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    Method for producing polyesters and a disk ring reactor for the method
    1.
    发明授权
    Method for producing polyesters and a disk ring reactor for the method 有权
    用于生产聚酯的方法和用于该方法的盘式环形反应器

    公开(公告)号：US07550116B2

    公开(公告)日：2009-06-23

    申请号：US11667156

    申请日：2005-10-20

    申请人： Fritz Wilhelm ,  Michael Reisen ,  Ludwig Hölting ,  Peter Seidel ,  Peter Reichwein

    发明人： Fritz Wilhelm ,  Michael Reisen ,  Ludwig Hölting ,  Peter Seidel ,  Peter Reichwein

    IPC分类号： B01J19/18 ,  B01J19/00 ,  C08F2/00

    CPC分类号： B01F7/00491 ,  B01F7/10 ,  B01J19/0066 ,  B01J19/18 ,  B01J19/1887 ,  B01J2219/00168 ,  B01J2219/182 ,  B01J2219/1943 ,  C08G63/183 ,  C08G63/785

    摘要： The invention relates to a method and a device for producing polyesters such as for example polyethylene terephthalate, polypropylene terephthalate and polybutylene terephthalate from precondensates. According to said method, vapors comprising precondensate components that are distributed therein in the form of an aerosol are guided through a polycondensation reactor in which precondensate components condense on the reactor wall and on a separator in an exit chamber of the reactor. The condensates are guided to the unstirred discharge sump and the upper layers of the discharge sump are continuously recirculated into the stirred reactor area thereby subjecting them to reconversion and additional polycondensation.

    摘要翻译： 本发明涉及一种用于从预缩合物生产聚酯的方法和装置，例如聚对苯二甲酸乙二醇酯，聚对苯二甲酸丙二醇酯和聚对苯二甲酸丁二醇酯。 根据所述方法，包含以气溶胶形式分布在其中的预缩合组分的蒸气被引导通过缩聚反应器，其中预缩合组分在反应器壁上和在反应器的出口室中的分离器上冷凝。 将冷凝物引导到未搅拌的排放池，并且排放池的上层连续地再循环到搅拌反应器区域中，从而使它们再转化和进一步缩聚。

    Method for Producing Polyesters and A Disk Ring Reactor for the Method
    3.
    发明申请
    Method for Producing Polyesters and A Disk Ring Reactor for the Method 有权
    方法生产聚酯和圆环反应器的方法

    公开(公告)号：US20080064834A1

    公开(公告)日：2008-03-13

    申请号：US11667156

    申请日：2005-10-20

    申请人： Fritz Wilhelm ,  Michael Reisen ,  Ludwig Holting ,  Peter Seidel ,  Peter Reichwein

    发明人： Fritz Wilhelm ,  Michael Reisen ,  Ludwig Holting ,  Peter Seidel ,  Peter Reichwein

    IPC分类号： B01J19/18 ,  C08F2/01

    CPC分类号： B01F7/00491 ,  B01F7/10 ,  B01J19/0066 ,  B01J19/18 ,  B01J19/1887 ,  B01J2219/00168 ,  B01J2219/182 ,  B01J2219/1943 ,  C08G63/183 ,  C08G63/785

    摘要： The invention relates to a method and a device for producing polyesters such as for example polyethylene terephthalate, polypropylene terephthalate and polybutylene terephthalate from precondensates. According to said method, vapors comprising precondensate components that are distributed therein in the form of an aerosol are guided through a polycondensation reactor in which precondensate components condense on the reactor wall and on a separator in an exit chamber of the reactor. The condensates are guided to the unstirred discharge sump and the upper layers of the discharge sump are continuously recirculated into the stirred reactor area, thereby subjecting them to reconversion and additional polycondensation.

    摘要翻译： 本发明涉及一种用于从预缩合物生产聚酯的方法和装置，例如聚对苯二甲酸乙二醇酯，聚对苯二甲酸丙二醇酯和聚对苯二甲酸丁二醇酯。 根据所述方法，包含以气溶胶形式分布在其中的预缩合组分的蒸气被引导通过缩聚反应器，其中预缩合组分在反应器壁上和在反应器的出口室中的分离器上冷凝。 将冷凝物引导到未搅拌的排放池，并且排放池的上层连续再循环到搅拌反应器区域中，从而使它们再转化和进一步缩聚。

    Method and device for producing polyesters, copolyesters and polycarbonates
    4.
    发明申请
    Method and device for producing polyesters, copolyesters and polycarbonates 有权
    用于生产聚酯，共聚酯和聚碳酸酯的方法和装置

    公开(公告)号：US20050222371A1

    公开(公告)日：2005-10-06

    申请号：US10513227

    申请日：2003-04-02

    申请人： Fritz Wilhelm ,  Michael Reisen

    发明人： Fritz Wilhelm ,  Michael Reisen

    IPC分类号： B01J19/18 ,  B01J19/20 ,  C08G63/78 ,  C08G64/20 ,  C08G64/30 ,  C08G64/00 ,  C08G63/02

    CPC分类号： B01J19/20 ,  B01J19/1856 ,  B01J19/1862 ,  B01J2219/00006 ,  B01J2219/182 ,  C08G63/78 ,  C08G63/785 ,  C08G64/205 ,  C08G64/307

    摘要： In a process for producing polyester, the esterification of dicarboxylic acids and diols is carried out in at least one reaction stage, the prepolycondensation of the esterification product in at least one reaction stage and the polycondensation of the prepolycondensation product in at least one reaction stage. To increase the capacity of the apparatus forming one or more of the reaction stages in the production of the polyesters, at at least one of the reaction stages the supplied product system before it enters the reaction stage or within the reaction stage is divided into at least two partial streams and the partial streams entirely or partially separate from one another is passed through the reaction stage.

    摘要翻译： 在制造聚酯的方法中，二羧酸和二醇的酯化在至少一个反应阶段进行，酯化产物在至少一个反应阶段中的预缩聚和预缩聚产物在至少一个反应阶段中的缩聚反应。 为了增加在聚酯生产中形成一个或多个反应阶段的装置的能力，在至少一个反应阶段，所提供的产物体系在其进入反应阶段之前或在反应阶段内被分成至少 两个部分流和完全或部分地彼此分离的部分流通过反应阶段。

    Method and device for the continuous production of polyesters
    6.
    发明授权
    Method and device for the continuous production of polyesters 有权
    连续生产聚酯的方法和装置

    公开(公告)号：US07244806B2

    公开(公告)日：2007-07-17

    申请号：US10530216

    申请日：2003-09-19

    申请人： Fritz Wilhelm ,  Michael Reisen

    发明人： Fritz Wilhelm ,  Michael Reisen

    IPC分类号： C08G64/00

    CPC分类号： C08G63/785 ,  B01J3/006 ,  B01J19/0066 ,  B01J19/18

    摘要： In the continuous production of polyesters, the esterification/transesterification of dicarboxylic acids or esters of the dicarboxylic acids with diols is performed in at least one reaction stage, the prepolycondensation of the esterification/transesterification product is performed under a vacuum in a reaction stage consisting of a vertical tube, and the polycondensation of the prepolycondensation product is performed in at least one reaction stage. To be able to perform the prepolycondensation in a reaction stage, while at the same time increasing the viscosity of the prepolycondensation product and decreasing the process temperatures, the esterification/transesterification product flowing into the prepolycondensation reactor successively traverses in a free movement under limited heating first at least one first reaction zone formed of an annular channel, is then introduced into the radially outer ring duct of at least one second reaction zone formed of an annular channel divided into a plurality of concentric ring ducts, thereafter is successively passed through the ring ducts to the outlet, and is then introduced into a stirred third reaction zone located at the bottom of the vertical tube.

    摘要翻译： 在聚酯的连续生产中，二羧酸或二醇的酯与二醇的酯化/酯交换在至少一个反应阶段进行，酯化/酯交换反应产物的预缩聚在真空下在由 垂直管，并且预缩聚产物的缩聚在至少一个反应阶段中进行。 为了能够在反应阶段中进行预缩聚，同时增加预缩聚产物的粘度并降低工艺温度，流入预缩聚反应器的酯化/酯交换反应产物在有限加热下自由移动 至少一个由环形通道形成的第一反应区然后被引入至少一个第二反应区的径向外环管道中，该第二反应区由分成多个同心环管道的环形通道形成，之后依次通过环管道 然后引入到位于垂直管底部的搅拌的第三反应区中。

    Method and device for the continuous production of polyesters
    8.
    发明申请
    Method and device for the continuous production of polyesters 有权
    连续生产聚酯的方法和装置

    公开(公告)号：US20060009608A1

    公开(公告)日：2006-01-12

    申请号：US10530216

    申请日：2003-09-19

    申请人： Fritz Wilhelm ,  Michael Reisen

    发明人： Fritz Wilhelm ,  Michael Reisen

    IPC分类号： B01J19/00 ,  B01J19/18 ,  C08G63/02

    CPC分类号： C08G63/785 ,  B01J3/006 ,  B01J19/0066 ,  B01J19/18

    摘要： In the continuous production of polyesters, the esterification/transesterification of dicarboxylic acids or esters of the dicarboxylic acids with diols is performed in at least one reaction stage, the prepolycondensation of the esterification/transesterification product is performed under a vacuum in a reaction stage consisting of a vertical tube, and the polycondensation of the prepolycondensation product is performed in at least one reaction stage. To be able to perform the prepolycondensation in a reaction stage, while at the same time increasing the viscosity of the prepolycondensation product and decreasing the process temperatures, the esterification/transesterification product flowing into the prepolycondensation reactor successively traverses in a free movement under limited heating first at least one first reaction zone formed of an annular channel, is then introduced into the radially outer ring duct of at least one second reaction zone formed of an annular channel divided into a plurality of concentric ring ducts, thereafter is successively passed through the ring ducts to the outlet, and is then introduced into a stirred third reaction zone located at the bottom of the vertical tube.

    摘要翻译： 在聚酯的连续生产中，二羧酸或二醇的酯与二醇的酯化/酯交换在至少一个反应阶段进行，酯化/酯交换反应产物的预缩聚在真空下在由 垂直管，并且预缩聚产物的缩聚在至少一个反应阶段中进行。 为了能够在反应阶段中进行预缩聚，同时增加预缩聚产物的粘度并降低工艺温度，流入预缩聚反应器的酯化/酯交换反应产物在有限加热下自由移动 至少一个由环形通道形成的第一反应区然后被引入至少一个第二反应区的径向外环管道中，该第二反应区由分成多个同心环管道的环形通道形成，之后依次通过环管道 然后引入到位于垂直管底部的搅拌的第三反应区中。

    Process of continuously producing polyesters or copolyesters
    9.
    发明授权
    Process of continuously producing polyesters or copolyesters 失效
    连续生产聚酯或共聚酯的工艺

    公开(公告)号：US07153927B2

    公开(公告)日：2006-12-26

    申请号：US10451292

    申请日：2001-11-27

    申请人： Fritz Wilhelm ,  Michael Reisen

    发明人： Fritz Wilhelm ,  Michael Reisen

    IPC分类号： C08G63/00

    CPC分类号： B01D3/14 ,  C08G63/78

    摘要： Process for producing polyesters and copolyesters, wherein a continuous esterification of dicarboxylic esters and diols or a continuous transesterification of dicarboxylic esters with diols is effected in “n” reaction pressure stages connected in series, the pressure in the first reaction pressure stage is higher than that of the remaining reaction pressure stages, and successively decreases from reaction pressure stage to succeeding reaction pressure stage, the combined vapor flows of the individual reaction pressure stages are rectified in a rectifying column, and the diol component obtained at the bottom of the rectifying column is recirculated at least to the first reaction pressure stage, and wherein at least the last reaction pressure stage operates at a vacuum, the pressure in the rectifying column is greater than that of the last reaction pressure stage, and the vapors discharged from the last reaction pressure stage are condensed to the pressure existing in the rectifying column.

    摘要翻译： 制备聚酯和共聚酯的方法，其中连续酯化二羧酸酯和二醇或二羧酸酯与二醇的连续酯交换在连续串联的“n”个反应压力阶段中进行，第一反应压力阶段的压力高于第 的剩余反应压力级，从反应压力阶段到后续反应压力阶段相继降低，各个反应压力级的组合蒸气流在精馏塔中精馏，精馏塔底部得到的二醇成分为 至少再循环到第一反应压力级，并且其中至少最后的反应压力级在真空下操作，精馏塔中的压力大于最后反应压力级的压力，并且从最后的反应压力排出的蒸气 阶段被压缩到整流库中存在的压力 嗯

    Method and device for the continuous pre-polycondensation of esterification/transesterification products
    10.
    发明申请
    Method and device for the continuous pre-polycondensation of esterification/transesterification products 审中-公开
    酯化/酯交换产物连续预缩聚的方法和装置

    公开(公告)号：US20060030727A1

    公开(公告)日：2006-02-09

    申请号：US11198872

    申请日：2005-08-06

    申请人： Fritz Wilhelm ,  Michael Reisen

    发明人： Fritz Wilhelm ,  Michael Reisen

    IPC分类号： C07C69/76 ,  B01J8/04

    CPC分类号： B01J19/006 ,  B01J19/1806 ,  B01J19/248 ,  B01J2219/00081 ,  B01J2219/00085 ,  B01J2219/00166 ,  B01J2219/00168 ,  B01J2219/00182 ,  B01J2219/00768 ,  B01J2219/00779

    摘要： In a method for the continuous pre-polycondensation of esterification/transesterification products the stream freely passes from top to bottom in a vertical reaction apparatus through a plurality of attached, heatable, sloped open-above bases, through product overflow channels connected with each other. In order to be able to set a determined, efficient as possible product level in the channels, the esterification/transesterification products are fed though closed, annular-type, concentric annular channels or through parallel channels, wherein a partial quantity of the product stream flowing in the channel is discharged at the product overflows and the remaining product stream is passed via drainage openings.

    摘要翻译： 在酯化/酯交换产物的连续预缩聚的方法中，流体通过多个连接，可加热，倾斜的开放的上部基底，通过彼此连接的产品溢流通道，在垂直反应装置中从顶部到底部自由地通过。 为了能够在通道中设定确定的，有效率的产品水平，酯化/酯交换产物通过封闭的，环形的，同心的环形通道或平行通道进料，其中部分量的产物流流动 在通道中产品溢出时排放，剩余的产品流通过排水口进入。