优选以高空间速度提供反应气体以最小化CO 2 2积聚。 该方法还考虑了再循环和再利用气体和催化颗粒材料的方法和设备，从而最大限度地提高成本效率，减少废物，减少对额外原材料的需求，以及大量生产碳纳米管，特别是SWNT，并降低成本 。
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公开(公告)号：US06413487B1
公开(公告)日：2002-07-02
申请号：US09587257
申请日：2000-06-02
IPC分类号： D01F912
CPC分类号： B01J8/388 , B01J8/0055 , B01J8/006 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/742 , Y10S977/75 , Y10S977/775 , Y10S977/842 , Y10S977/843 , Y10S977/845
摘要： A method and apparatus for catalytic production of carbon nanotubes. Catalytic particles are exposed to different process conditions at successive stages wherein the catalytic particles do not come in contact with reactive (catalytic) gases until preferred process conditions have been attained, thereby controlling the quantity and form of carbon nanotubes produced. The method also contemplates methods and apparatus which recycle and reuse the gases and catalytic particulate materials, thereby maximizing cost efficiency, reducing wastes, reducing the need for additional raw materials, and producing the carbon nanotubes, especially SWNTs, in greater quantities and for lower costs.
摘要翻译： 一种催化生产碳纳米管的方法和装置。 催化颗粒在连续阶段暴露于不同的工艺条件，其中催化剂颗粒不与反应（催化）气体接触，直到获得优选的工艺条件，从而控制产生的碳纳米管的数量和形式。 该方法还考虑了再循环和再利用气体和催化颗粒材料的方法和设备，从而最大限度地提高成本效率，减少废物，减少对额外原材料的需求，以及大量生产碳纳米管，特别是SWNTs，并降低成本 。
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公开(公告)号：US07585482B2
公开(公告)日：2009-09-08
申请号：US11251968
申请日：2005-10-17
IPC分类号： B82B3/00
CPC分类号： B01J8/388 , B01J8/0055 , B01J8/006 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/742 , Y10S977/75 , Y10S977/775 , Y10S977/842 , Y10S977/843 , Y10S977/845
摘要： A method of purifying a single-walled carbon nanotube catalytic product having the steps of providing a catalytic product including single-walled carbon nanotubes, and a Group VIII and/or Group VIb transition metal, exposing the catalytic product to a heated oxidative gas to provide a treated carbon nanotube product including single-walled carbon nanotubes and the Group VIII and/or Group VIb transition metal, and exposing the treated carbon nanotube product to an acid to separate the single-walled carbon nanotubes from the Group VIII and/or Group VIb transition metal. The catalytic product may include a support material and amorphous carbon.
摘要翻译： 一种纯化单壁碳纳米管催化剂产品的方法，其具有提供包括单壁碳纳米管的催化产物和VIII族和/或VIb族过渡金属的步骤，将催化产物暴露于加热的氧化气体中以提供 包括单壁碳纳米管和VIII族和/或VIb族过渡金属的经处理的碳纳米管产物，并将经处理的碳纳米管产物暴露于酸以将单壁碳纳米管与VIII族和/或VIb族分离 过渡金属。 催化产物可以包括载体材料和无定形碳。
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公开(公告)号：US06955800B2
公开(公告)日：2005-10-18
申请号：US10145193
申请日：2002-05-13
CPC分类号： B01J8/388 , B01J8/0055 , B01J8/006 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/742 , Y10S977/75 , Y10S977/775 , Y10S977/842 , Y10S977/843 , Y10S977/845
摘要： A method and apparatus for catalytic production of carbon nanotubes. Catalytic particles are exposed to different process conditions at successive stages wherein the catalytic particles do not come in contact with reactive (catalytic) gases until preferred process conditions have been attained, thereby controlling the quantity and form of carbon nanotubes produced. The method also contemplates methods and apparatus which recycle and reuse the gases and catalytic particulate materials, thereby maximizing cost efficiency, reducing wastes, reducing the need for additional raw materials, and producing the carbon nanotubes, especially SWNTs, in greater quantities and for lower costs.
摘要翻译： 一种催化生产碳纳米管的方法和装置。 催化颗粒在连续阶段暴露于不同的工艺条件，其中催化剂颗粒不与反应（催化）气体接触，直到获得优选的工艺条件，从而控制产生的碳纳米管的数量和形式。 该方法还考虑了再循环和再利用气体和催化颗粒材料的方法和设备，从而最大限度地提高成本效率，减少废物，减少对额外原材料的需求，以及大量生产碳纳米管，特别是SWNTs，并降低成本 。
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公开(公告)号：US20060039849A1
公开(公告)日：2006-02-23
申请号：US10976216
申请日：2004-10-28
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B01J8/0055 , B01J8/388 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/843
摘要： A process and apparatus for catalytic production of single walled carbon nanotubes. Catalytic particles are exposed to different process conditions at successive stages wherein the catalytic particles do not come in contact with reactive (catalytic) gases until preferred process conditions have been attained, thereby controlling the quantity and form of carbon nanotubes produced. The reaction gas is preferably provided at a high space velocity to minimize CO2 build-up. The process also contemplates processes and apparatus which recycle and reuse the gases and catalytic particulate materials, thereby maximizing cost efficiency, reducing wastes, reducing the need for additional raw materials, and producing the carbon nanotubes, especially SWNTs, in greater quantities and for lower costs.
摘要翻译： 用于催化生产单壁碳纳米管的方法和装置。 催化颗粒在连续阶段暴露于不同的工艺条件，其中催化剂颗粒不与反应（催化）气体接触，直到获得优选的工艺条件，从而控制产生的碳纳米管的数量和形式。 优选以高空间速度提供反应气体以最小化CO 2 2积聚。 该方法还考虑了再循环和再利用气体和催化颗粒材料的方法和设备，从而最大限度地提高成本效率，减少废物，减少对额外原材料的需求，以及大量生产碳纳米管，特别是SWNT，并降低成本 。
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公开(公告)号：US06333016B1
公开(公告)日：2001-12-25
申请号：US09389553
申请日：1999-09-03
IPC分类号： D01F9127
CPC分类号： B82Y15/00 , B01J21/185 , B01J23/85 , B01J23/88 , B01J23/882 , B01J23/888 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/127 , D01F9/1272 , D01F9/1278 , Y10S977/742 , Y10S977/75 , Y10S977/775 , Y10S977/813 , Y10S977/835 , Y10S977/842 , Y10S977/843 , Y10T428/2918
摘要： A method for producing carbon nanotubes by contacting a carbon containing gas with metallic catalytic particles. The catalytic particles contain at least one metal from Group VIII, including for example Co, Ni, Ru, Rh, Pd, Ir, and Pt, and at least one metal from Group VIb including for example Mo, W and Cr. The metal component may be deposited on a support. Preferably, a substantial percentage of the nanotubes formed are single-walled carbon nanotubes. Further, a method for determining catalyst composition and reaction conditions for optimizing production of single-walled carbon nanotubes is also disclosed.
摘要翻译： 一种通过使含碳气体与金属催化剂颗粒接触来制造碳纳米管的方法。 催化剂颗粒含有至少一种来自第VIII族的金属，包括例如Co，Ni，Ru，Rh，Pd，Ir和Pt，以及至少一种VIb族金属，包括例如Mo，W和Cr。 金属组分可以沉积在载体上。 优选地，形成的纳米管的大部分是单壁碳纳米管。 此外，还公开了用于确定用于优化单壁碳纳米管的生产的催化剂组成和反应条件的方法。
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公开(公告)号：US20050042162A1
公开(公告)日：2005-02-24
申请号：US09996142
申请日：2001-11-28
CPC分类号： B82Y30/00 , B01J8/0055 , B01J8/388 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/843
摘要： A process and apparatus for catalytic production of single walled carbon nanotubes. Catalytic particles are exposed to different process conditions at successive stages wherein the catalytic particles do not come in contact with reactive (catalytic) gases until preferred process conditions have been attained, thereby controlling the quantity and form of carbon nanotubes produced. The process also contemplates processes and apparatus which recycle and reuse-the gases and catalytic particulate materials, thereby maximizing cost efficiency, reducing wastes, reducing the need for additional raw materials, and producing the carbon nanotubes, especially SWNTs, in greater quantities and for lower costs.
摘要翻译： 用于催化生产单壁碳纳米管的方法和装置。 催化颗粒在连续阶段暴露于不同的工艺条件，其中催化剂颗粒不与反应（催化）气体接触，直到获得优选的工艺条件，从而控制产生的碳纳米管的数量和形式。 该方法还考虑了再循环和再利用的方法和装置 - 气体和催化颗粒材料，从而最大限度地提高成本效率，减少废物，减少对额外原材料的需求，以及大量生产碳纳米管，特别是SWNTs，并降低 费用
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公开(公告)号：US20080008644A1
公开(公告)日：2008-01-10
申请号：US11251968
申请日：2005-10-17
IPC分类号： D01F9/12
CPC分类号： B01J8/388 , B01J8/0055 , B01J8/006 , B01J38/12 , B01J38/60 , B01J38/64 , B01J2208/00292 , B82Y15/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/127 , D01F9/1271 , D01F9/1272 , D01F9/1278 , Y02P20/584 , Y10S977/742 , Y10S977/75 , Y10S977/775 , Y10S977/842 , Y10S977/843 , Y10S977/845
摘要： A method of purifying a single-walled carbon nanotube catalytic product having the steps of providing a catalytic product including single-walled carbon nanotubes, and a Group VIII and/or Group VIb transition metal, exposing the catalytic product to a heated oxidative gas to provide a treated carbon nanotube product including single-walled carbon nanotubes and the Group VIII and/or Group VIb transition metal, and exposing the treated carbon nanotube product to an acid to separate the single-walled carbon nanotubes from the Group VIII and/or Group VIb transition metal. The catalytic product may include a support material and amorphous carbon.
摘要翻译： 一种纯化单壁碳纳米管催化剂产品的方法，其具有提供包括单壁碳纳米管的催化产物和VIII族和/或VIb族过渡金属的步骤，将催化产物暴露于加热的氧化气体中以提供 包括单壁碳纳米管和VIII族和/或VIb族过渡金属的经处理的碳纳米管产物，并将经处理的碳纳米管产物暴露于酸以将单壁碳纳米管与VIII族和/或VIb族分离 过渡金属。 催化产物可以包括载体材料和无定形碳。
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公开(公告)号：US20080107588A1
公开(公告)日：2008-05-08
申请号：US11805917
申请日：2007-05-25
IPC分类号： D01F9/12
CPC分类号： B82Y15/00 , B01J21/185 , B01J23/85 , B01J23/88 , B01J23/882 , B01J23/888 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , D01F9/127 , D01F9/1272 , D01F9/1278 , Y10S977/742 , Y10S977/75 , Y10S977/775 , Y10S977/813 , Y10S977/835 , Y10S977/842 , Y10S977/843 , Y10T428/2918
摘要： A method of producing a carbon nanotube product comprising a catalytic particle and carbon nanotubes deposited thereon. The catalytic particles preferably contain Co or Ni metal from Group VIII, and Mo or W metal from Group VIb. The catalytic particle preferably comprises a support material upon which the metals are disposed. The carbon nanotube product is preferably formed by exposing the catalytic particle to a carbon-containing gas at a temperature sufficient to form the carbon nanotubes as a primary portion of a solid carbon product with minor amounts of graphite and amorphous carbon residue.
摘要翻译： 一种生产包含催化颗粒和沉积在其上的碳纳米管的碳纳米管产品的方法。 催化颗粒优选含有来自VIII族的Co或Ni金属，以及来自VIb族的Mo或W金属。 催化剂颗粒优选地包括在其上设置金属的载体材料。 碳纳米管产物优选通过在足以形成碳纳米管作为具有少量石墨和无定形碳残基的固体碳产物的主要部分的温度下将催化颗粒暴露于含碳气体中而形成。
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