Container for receiving and safely storing radioactive materials and
method for tightly sealing the same
    1.
    发明授权
    Container for receiving and safely storing radioactive materials and method for tightly sealing the same 失效
    用于接收和安全储存放射性物质的容器及其密封方法

    公开(公告)号:US4673814A

    公开(公告)日:1987-06-16

    申请号:US416679

    申请日:1982-09-10

    CPC classification number: G21F5/12 G21F9/36 Y10S220/29

    Abstract: The invention is directed to a container for receiving and safely storing radioactive or other materials damaging to living organisms, especially such materials as vitrified radioactive fission products or irradiated nuclear reactor fuel elements. The container includes a vessel and a sealing cover. The vessel has a circular opening at one of its ends for receiving the materials to be stored therein, and a sealing cover is seated in this opening to tightly seal the container. In order to obtain a container of the kind which has the required high impermeability to gas, the open end of the inner bore of the vessel is widened to define a conical surface. A sealing cover is pressed into the vessel at this conical surfce. The sealing cover has a peripheral surface which converges toward the interior of the vessel and which has a taper corresponding to that of the conical surface of the vessel. The vessel wall and sealing cover are welded together by means of a fused-mass joint extending around the entire periphery of the cover. By means of the conical configuration of the upper end portion of the vessel and of the sealing cover, a considerably improved seal between the vessel wall and the sealing cover is obtained. A method for sealing the container is also disclosed.

    Abstract translation: 本发明涉及用于接收和安全地储存对生物体,特别是诸如玻璃化的放射性裂变产物或照射的核反应堆燃料元件的材料的放射性或其它材料的容器。 容器包括容器和密封盖。 该容器在其一端具有一个圆形开口,用于容纳待存储的材料,密封盖位于该开口中,以密封容器。 为了获得对气体具有所需的高不可渗透性的容器,容器的内孔的开口端被加宽以限定圆锥形表面。 密封盖在该锥形表面被压入容器中。 密封盖具有朝向容器内部会聚的周边表面,并且其具有对应于容器的锥形表面的锥度。 容器壁和密封盖通过围绕盖的整个周边延伸的熔合质量接头焊接在一起。 通过容器的上端部分和密封盖的圆锥形结构,获得容器壁和密封盖之间的显着改进的密封。 还公开了一种密封容器的方法。

    Method of making methacrylamides
    2.
    发明授权
    Method of making methacrylamides 失效
    制备甲基丙烯酰胺的方法

    公开(公告)号:US4675442A

    公开(公告)日:1987-06-23

    申请号:US709343

    申请日:1985-03-06

    CPC classification number: C07C231/02

    Abstract: What is disclosed is a method for making an amide of acrylic acid or of methacrylic acid by the reaction of an alkyl ester of acrylic acid or of methacrylic acid with an amine at a temperature between 50.degree. C. and 180.degree. C., whereby the reaction with the amine is carried out in the presence of a catalytic amount of a compound of a metal of Group IVB of the periodic table of the elements or of a compound of lead, zinc, or tantalum.

    Abstract translation: 公开的是通过丙烯酸或甲基丙烯酸的烷基酯与胺在50℃至180℃的温度下反应制备丙烯酸或甲基丙烯酸的酰胺的方法,其中 与胺的反应在催化量的元素周期表第IVB族金属化合物或铅,锌或钽化合物的存在下进行。

    Method for making cyanogen chloride
    6.
    发明授权
    Method for making cyanogen chloride 失效
    制造氯化氰的方法

    公开(公告)号:US3976754A

    公开(公告)日:1976-08-24

    申请号:US607599

    申请日:1975-08-25

    CPC classification number: C01C3/004

    Abstract: A method for making cyanogen chloride which comprises passing an approximately equimolar mixture of dicyan and chlorine over a charcoal catalyst at a temperature between 500.degree.C. and 950.degree.C. at a space velocity between 1000 and 10000 liters, measured at room temperature, per liter of catalyst and per hour.

    Abstract translation: 一种制备氯化氰的方法,其包括在500℃和950℃之间的温度下,在室温下测量的空气速度,在室温下测量二氰和氯的大约等摩尔的混合物,在一个木炭催化剂上, 升催化剂和每小时。

    Method for making isobutyric acid
    9.
    发明授权
    Method for making isobutyric acid 失效
    制备异丁酸的方法

    公开(公告)号:US4647696A

    公开(公告)日:1987-03-03

    申请号:US474799

    申请日:1983-03-14

    CPC classification number: C07C51/14 C07C67/38

    Abstract: What is disclosed is a continuous one-step method for the preparation of isobutyric acid or a lower alkyl ester thereof by the Koch synthesis, which method comprises reacting propylene, carbon monoxide, and water or a lower alcohol, in the gaseous and liquid phases, in the presence of hydrogen fluoride as a Koch catalyst, at a temperature between 80.degree. C. and 160.degree. C., at a dwell time of the liquid phase of less than 20 minutes, and with a high degree of backmixing, while maintaining the content of propylene in the reaction mixture at less than one percent by weight of the liquid phase, wherein all or part of the propylene, carbon monoxide, and water or lower alcohol can be replaced by binary addition compounds formed pairwise between these materials. In the alternative, isopropylformiate can be continuously rearranged in the presence of hydrogen fluoride to produce isobutyric acid.

    Abstract translation: 所公开的是通过Koch合成制备异丁酸或其低级烷基酯的连续一步法,该方法包括在气相和液相中使丙烯,一氧化碳和水或低级醇反应, 在作为Koch催化剂的氟化氢的存在下,在80℃至160℃的温度下,在液相的停留时间小于20分钟,并具有高度的回混,同时保持 反应混合物中丙烯的含量小于液相的1重量%,其中全部或部分丙烯,一氧化碳和水或低级醇可以由这些材料成对形成的二元加成化合物代替。 在替代方案中,异丙基甲酸酯可以在氟化氢的存在下连续重排以产生异丁酸。

    Polyarylene esters containing phosphorus
    10.
    发明授权
    Polyarylene esters containing phosphorus 失效
    含聚磷脂的聚亚芳基酯

    公开(公告)号:US4463159A

    公开(公告)日:1984-07-31

    申请号:US499526

    申请日:1983-05-31

    CPC classification number: C08G63/6926 C07F9/5325

    Abstract: What are disclosed are phosphorus-containing polyarylene esters,--O--A--O--CO--B--CO].sub.n,wherein A represents at least in part groups of the structure ##STR1## wherein x is 0 or 1 and R is aromatic or aliphatic, and wherein B represents either two different aromatic groups or at least one group with the structure --C.sub.6 H.sub.4 --R'--C.sub.6 H.sub.4 --, wherein R' is a bridging link of the group --O--, --S--, --SO.sub.2 --, --CO--, or isopropylidene, and wherein n is greater than 20, which esters have a phosphorus content of over 1 weight percent, are distinguished by improved thermoplastic processability, and are prepared by condensation of HO--A--OH, for example with ClCO--B--COCl in the presence of a base.

    Abstract translation: 所公开的是含磷聚亚芳基酯-OAO-CO-B-CO] n,其中A表示至少部分结构单元组,其中x是0或1,R是芳族或脂族的,其中 B表示两个不同的芳族基团或至少一个具有结构-C 6 H 4 -R'-C 6 H 4 - 的基团,其中R'是-O - , - S - , - SO 2 - , - CO- 或异丙叉,并且其中n大于20,所述酯的磷含量大于1重量%,其特征在于改进的热塑性加工性,并且通过HO-A-OH例如与ClCO-B-COCl 在一个基地的存在。

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