摘要:
Particles of compound useful in imaging elements are milled using a milling media comprising a polymeric resin. The use of polymeric milling media permits the production of particles having an average particle size less than 1 micron. Further, the resulting particles are free from the contamination resulting from conventional milling media of, for example, glass, ceramic or steel.
摘要:
The present invention provides a photographic element comprises a support, at least one hydrophilic light-sensitive layer, and a light-insensitive layer containing a binder and polymer matte particles having the formula:(A).sub.x (B).sub.y (C).sub.z (I)where A is a monofunctional ethylenically unsaturated monomer which forms a homopolymer with a Tg less than 20.degree. C., B is a monofunctional ethylenically unsaturated monomer which forms a homopolymer with a Tg greater than 60.degree. C., C is a monomer with two or more ethylenically unsaturated groups, x is about 10 to 95 mole %, y is less than 85 mole %, and z is about 5 to 90 mole %.
摘要:
A limited coalescence method of making polymer particles having an average particle size of 3 .mu.m or less comprising dispersing the polymer particles in an organic liquid diluent after they are separated from the aqueous suspension medium in which they are prepared, to thereby eliminate or substantially avoid agglomeration between the polymer particles upon drying.
摘要:
This invention comprises thermally processable imaging element comprising: (a) a support, (b) a thermally processable imaging layer on one side of the support; and (c) a protective layer comprising a binder and matte particles comprising a crosslinked polymer, wherein the protective layer has been applied as a solution of binder and matte particles in a coating solvent in which the binder is soluble and the matte particles are swellable to the extent of about 160 to about 390%.
摘要:
A process for making an ink jet ink comprising: a) providing an organic pigment dispersion containing a pigment and a carrier; b) mixing the pigment dispersion with rigid milling media having an average size less than about 100 &mgr;m; c) introducing the mixture from step b) into a high speed mill; d) milling the mixture from step c) until a pigment particle size distribution is obtained wherein about 50% by weight of the pigment particles have a particle size less than about 100 nanometers; e) separating the milling media from the mixture milled in step d); and f) diluting the mixture from step d) to obtain the ink jet ink; wherein the milling media comprises negatively-charged polymeric beads which are crosslinked sufficiently to prevent swelling of the polymeric beads to levels greater than or equal to about 50 volume % within 4 hours at 25° C. in the carrier.
摘要:
A process of forming milled solid particles of a compound comprising milling solid particles of the compound in a liquid organic medium continuous phase in the presence of polymeric milling media to reduce the average size of the compound particles, wherein the liquid continuous phase comprises a solvent for the milling media polymer in the uncrosslinked form and the milling media is crosslinked sufficiently to prevent 50 vol. % swelling of the polymeric milling media in the liquid continuous phase within four hours at 25.degree. C. In various preferred embodiments of the invention, polymeric milling media having a mean particle size of less than about 100 .mu.m in the unswelled state (i.e., prior to addition to the liquid organic continuous phase) is used; the compound particles are milled to an average particle size of less than 100 nm; the compound comprises electrophotographic toner pigment; the liquid continuous phase comprises an ethylenically unsaturated polymerizable monomer; and the milling media polymer comprises polymerized styrene and divinylbenzene monomers. In an additional preferred embodiment of the invention wherein the compound comprises electrophotographic toner pigment and the liquid organic medium continuous phase comprises an ethylenically unsaturated polymerizable monomer, electrophotographic toner particles are formed by polymerizing the ethylenically unsaturated polymerizable monomer after the toner pigment compound is milled. It is a particularly advantageous feature of this invention that there is provided a method of preparing extremely fine solid particles of a compound free of unacceptable contamination and/or discoloration using polymeric milling media in a liquid continuous phase which is an effective solvent for the milling media polymer in uncrosslinked form. It is a further advantage of the invention to allow for preparing electrophotographic toner particles directly from a milled toner pigment particle dispersion without first needing to separate the milled particles from the liquid milling medium continuous phase. The ability to form extremely fine, e.g., less than 100 nm, size pigment particles in accordance with the invention is especially advantageous where toner particles are subsequently formed by suspension polymerization of ethylenically unsaturated monomers after milling of the pigment particles.
摘要:
A method for operating a navigation system computes a pedestrian route for travel by a pedestrian. A request to calculate the pedestrian route from an origin to a destination and a walking preference for the pedestrian route identifying a feature of the pedestrian route are obtained. A geographic database associated with the navigation system is accessed for data representing at least one pedestrian path. The data representing the pedestrian path includes lighting level attribute information for the pedestrian path. A valid solution pedestrian route from the origin to the destination comprising a series of connected pedestrian paths that support the walking preference is determined.
摘要:
The invention relates to an inkjet recording element that comprises, on a support, a porous hydrophilic image-receiving layer made by a subtractive method involving removal of water-insoluble polymeric latex from a coated non-porous layer to form the porous layer. Also disclosed is a method for making the inkjet recording element and a method of printing on such an inkjet recording
摘要:
A process for forming polymer particles with aligned pores and controlled narrow particle size distribution, including: a) forming an oil phase by dissolving a polymeric binder in a solvent; b) dispersing the oil phase into a water phase containing a controlled amount of particulate stabilizer and forming an oil-in-water emulsion of controlled narrow dispersed oil phase droplet size distribution; c) freezing the emulsion to freeze solvent in the oil droplets to form frozen solvent domains within the polymeric binder, and also the water in the continuous water phase; and d) removing the frozen solvent from the polymeric binder and the frozen water in the continuous water phase, thereby forming porous polymer particles of controlled narrow particle size distribution and containing directional aligned non-spherical pore structures. Optionally, the porous particles may contain encapsulated functional ingredients.
摘要:
The present invention is a method of manufacturing porous polymer particles comprising: forming a dispersion of porous polymer particles in an external aqueous phase, wherein individual porous particles each comprise a continuous polymer phase and internal pores containing an internal aqueous phase; and filtering the dispersion of porous polymer particles with a filter to remove the external aqueous phase, wherein the filtering is done while agitating the porous particles.