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公开(公告)号：US08529684B2
公开(公告)日：2013-09-10
申请号：US13587433
申请日：2012-08-16
CPC分类号： A61B5/1172
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C3-C4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.
摘要翻译： 提供了一种用于将潜在生理学生物转化为可见生理生物学的方法和组合物，所述方法包括：提供设置在制品表面上的潜伏生物测定，其中所述生物测定包含至少一种衍生化合物; 使所述潜在生物测定与显影溶液接触，其中所述显影溶液包含至少一种选自茚三酮和1,8-二氮杂芴-9-酮的成像试剂和包含至少一种C 3 -C 4氢氟烃的载体溶剂; 并使所述成像试剂与所述外分泌衍生的化合物反应以产生可见的生理学生物学特征。
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公开(公告)号：US20090269478A1
公开(公告)日：2009-10-29
申请号：US12422260
申请日：2009-04-11
CPC分类号： A61B5/1172
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C3-C4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.
摘要翻译： 提供了一种用于将潜在生理学生物转化为可见生理生物学的方法和组合物，所述方法包括：提供设置在制品表面上的潜伏生物测定，其中所述生物测定包含至少一种衍生化合物; 使所述潜在生物测定与显影溶液接触，其中所述显影溶液包含至少一种选自茚三酮和1,8-二氮杂芴-9-酮的成像试剂和包含至少一种C 3 -C 4氢氟烃的载体溶剂; 并使所述成像试剂与所述外分泌衍生的化合物反应以产生可见的生理学生物学特征。
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公开(公告)号：US08268063B2
公开(公告)日：2012-09-18
申请号：US12422260
申请日：2009-04-11
IPC分类号： C09D11/00
CPC分类号： A61B5/1172
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C3-C4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.
摘要翻译： 提供了一种用于将潜在生理学生物转化为可见生理生物学的方法和组合物，所述方法包括：提供设置在制品表面上的潜伏生物测定，其中所述生物测定包含至少一种衍生化合物; 使所述潜在生物测定与显影溶液接触，其中所述显影溶液包含至少一种选自茚三酮和1,8-二氮杂芴-9-酮的成像试剂和包含至少一种C 3 -C 4氢氟烃的载体溶剂; 并使所述成像试剂与所述外分泌衍生的化合物反应以产生可见的生理学生物学特征。
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公开(公告)号：US06551469B1
公开(公告)日：2003-04-22
申请号：US09994438
申请日：2001-11-27
申请人： Haridasan K. Nair , Michael Van Der Puy , David Nalewajek , Timothy R. Demmin , Andrew J. Poss , David E. Bradley , Ian R. Shankland , Martin E. Cheney
发明人： Haridasan K. Nair , Michael Van Der Puy , David Nalewajek , Timothy R. Demmin , Andrew J. Poss , David E. Bradley , Ian R. Shankland , Martin E. Cheney
IPC分类号： C07C1700
摘要： A process for preparing 1-chloro-1,1,3,3,3-pentafluoropropane, CF3CH2CF2Cl, comprising contacting in a reaction zone in the substantial absence of oxygen, reactants comprising chlorine and 1,1,1,3,3-pentafluoropropane, CF3CH2CHF2 (also referred to as HFC-245fa), and subjecting the reactants to actinic radiation, such as UV light at about 2,000 to 4,000 Angstroms, wherein: (1) inert gas is present at a concentration equal to or less than about 5 wt. % of the total weight of reactants; (2) the molar ratio of chlorine to CF3CH2CHF2 is from about 0.2:1 to about 1.5:1; and (3) the concentration of chlorinated product produced having greater than one chlorine present in the molecule is less than or equal to about 10 wt. %.
摘要翻译： 制备1-氯-1,1,3,3,3-五氟丙烷CF 3 CH 2 CF 2 Cl的方法，包括在基本不存在氧的反应区中接触，包含氯的反应物和1,1,1,3,3-五氟丙烷 ，CF 3 CH 2 CHF 2（也称为HFC-245fa），并使反应物进行光化辐射，例如约2,000至4,000埃的紫外光，其中：（1）惰性气体的存在浓度等于或小于约5 重量 反应物总重量的百分比; （2）氯与CF 3 CH 2 CHF 2的摩尔比为约0.2:1至约1.5:1; 和（3）分子中存在的具有大于一个氯的氯化产物的浓度小于或等于约10wt。 ％。
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公开(公告)号：US06548719B1
公开(公告)日：2003-04-15
申请号：US09962974
申请日：2001-09-25
申请人： Haridasan K. Nair , Michael Van Der Puy , David Nalewajek , Timothy R. Demmin , Andrew J. Poss , David E. Bradley , Ian R. Shankland
发明人： Haridasan K. Nair , Michael Van Der Puy , David Nalewajek , Timothy R. Demmin , Andrew J. Poss , David E. Bradley , Ian R. Shankland
IPC分类号： C07C1725
摘要： A process for producing a fluoroolefin of the formula: CF3CY═CXnHp wherein Y is a hydrogen atom or a halogen atom (i.e., fluorine, chlorine, bromine or iodine); X is a hydrogen atom or a halogen atom (i.e., fluorine, chlorine, bromine or iodine); n and p are integers independently equal to 0, 1 or 2, provided that (n+p)=2; comprising contacting, in the presence of a phase transfer catalyst, a compound of the formula: CF3C(R1aR2b)C(R3cR4d), wherein R1, R2, R3, and R4 are independently a hydrogen atom or a halogen selected from the group consisting of fluorine, chlorine, bromine and iodine, provided that at least one of R1, R2, R3, and R4 is halogen and there is at least one hydrogen and one halogen on adjacent carbon atoms; a and b are independently=0, 1 or 2 and (a+b)=2; and c and d are independently=0, 1, 2 or 3 and (c+d)=3; and at least one alkali metal hydroxide. The alkali metal hydroxide can be, for example, potassium or sodium hydroxide and the phase transfer catalyst can be, for example, at least one: crown ether such as 18-crown-6 and 15-crown-5; or onium salt such as, quaternary phosphonium salt and quaternary ammonium salt. The olef in is useful, for example, as an intermediate for producing other industrial chemicals and as a monomer for producing oligomers and polymers.
摘要翻译： 制备下式的氟代烯烃的方法：CF 3 CY = CXnHp其中Y是氢原子或卤素原子（即氟，氯，溴或碘）; X是氢原子或卤素原子（即氟，氯，溴或碘）; n和p是独立地等于0,1或2的整数，条件是（n + p）= 2; 包括在相转移催化剂存在下使下式化合物：其中R 1，R 2，R 3和R 4独立地为氢原子或选自以下的卤素：式中：CF 3 C（R 1a R 2b）C（R 3 c R 4d） 氟，氯，溴和碘，条件是R 1，R 2，R 3和R 4中的至少一个是卤素，并且在相邻碳原子上具有至少一个氢和一个卤素; a和b独立地为0,1或2，（a + b）= 2; 且c和d独立地为0,1,2或3和（c + d）= 3; 和至少一种碱金属氢氧化物。 碱金属氢氧化物可以是例如氢氧化钾或氢氧化钠，相转移催化剂可以是例如至少一种：冠醚如18-冠-6和15-冠-5; 或鎓盐如季鏻盐和季铵盐。 烯烃可用作例如生产其它工业化学品的中间体，以及用作生产低聚物和聚合物的单体。
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公开(公告)号：US5824826A
公开(公告)日：1998-10-20
申请号：US883931
申请日：1997-06-27
IPC分类号： C07C17/23 , C07C17/281 , C07C19/08 , C07C21/18
CPC分类号： C07C19/08 , C07C17/23 , C07C17/281
摘要： The invention provides a process for the preparation of 1,1,2,3,3,4-hexafluorobutane by telomerization of chlorotrifluoroethylene to produce 1,1,3,4-tetrachlorohexafluorobutane followed by reduction of that compound to 1,1,2,3,3,4-hexafluorobutane.
摘要翻译： 本发明提供了通过氯三氟乙烯调聚制备1,1,2,3,3,4-六氟丁烷的方法制备1,1,3,4-四氯六氟丁烷，然后将该化合物还原成1,1,2， 3,3,4-六氟丁烷。
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公开(公告)号：US20120168663A1
公开(公告)日：2012-07-05
申请号：US13377915
申请日：2010-06-15
CPC分类号： C09K5/041 , C08J9/14 , C08J9/149 , C08J2203/06 , C08J2203/162 , C08J2203/182 , C09K3/30 , C09K5/045 , C09K2205/126 , C09K2205/132
摘要： Disclosed are heat transfer fluids which possess a highly desirable and unexpectedly superior combination of properties, and heat transfer systems and methods based on these fluids. The heat transfer fluid comprise from about 30 to about 70 percent, on a molar basis, of carbon dioxide (CO2) and from about 30 to about 70 percent, on a molar basis, of hydrofluorocarbon (HFC), preferably HFC having one to two carbon atoms, and even more preferably trans-1,1,1,3-tetrafluoropropene (HFC-32). The preferred fluids of the present invention have a vapor pressure of at least about 100 psia at 40?F and are also preferably not azeotropic.
摘要翻译： 公开了具有非常理想和意想不到的性能组合的传热流体，以及基于这些流体的传热系统和方法。 传热流体包含基于摩尔计约30至约70％的二氧化碳（CO 2）和约30至约70％（以摩尔计）的氢氟烃（HFC），优选HFC为一至二 碳原子，甚至更优选反式-1,1,1,3-四氟丙烯（HFC-32）。 本发明的优选流体在40°F时具有至少约100psia的蒸汽压，并且也优选不是共沸的。
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8.发明授权Azeotrope-like compositions of 1-chloro-3,3,3-trifluoropropene and methyl iodide 失效1-氯-3,3,3-三氟丙烯和甲基碘的类共沸组合物公开(公告)号：US07695635B2
公开(公告)日：2010-04-13
申请号：US12258537
申请日：2008-10-27
申请人： Rajiv R. Singh , Hang T. Pham , Andrew J. Poss
发明人： Rajiv R. Singh , Hang T. Pham , Andrew J. Poss
CPC分类号： A01N29/02 , A01N2300/00
摘要： An azeotropic or azeotrope-like composition comprising a mixture of methyl iodide, 1-chloro-3,3,3,-trifluoropropene, and optionally one or more of fluorocarbons and/or hydrofluorocarbons. The compositions are present as a gas, at temperatures of about 30° C. or below. The inventive compositions serve as a non-ozone-depleting gaseous fumigant which is useful in a variety of applications, in place of methyl bromide. These compositions serve as a drop-in replacement for gaseous methyl bromide, providing the benefits of a methyl iodide fumigant while also utilizing existing methyl bromide equipment.
摘要翻译： 包含甲基碘，1-氯-3,3,3-三氟丙烯和任选的一种或多种氟代烃和/或氢氟烃的混合物的共沸或类共沸组合物。 该组合物以约30℃或更低的温度作为气体存在。 本发明的组合物用作非消耗臭氧气体熏蒸剂，其可用于各种应用，代替甲基溴。 这些组合物用作气态甲基溴的替代品，提供甲基碘熏蒸剂的优点，同时还利用现有的甲基溴设备。
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9.发明授权Polyurethane foam premixes containing halogenated olefin blowing agents and foams made from same 有权含有卤代烯烃发泡剂的聚氨酯泡沫预混物和由其制成的泡沫公开(公告)号：US09051442B2
公开(公告)日：2015-06-09
申请号：US13400559
申请日：2012-02-20
IPC分类号： C08G18/22 , C08J9/14 , C08G18/09 , C08G18/18 , C08G18/40 , C08G18/42 , C08G18/50 , C08G18/54 , C08J9/00 , C08G101/00
CPC分类号： C08J9/146 , C08G18/092 , C08G18/1816 , C08G18/222 , C08G18/225 , C08G18/227 , C08G18/4018 , C08G18/4027 , C08G18/4208 , C08G18/5021 , C08G18/546 , C08G2101/0016 , C08G2101/0025 , C08G2105/02 , C08J9/0028 , C08J2203/162 , C08J2375/04
摘要： The invention provides polyurethane and polyisocyanurate foams and methods for the preparation thereof. More particularly, the invention relates to closed-celled, polyurethane and polyisocyanurate foams and methods for their preparation. The foams are characterized by a fine uniform cell structure and little or no foam collapse. The foams are produced with a polyol premix composition which comprises a combination of a hydrohaloolefin blowing agent, a polyol, a silicone surfactant, and a non-amine catalyst used alone or in combination with an amine catalyst.
摘要翻译： 本发明提供聚氨酯和聚异氰脲酸酯泡沫及其制备方法。 更具体地说，本发明涉及闭孔，聚氨酯和聚异氰脲酸酯泡沫及其制备方法。 泡沫的特征在于细小的均匀的细胞结构和很少或没有泡沫崩溃。 泡沫体是用多元醇预混物组合物生产的，该组合物包含氢卤烯烃发泡剂，多元醇，硅氧烷表面活性剂和单独使用或与胺催化剂组合使用的非胺催化剂的组合。
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公开(公告)号：US20080199408A1
公开(公告)日：2008-08-21
申请号：US11707498
申请日：2007-02-16
申请人： Andrew J. Poss , Rajiv R. Singh , Hang T. Pham
发明人： Andrew J. Poss , Rajiv R. Singh , Hang T. Pham
IPC分类号： A01N25/18
CPC分类号： A01N29/02 , A01N2300/00
摘要： Azeotropic and azeotrope-like compositions of methyl iodide and at least one fluorocarbon or hydrofluorocarbon such as 1,1,1,3,3-pentafluoropropane (HFC-245fa). The compositions are present as a gas, at temperatures of about 30° C. or below. The inventive compositions serve as a non-ozone-depleting gaseous fumigant which is useful in a variety of applications, in place of methyl bromide. These compositions serve as a drop-in replacement for gaseous methyl bromide, providing the benefits of a methyl iodide fumigant while also utilizing existing methyl bromide equipment.
摘要翻译： 甲基碘和至少一种碳氟化合物或氢氟烃如1,1,1,3,3-五氟丙烷（HFC-245fa）的共沸和类共沸组合物。 该组合物以约30℃或更低的温度作为气体存在。 本发明的组合物用作非消耗臭氧气体熏蒸剂，其可用于各种应用中，代替甲基溴。 这些组合物用作气态甲基溴的替代品，提供甲基碘熏蒸剂的优点，同时还利用现有的甲基溴设备。
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