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1.发明授权Disperse monoazo dyestuffs derived from 3,5-dinitro-2-amino thiophene as disazo component and an arylamine coupling component 失效衍生自3,5-二硝基-2-氨基噻吩的分散单偶氮染料作为双偶氮组分和芳基胺偶联组分
公开(公告)号：US4211696A
公开(公告)日：1980-07-08
申请号：US656593
申请日：1976-02-09
IPC分类号： C07D333/38 , C07D333/44 , C09B29/00 , C09B29/06 , C09B29/08 , C09B29/36 , C09B29/26 , D06P1/18 , D06P3/54
CPC分类号： C07D333/38 , C07D333/44 , C09B29/0059 , C09B29/06 , C09B29/08 , C09B29/3695
摘要： Disperse monoazo dyestuffs, free from carboxylic and sulphonic acid groups, derived from 3,5-dinitro-2-amino thiophene as disazo component and an arylamine coupling component exhibit superior properties when used to give colorations to textile materials such as secondary cellulose acetate and cellulose triacetate, polyamide and aromatic polyester textile materials, said colorations having excellent fastness to light and to wet and dry heat treatments. The dyestuffs also have high tinctorial strength and excellent dyeing and build-up properties and produce depths of shade which are relatively independent of the dyebath pH, or the temperature of the dyebath or the liquor ratio of the dyebath.
摘要翻译： 衍生自3,5-二硝基-2-氨基噻吩作为双偶氮组分和芳基胺偶联组分的不含羧酸和磺酸基团的分散单偶氮染料在用于赋予织物材料如二乙酸纤维素和纤维素时显示出优异的性能 三醋酸酯，聚酰胺和芳族聚酯纺织材料，所述着色具有优异的耐光牢度和湿和干热处理。 染料也具有高的着色强度和优异的染色和聚集性能，并产生相对独立于染浴pH或染浴温度或染浴的浴比的色调深度。
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公开(公告)号：US4590308A
公开(公告)日：1986-05-20
申请号：US694161
申请日：1985-01-23
申请人： Alan T. Costello , David J. Milner
发明人： Alan T. Costello , David J. Milner
CPC分类号： C07C29/62
摘要： Process for the monohalogenation of a benzene compound which has 2 or 3 CH.sub.2 OH substituents to obtain a product wherein one of the CH.sub.2 OH substituents is monohalogenated which comprises reacting an aqueous solution of the compound with hydrochloric or hydrobromic acid in the presence of a water immiscible organic solvent which is inert to the reactants, the partition coefficient of the compound in the aqueous/organic phases being greater, with respect to the aqueous phase, than the partition coefficient of the product. The novel compounds4-chloromethyl-2,3,5,6-tetrafluorobenzene methanol and4-bromomethyl-2,3,5,6-tetrafluorobenzene methanol are also disclosed.
摘要翻译： 具有2或3个CH 2 OH取代基的苯化合物的单卤化方法，以获得其中一个CH 2 OH取代基被单卤代的产物，其中包括使化合物的水溶液与盐酸或氢溴酸在水不混溶的有机溶剂存在下反应 对反应物是惰性的，化合物在水相/有机相中的分配系数相对于水相比分配系数大。 还公开了新化合物4-氯甲基-2,3,5,6-四氟苯甲醇和4-溴甲基-2,3,5,6-四氟苯甲醇。
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公开(公告)号：US4236018A
公开(公告)日：1980-11-25
申请号：US56305
申请日：1979-07-10
IPC分类号： C07C69/747 , B01J27/00 , B01J27/02 , C07C51/00 , C07C51/06 , C07C61/40 , C07C67/00 , C07C67/20 , C07C67/22 , C07C69/743 , C07C231/00 , C07C231/06 , C07C233/58 , C07C61/16
CPC分类号： C07C51/06
摘要： 1-Cyano-3-[2',2'-(dihalogeno and/or trifluoromethyl)vinyl]-2,2-dimethylcyclopropanes are converted into the corresponding 1-amides and 1-carboxylic acids by reaction with sulphuric acid and water, or into the corresponding 1-carboxylic acid esters by reaction with sulphuric acid, water and a lower alkanol. High yields are obtained.
摘要翻译： 1-氰基-3- [2'，2' - （二卤代和/或三氟甲基）乙烯基] -2,2-二甲基环丙烷通过与硫酸和水反应转化为相应的1-酰胺和1-羧酸，或 通过与硫酸，水和低级链烷醇的反应转化为相应的1-羧酸酯。 获得高产率。
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4.发明授权Reactive dyestuffs containing chlorine or fluorine substituents and one or more pyridine radicals linked to the dyestuff at the 2-, 4- or 6-position 失效含有氯或氟取代基的反应性染料和一个或多个与2-，4-或6-位上的染料连接的吡啶基
公开(公告)号：US4213899A
公开(公告)日：1980-07-22
申请号：US886127
申请日：1978-03-13
摘要： A dyestuff of the formula ##STR1## where D is a chromophoric residuen is 1 or 2Z is ##STR2## where R is H, C.sub.1-4 alkyl, C.sub.1-4 alkyl substituted by OH, OSO.sub.3 H, CN or SO.sub.3 H or is phenyleach hal independently represents a chlorine or fluorine atom occupying one of the remaining 2-, 4- and 6-positions of the pyridine nucleusX is F, Cl, CN or NO.sub.2Y is H, F, Cl, CN or NO.sub.2.These dyestuffs reactively dye cellulose at low temperatures and are less prone to "acid bleeding" than some known reactive dyes.
摘要翻译： 其中D是发色团残基n的式[1]的染料是1或2，Z是
，其中R是H，C 1-4烷基，被OH，OSO 3 H，CN或SO 3 H取代的C 1-4烷基， 独立地表示占据吡啶核的剩余2-，4-和6-位之一的氯或氟原子，X是F，Cl，CN或NO 2，Y是H，F，Cl，CN或NO 2。 这些染料在低温下反应性地染色纤维素，并且比一些已知的活性染料更不易于“酸性渗色”。
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