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    Suspension polymerization process for the preparation of polymeric material from gaseous and non-gaseous monomers
    1.
    发明授权
    Suspension polymerization process for the preparation of polymeric material from gaseous and non-gaseous monomers 失效
    用于从气态和非气态单体制备聚合物材料的悬浮聚合方法

    公开(公告)号：US5177153A

    公开(公告)日：1993-01-05

    申请号：US896778

    申请日：1992-06-10

    申请人： George Liebermann ,  William J. Dale ,  Nam S. Ro ,  Daniel M. McNeil ,  Stephan Drappel

    发明人： George Liebermann ,  William J. Dale ,  Nam S. Ro ,  Daniel M. McNeil ,  Stephan Drappel

    IPC分类号： C08F2/18 ,  C08F236/10

    CPC分类号： C08F2/18 ,  C08F236/10

    摘要： A suspension polymerization process for the preparation of a polymeric material formed from at least two monomers, a non-gaseous monomer and a gaseous monomer. The composition of the beads or particles of the polymeric material is controlled by adding gaseous monomer to the vapor phase after polymerization of about 5% to about 90% by weight of the non-gaseous monomer or by removing a portion or substantially all of the gaseous monomer in the vapor phase before polymerization of about 70% by weight of the gaseous monomer in the aqueous suspension, or a combination thereof.

    摘要翻译： 一种用于制备由至少两种单体，非气态单体和气体单体形成的聚合物材料的悬浮聚合方法。 聚合材料的珠粒或颗粒的组成通过在约5％至约90％重量的非气态单体的聚合之后，将气体单体加入到气相中，或通过除去气态单体的一部分或基本上全部气态 在水性悬浮液中约70重量％的气态单体聚合前的气相中的单体，或其组合。

    Latex processes
    2.
    发明授权
    Latex processes 失效
    乳胶工艺

    公开(公告)号：US06503680B1

    公开(公告)日：2003-01-07

    申请号：US09940926

    申请日：2001-08-29

    申请人： Allan K. Chen ,  George Liebermann ,  Tie Hwee Ng ,  Arthur Helbrecht ,  Emily L. Moore ,  Abdisamed Sheik-qasim ,  Patricia A. Burns ,  Nam S. Ro

    发明人： Allan K. Chen ,  George Liebermann ,  Tie Hwee Ng ,  Arthur Helbrecht ,  Emily L. Moore ,  Abdisamed Sheik-qasim ,  Patricia A. Burns ,  Nam S. Ro

    IPC分类号： G03G9087

    CPC分类号： G03G9/08702 ,  C08F291/00 ,  G03G9/0806 ,  G03G9/081 ,  C08F2/22

    摘要： A process for the preparation of a latex polymer consistent with E/A (emulsion/aggregation/coalescence) toner manufacture. The process utilizes a standard (universal) latex composition and involves chain-transfer agent partitioning, emulsion polymerization that provides a latex polymer with a wide range of molecular properties. In particular, the process customizes a wide range Mw (weight average molecular weight) latex, without substantially varying the Mn (number average molecular weight) and hence, without substantially varying Tg (glass transition temperature) such that good toner performance is maintained. In a preferred process, a latex polymer is prepared by mixing a seed particle latex, generated by aqueous emulsion polymerization of a first portion of a monomer emulsion, with a second portion of the monomer emulsion and at least one chain-transfer agent. The mixing is done in the presence of a free-radical initiator and heated, and wherein the monomer emulsion comprises a mixture of polymerization reagents of at least one monomer, at least one chain-transfer agent, at least one surfactant, and water. This process may be applied to core-shell polymerization as well. These latex polymers are ideally suited in the manufacture of toner and developer for electrophotographic imaging and printing.

    摘要翻译： 制备与E / A（乳液/聚集/聚​​结）调色剂制造一致的胶乳聚合物的方法。 该方法使用标准（通用）胶乳组合物，并涉及链转移剂分配，乳液聚合，其提供具有广泛分子性质的胶乳聚合物。 特别地，该方法定制了宽范围的Mw（重均分子量）胶乳，而基本上不改变Mn（数均分子量），因此没有实质上改变的Tg（玻璃化转变温度），使得维持良好的调色剂性能。 在优选的方法中，通过混合通过单体乳液的第一部分的水乳液聚合产生的种子颗粒胶乳与第二部分单体乳液和至少一种链转移剂来制备胶乳聚合物。 混合在自由基引发剂的存在下进行并加热，其中单体乳液包含至少一种单体，至少一种链转移剂，至少一种表面活性剂和水的聚合试剂的混合物。 该方法也可以应用于核 - 壳聚合。 这些胶乳聚合物非常适用于制造用于电子照相成像和印刷的调色剂和显影剂。

    Conductive polymers
    4.
    发明授权
    Conductive polymers 失效
    导电聚合物

    公开(公告)号：US5958302A

    公开(公告)日：1999-09-28

    申请号：US100905

    申请日：1998-06-19

    申请人： Michael F. Cunningham ,  George Liebermann ,  Hadi K. Mahabadi ,  Daniel M. McNeil ,  Michael S. Hawkins ,  Thomas E. Enright ,  Aron J. Cogswell

    发明人： Michael F. Cunningham ,  George Liebermann ,  Hadi K. Mahabadi ,  Daniel M. McNeil ,  Michael S. Hawkins ,  Thomas E. Enright ,  Aron J. Cogswell

    IPC分类号： C08F2/18 ,  C08F2/44 ,  C08F292/00 ,  H01B1/20 ,  H01B1/22 ,  H01B1/24 ,  H01B1/00 ,  H01B1/06

    CPC分类号： C08F292/00 ,  H01B1/20 ,  H01B1/22 ,  H01B1/24

    摘要： A process for the preparation of conductive polymers which comprises (a) mixing at least one monomer with at least one conductive component, solvent, at least one polymerization initiator, and an optional chain transfer component; (b) effecting solution polymerization by heating; (c) removing said solvent by azeotropic distillation in an aqueous phase to generate a mixture of polymer and conductive component; (d) drying and grinding the resulting mixture; thereafter dissolving the product resulting in at least one monomer, at least one initiator, and at least one crosslinking component, and an optional chain transfer agent to form an organic phase; (e) mixing said organic phase with a second aqueous phase comprised of water, stabilizer, and an alkali halide; (f) polymerizing the resulting suspension by heating; and (g) subsequently optionally washing and drying the polymeric product, and which product is comprised of polymer and conductive component dispersed therein.

    摘要翻译： 一种制备导电聚合物的方法，其包括（a）将至少一种单体与至少一种导电组分，溶剂，至少一种聚合引发剂和任选的链转移组分混合; （b）通过加热进行溶液聚合; （c）通过在水相中共沸蒸馏除去所述溶剂以产生聚合物和导电组分的混合物; （d）干燥和研磨所得混合物; 然后将产物溶解得到至少一种单体，至少一种引发剂和至少一种交联组分和任选的链转移剂以形成有机相; （e）将所述有机相与由水，稳定剂和碱金属卤化物组成的第二水相混合; （f）通过加热使得到的悬浮液聚合; 和（g）随后任选地洗涤和干燥聚合物产物，哪种产物由分散在其中的聚合物和导电组分组成。

    Imaging members
    7.
    发明授权
    Imaging members 失效
    成像成员

    公开(公告)号：US06645687B1

    公开(公告)日：2003-11-11

    申请号：US10144120

    申请日：2002-05-10

    申请人： Cuong Vong ,  George Liebermann ,  Richard A. Burt ,  Ah-Mee Hor

    发明人： Cuong Vong ,  George Liebermann ,  Richard A. Burt ,  Ah-Mee Hor

    IPC分类号： G03G5047

    CPC分类号： C09B67/0035 ,  G03G5/0696

    摘要： A process comprising forming chlorogallium phthalocyanine (ClGaPc) in N-methyl-2-pyrrolidinone (NMP) to provide a ClGaPc (NMP) Type I; separately dry milling and then wet treating the Type I product to form Type II ClGaPc (NMP); blending the ClGaPc Type II product with hydroxygallium phthalocyanine (HOGaPc) Type V and a resin to form a coating mixture; coating the resulting mixture to form a photoconductive charge generator layer.

    摘要翻译： 一种包括在N-甲基-2-吡咯烷酮（NMP）中形成氯镓酞菁（ClGaPc）以提供I型的ClGaPc（NMP）的方法; 分别干磨，然后湿法处理I型产物形成II型ClGaPc（NMP）; 将ClGaPc II型产物与V型羟基镓酞菁（HOGaPc）和树脂混合以形成涂料混合物; 涂覆所得混合物以形成光导电荷发生器层。

    Processes for preparing dianthranilate compounds and diazopyridone colorants
    8.
    发明授权
    Processes for preparing dianthranilate compounds and diazopyridone colorants 失效
    制备二邻氨基苯甲酸酯化合物和重氮吡啶酮着色剂的方法

    公开(公告)号：US06576747B1

    公开(公告)日：2003-06-10

    申请号：US10185261

    申请日：2002-06-27

    申请人： Rina Carlini ,  James M. Duff ,  Stephen G. Robinson ,  George Liebermann ,  Roger E. Gaynor ,  Tania Pereira ,  Jeffrey H. Banning ,  James D. Mayo

    发明人： Rina Carlini ,  James M. Duff ,  Stephen G. Robinson ,  George Liebermann ,  Roger E. Gaynor ,  Tania Pereira ,  Jeffrey H. Banning ,  James D. Mayo

    IPC分类号： C09B35031

    CPC分类号： C09B35/031 ,  C07C227/18 ,  C07C227/22 ,  C07C229/56 ,  C07D213/85 ,  Y10S534/02

    摘要： Disclosed is a process for preparing dianthranilate compounds which comprises (a) admixing reactants as follows: (1) a diol of the formula R1(OH)2, wherein R1 is an alkylene group having at least about 20 carbon atoms, and wherein the —OH groups are primary or secondary, (2) isatoic anhydride, present in an amount of at least, about 2 moles of isatoic anhydride per every one mole of diol, (3) a catalyst which is 1,4-diazabicyclo [2.2.2]octane, N,N,N′,N′-tetramethylethylene diamine, or a mixture thereof, said catalyst being present in an amount of at least about 0.2 mole of catalyst per every one mole of diol, and (4) a solvent; and (b) heating the mixture thus formed to form a dianthranilate compound of the formula Also disclosed is a process for preparing diazopyridone colorants which comprises (I) preparing a dianthranilate compound by the aforementioned method, (II) reacting the dianthranilate compound with nitrosylsulfuric acid to form a diazonium salt, and (III) reacting the, diazonium salt with a pyridone compound to form a diazopyridone compound.

    摘要翻译： 公开了一种制备二氨基甲酸盐化合物的方法，其包括（a）如下混合反应物：（1）式R 1（OH）2的二醇，其中R 1是具有至少约20个碳原子的亚烷基， OH基团是伯或仲，（2）丙酸酐，每1摩尔二醇存在量至少约2摩尔丙烯酸酐，（3）作为1,4-二氮杂双环[2.2.2 ]辛烷，N，N，N'，N'-四甲基乙二胺或其混合物，所述催化剂的存在量为每一摩尔二醇至少约0.2摩尔催化剂，和（4）溶剂; 和（b）加热由此形成的混合物以形成下式的二邻氨基苯甲酸酯化合物。另外公开的是一种制备重氮吡啶酮着色剂的方法，其包括（I）通过上述方法制备二氨基甲酸酯化合物，（II）使二邻氨基苯甲酸酯化合物与亚硝酰基磺酸反应 形成重氮盐，和（III）使重氮盐与吡啶酮化合物反应形成二叠氮基吡啶酮化合物。

    Arylamine processes
    9.
    发明授权
    Arylamine processes 失效
    芳胺方法

    公开(公告)号：US5902901A

    公开(公告)日：1999-05-11

    申请号：US74620

    申请日：1998-05-07

    申请人： H. Bruce Goodbrand ,  George Liebermann ,  Roger E. Gaynor

    发明人： H. Bruce Goodbrand ,  George Liebermann ,  Roger E. Gaynor

    IPC分类号： C07C209/10 ,  C07C211/54

    CPC分类号： C07C209/10

    摘要： A process for the preparation of N,N-bis(3,4-dimethylphenyl)-4-biphenylamine which comprises the reaction of N,N-bis(3,4-dimethylphenyl)amine and an iodobiphenyl in the presence of a ligand copper catalyst, and wherein the ligand is selected from the group consisting of monodentate tertiary amines and bidentate tertiary amines, and which reaction is accomplished at a temperature of, for example, from about 120.degree. C. to about 150.degree. C.

    摘要翻译： 一种制备N，N-双（3,4-二甲基苯基）-4-联苯胺的方法，其包括在配体铜的存在下N，N-双（3,4-二甲基苯基）胺和碘代联苯的反应 催化剂，并且其中所述配体选自单齿叔胺和二齿叔胺，并且该反应在例如约120℃至约150℃的温度下进行。

    Hydroxygallium phthalocyanine photoconductive imaging members
    10.
    发明授权
    Hydroxygallium phthalocyanine photoconductive imaging members 失效
    羟基镓酞菁光导成像构件

    公开(公告)号：US5563261A

    公开(公告)日：1996-10-08

    申请号：US469240

    申请日：1995-06-06

    申请人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao Murti ,  Sandra J. Gardner

    发明人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao Murti ,  Sandra J. Gardner

    IPC分类号： C07D487/22 ,  C09B67/16 ,  C09B67/50 ,  G03G5/06 ,  C09B67/12

    CPC分类号： G03G5/0696

    摘要： A process for the preparation of hydroxygallium phthalocyanines which comprises hydrolyzing a gallium phthalocyanine precursor pigment by dissolving said hydroxygallium phthalocyanine in a strong acid and then reprecipitating the resulting dissolved pigment in basic aqueous media; removing any ionic species formed by washing with water, concentrating the resulting aqueous slurry comprised of water and hydroxygallium phthalocyanine to a wet cake; removing water from said slurry by azeotropic distillation with an organic solvent, and subjecting said resulting pigment slurry to mixing with the addition of a second solvent to cause the formation of said hydroxygallium phthalocyanine polymorphs.

    摘要翻译： 一种制备羟基镓酞菁的方法，其包括通过将所述羟基镓酞菁溶解在强酸中，然后将所得溶解的颜料再沉淀在碱性水性介质中来水解镓酞菁前体颜料; 去除通过用水洗涤形成的任何离子物质，将由水和羟基镓酞菁组成的所得水性浆料浓缩到湿饼; 通过与有机溶剂共沸蒸馏从所述浆料中除去水，并将所得颜料浆料加入第二溶剂进行混合，形成所述羟基镓酞菁多晶型物。