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32 条记录 (耗时 0.019 秒)

    Alkenyl acetamides
    1.
    发明授权
    Alkenyl acetamides 失效
    乙烯基乙酰胺

    公开(公告)号：US4665228A

    公开(公告)日：1987-05-12

    申请号：US848185

    申请日：1986-04-04

    申请人： Gerhard H. Alt ,  John P. Chupp ,  Lane A. Clizbe

    发明人： Gerhard H. Alt ,  John P. Chupp ,  Lane A. Clizbe

    IPC分类号： A01N37/26 ,  A01N49/00 ,  A01N53/00 ,  C07C103/30 ,  C07C125/06

    CPC分类号： A01N53/00 ,  A01N37/26 ,  A01N49/00

    摘要： Compounds of the formula: ##STR1## wherein R.sub.1, R.sub.2, and R.sub.3 are independently hydrogen, halogen, C.sub.1-6 alkyl, or haloalkyl; R.sub.4 is hydrogen; C.sub.1-4 alkyl, alkenyl, alkoxy, haloalkyl; C.sub.1-2 alkylamino, C.sub.1-2 alkylthio, C.sub.2-4 cycloalkyl, C.sub.2-6 alkoxyalkyl, C.sub.2-6 alkylthiomethyl, amino, phenoxy, phenamino, or furan; and R.sub.5 is hydrogen or C.sub.1-4 alkyl, are useful to retard the growth of turf grass.

    摘要翻译： 下式的化合物：其中R 1，R 2和R 3独立地是氢，卤素，C 1-6烷基或卤代烷基; R4是氢; C 1-4烷基，烯基，烷氧基，卤代烷基; C1-2烷基氨基，C1-2烷硫基，C2-4环烷基，C2-6烷氧基烷基，C2-6烷硫基甲基，氨基，苯氧基，苯氨基或呋喃; 并且R 5是氢或C 1-4烷基，可用于延缓草坪草的生长。

    Nitro-methyl or ethyl substituted benzotrifluoride
    3.
    发明授权
    Nitro-methyl or ethyl substituted benzotrifluoride 失效
    硝基甲基或乙基取代的三氟甲苯

    公开(公告)号：US4467125A

    公开(公告)日：1984-08-21

    申请号：US503375

    申请日：1983-06-10

    申请人： John P. Chupp ,  Gerhard H. Alt

    发明人： John P. Chupp ,  Gerhard H. Alt

    IPC分类号： C07C205/11 ,  C07C79/12

    CPC分类号： C07C205/11

    摘要： The invention herein pertains to nitro-methyl or ethyl substituted benzotrifluoride compounds useful as chemical intermediates and a process for their preparation. The chemical intermediates are useful for the preparation of substituted anilines which are precursors for a new class of 2-haloacetanilide herbicides.

    摘要翻译： 本发明涉及可用作化学中间体的硝基甲基或乙基取代的三氟甲苯化合物及其制备方法。 化学中间体可用于制备作为新一类2-卤代乙酰苯胺除草剂前体的取代苯胺。

    Alpha-chloro-alkoxymethyl-N-(2,6-dialkoxyphenyl)acetamides as effective turfgrass regulants
    4.
    发明授权
    Alpha-chloro-alkoxymethyl-N-(2,6-dialkoxyphenyl)acetamides as effective turfgrass regulants 失效
    α-氯 - 烷氧基甲基-N-（2,6-二烷氧基苯基）乙酰胺作为有效的草坪草调节剂

    公开(公告)号：US4288242A

    公开(公告)日：1981-09-08

    申请号：US133762

    申请日：1980-03-25

    申请人： Gerhard H. Alt ,  John P. Chupp

    发明人： Gerhard H. Alt ,  John P. Chupp

    IPC分类号： A01N37/26 ,  A01N37/24

    CPC分类号： A01N37/26

    摘要： This disclosure relates to a class of alpha-chloro-N-alkoxymethyl-N-(2,6-dialkoxyphenyl)acetamides which are effective in regulating the natural growth or development of plants. As employed herein, the term "natural growth or development" designates the normal life cycle of the plant in accordance with its genetics and its environment, in the absence of artificial, external influences. More particularly, this disclosure is concerned with a method wherein turfgrasses are treated with an alpha-chloro-N-alkoxymethyl-N-(2,6-dialkoxyphenyl)acetamide which serves to retard or reduce the rate of turfgrass growth. Such a treatment may also serve to retard or reduce the formation of seedheads and seedhead stalk elongation.

    摘要翻译： 本公开涉及一类有效调节植物的天然生长或发育的α-氯-N-烷氧基甲基-N-（2,6-二烷氧基苯基）乙酰胺。 如本文所使用的，在没有人为的外部影响的情况下，术语“自然生长或发育”表示植物根据其遗传学及其环境的正常生命周期。 更具体地说，本公开涉及一种方法，其中草坪草用α-氯-N-烷氧基甲基-N-（2,6-二烷氧基苯基）乙酰胺处理，其用于延缓或降低草坪草生长速率。 这种处理也可以用于延缓或减少种子头和种子茎茎伸长的形成。

    Process for the in-solvent, in-situ generation of haloalkyl alkyl ethers
    6.
    发明授权
    Process for the in-solvent, in-situ generation of haloalkyl alkyl ethers 失效
    卤代烷基烷基醚的溶剂，原位产生方法

    公开(公告)号：US4371717A

    公开(公告)日：1983-02-01

    申请号：US230996

    申请日：1981-02-03

    申请人： Gerhard H. Alt ,  John P. Chupp

    发明人： Gerhard H. Alt ,  John P. Chupp

    IPC分类号： C07D309/06 ,  C07C41/01

    CPC分类号： C07D309/06

    摘要： The present invention is directed to a process for the preparation of certain N-substituted-2-haloacetanilides via the reaction of a secondary 2-haloacetanilide with a haloalkyl ether, particularly, halomethyl ethers, which comprises forming the ether in situ by the in-solvent reaction of an alcohol, formaldehyde or other aldehyde and an acid halide to produce high purity haloalkyl ethers, while decreasing the concentration of undesirable bis by products, as for example bis(chloromethyl) ether. The ether formed in situ thereafter reacts with the secondary 2-haloacetanilide in the presence of a phase transfer catalyst and base to form the N-substituted-2-haloacetanilide.

    摘要翻译： 本发明涉及一种通过二次2-卤代乙酰苯胺与卤代烷基醚，特别是卤代甲基醚的反应制备某些N-取代-2-卤代乙酰苯胺的方法，该方法包括通过在室温下原位形成醚， 醇，甲醛或其它醛和酰卤的溶剂反应产生高纯度卤代烷基醚，同时降低不期望的双产物浓度，例如双（氯甲基）醚。 原位形成的醚在相转移催化剂和碱存在下与仲2-卤代乙酰苯胺反应形成N-取代-2-卤代乙酰苯胺。

    Preparation of 2-(methylthiomethyl)-6-(trifluoromethyl)aniline from ortho-aminobenzotrifluoride
    10.
    发明授权
    Preparation of 2-(methylthiomethyl)-6-(trifluoromethyl)aniline from ortho-aminobenzotrifluoride 失效
    由邻氨基三氟甲苯制备2-（甲硫基甲基）-6-（三氟甲基）苯胺

    公开(公告)号：US4496765A

    公开(公告)日：1985-01-29

    申请号：US530153

    申请日：1983-09-07

    申请人： Audrey Y. Ku ,  John P. Chupp ,  Terry M. Balthazor

    发明人： Audrey Y. Ku ,  John P. Chupp ,  Terry M. Balthazor

    IPC分类号： C07C20060101 ,  C07C85/24

    CPC分类号： C07C319/14 ,  C07C381/10

    摘要： This invention relates to a process for the preparation of 2-(methylthiomethyl)-6-(trifluoromethyl) aniline, [MTA], from ortho-aminobenzotrifluoride, (OABT), employing a single solvent transformation via a sulfilimine intermediate. A sulfilimine hydrochloride salt is prepared by the oxidative addition of dimethyl sulfide to OABT in the presence of N-chlorosuccinimide. Neutralization of the sulfilimine hydrochloride salt with aqueous sodium hydroxide followed by phase separation results in an organic phase containing free sulfilimine and an aqueous phase generally containing succinimide and/or sodium succinimide. In a preferred embodiment the phase separation is performed in such a manner to leave a catalytic amount of succinimide in the organic phase. The free sulfilimine catalytically rearranges at moderate temperatures in the presence of this succinimide catalyst to form MTA. The aqueous phase separated after neutralization of the sulfilimine hydrochloride salt contains succinimide and/or sodium succinimide which may be converted by the action of chlorine to N-chlorosuccinimide which in turn may be recycled to the first step in the process.

    摘要翻译： 本发明涉及一种由邻氨基三氟甲苯（OABT）制备2-（甲硫基甲基）-6-（三氟甲基）苯胺[MTA]的方法，采用经由亚硫酰亚胺中间体的单一溶剂转化。 通过在N-氯琥珀酰亚胺的存在下将二甲硫
    化物氧化加成到OABT中来制备盐酸亚硫酰胺盐。 将亚硫酰胺盐酸盐与氢氧化钠水溶液中和，随后进行相分离，得到含有游离的亚硫酰亚胺和通常含有琥珀酰亚胺和/或琥珀酰亚胺钠的水相的有机相。 在优选的实施方案中，相分离以这样一种方式进行，即在有机相中留下催化量的琥珀酰亚胺。 在该琥珀酰亚胺催化剂的存在下，游离的亚硫酰亚胺在中等温度下催化重排以形成MTA。 在中和硫酸亚胺盐酸盐后分离的水相含有琥珀酰亚胺和/或琥珀酰亚胺钠，其可以通过氯的作用转化为N-氯代琥珀酰亚胺，而N-氯代琥珀酰亚胺又可以再循环到该方法的第一步。