Method for the continuous production of silicon oxide powder
    4.
    发明授权
    Method for the continuous production of silicon oxide powder 有权
    连续生产氧化硅粉末的方法

    公开(公告)号:US06821495B2

    公开(公告)日:2004-11-23

    申请号:US09773677

    申请日:2001-02-02

    IPC分类号: C01B3320

    摘要: A silicon oxide powder can be continuously prepared by feeding a raw material powder mixture containing silicon dioxide powder into a reaction chamber (2) at a temperature of 1,100-1,600° C., to produce a silicon oxide gas, transferring the silicon oxide gas to a deposition chamber (11) through a transfer conduit (10) maintained at a temperature of from higher than 1,000° C. to 1,300° C., causing silicon oxide to deposit on a substrate (13) which is disposed and cooled in the deposition chamber, scraping the silicon oxide deposit, and recovering the deposit in a recovery chamber (18). The method and apparatus is capable of continuous and stable production of amorphous silicon oxide powder of high purity.

    摘要翻译: 可以通过在1100〜1600℃的温度下将含有二氧化硅粉末的原料粉末混合物进料到反应室(2)中来连续制备氧化硅粉末,以产生氧化硅气体,将氧化硅气体转移到 沉积室(11),其通过保持在高于1,000℃至1300℃的温度的转移管道(10),使得氧化硅沉积在沉积物中的基底(13)上,所述基底(13)在沉积物中被设置和冷却 刮除氧化硅沉积物,并将沉积物回收到回收室(18)中。 该方法和装置能够连续且稳定地生产高纯度的无定形氧化硅粉末。

    Apparatus for the continuous production of silicon oxide powder
    5.
    发明授权
    Apparatus for the continuous production of silicon oxide powder 有权
    用于连续生产氧化硅粉末的设备

    公开(公告)号:US07431899B2

    公开(公告)日:2008-10-07

    申请号:US10784259

    申请日:2004-02-24

    IPC分类号: C01B33/20

    摘要: A silicon oxide powder can be continuously prepared by feeding a raw material powder mixture containing silicon dioxide powder into a reaction chamber (2) at a temperature of 1,100-1,600° C., to produce a silicon oxide gas, transferring the silicon oxide gas to a deposition chamber (11) through a transfer conduit (10) maintained at a temperature of from higher than 1,000° C. to 1,300° C., causing silicon oxide to deposit on a substrate (13) which is disposed and cooled in the deposition chamber, scraping the silicon oxide deposit, and recovering the deposit in a recovery chamber (18). The method and apparatus is capable of continuous and stable production of amorphous silicon oxide powder of high purity.

    摘要翻译: 可以通过在1100〜1600℃的温度下将含有二氧化硅粉末的原料粉末混合物进料到反应室(2)中来连续制备氧化硅粉末,以产生氧化硅气体,将氧化硅气体转移到 沉积室(11),其通过保持在高于1,000℃至1300℃的温度的转移管道(10),使得氧化硅沉积在沉积物中的基底(13)上,所述基底(13)在沉积物中被设置和冷却 刮擦氧化硅沉积物,并将沉积物回收到回收室(18)中。 该方法和装置能够连续且稳定地生产高纯度的无定形氧化硅粉末。

    Catalyst for living radical polymerization and polymerization method
    6.
    发明授权
    Catalyst for living radical polymerization and polymerization method 有权
    催化剂用于活性自由基聚合和聚合方法

    公开(公告)号:US09546226B2

    公开(公告)日:2017-01-17

    申请号:US13388811

    申请日:2010-05-10

    摘要: Provided is a low-cost, highly active, environmentally friendly living radical polymerization catalyst which does not require a radical initiator. An organic compound having an oxidation-reduction capability is used as a catalyst. Even if a radical initiator is not used, a monomer can be subjected to a radical polymerization to obtain a polymer having narrow molecular weight distribution. The cost of the living radical polymerization can be remarkably reduced. It is made possible to prevent adverse effects of using a radical initiator. The present invention is significantly more environmentally friendly and economically excellent than conventional living radical polymerization methods, due to advantages of the catalyst such as low toxicity of the catalyst, low amount of the catalyst necessary, high solubility of the catalyst, mild reaction conditions, and no coloration/no odor (which do not require a post-treatment for a molded article), etc.

    摘要翻译: 提供了不需要自由基引发剂的低成本,高活性,环保的活性自由基聚合催化剂。 使用具有氧化还原能力的有机化合物作为催化剂。 即使不使用自由基引发剂,也可以对单体进行自由基聚合,得到分子量分布窄的聚合物。 活性自由基聚合的成本可以显着降低。 可以防止使用自由基引发剂的不利影响。 由于催化剂的优点,催化剂的低毒性,必需的催化剂量低,催化剂的溶解度高,反应条件温和,反应条件好,因此本发明的环保性和经济性优于常规的活性自由基聚合方法。 无着色/无异味(不需要后处理成型品)等

    Method for producing tolylene diisocyanate
    8.
    发明授权
    Method for producing tolylene diisocyanate 有权
    甲苯二异氰酸酯的制备方法

    公开(公告)号:US08748654B2

    公开(公告)日:2014-06-10

    申请号:US14115852

    申请日:2012-04-06

    摘要: A method for producing tolylene diisocyanate includes: mixing a first diaminotoluene containing 2,4-diaminotoluene and 2,6-diaminotoluene at a first isomer ratio and a second diaminotoluene containing 2,4-diaminotoluene and/or 2,6-diaminotoluene at a second isomer ratio that is different from the first isomer ratio so as to prepare mixed diaminotoluene; producing tolylene dicarbamate by reaction of the mixed diaminotoluene, urea and/or N-unsubstituted carbamic acid ester and alcohol; and thermally decomposing the tolylene dicarbamate.

    摘要翻译: 一种制备甲苯二异氰酸酯的方法包括:以第一异构体比例混合含有2,4-二氨基甲苯和2,6-二氨基甲苯的第一二氨基甲苯和第二异构体含有2,4-二氨基甲苯和/或2,6-二氨基甲苯的第二二氨基甲苯 异构体比例与第一异构体比例不同,以制备混合的二氨基甲苯; 通过混合的二氨基甲苯,脲和/或N-未取代的氨基甲酸酯和醇的反应制备甲苯二甲氨基甲酸酯; 并分解甲苯二氨基甲酸酯。

    Catalyst for living radical polymerization
    10.
    发明授权
    Catalyst for living radical polymerization 有权
    活性自由基聚合催化剂

    公开(公告)号:US08575285B2

    公开(公告)日:2013-11-05

    申请号:US13062688

    申请日:2009-09-08

    摘要: Provided is a catalyst used for a living radical polymerization method, which contains a central element consisting of carbon and at least one halogen atom binding to the central element. Further, a hydrocarbon compound can be used as a catalyst precursor. A monomer having a radical-reactive unsaturated bond is subjected to a radical polymerization reaction in the presence of the catalyst, consequently a polymer having narrow molecular weight distribution can be obtained, and thus the cost of the living radical polymerization can be remarkably reduced. The present invention is significantly more environmentally friendly and economically excellent than conventional living radical polymerization methods, due to advantages such as low toxicity of the catalyst, low amount of the catalyst used, high solubility of the catalyst, mild reaction conditions, and no coloration/no odor (no need of any post-treatments for a molded article), and the like.

    摘要翻译: 提供了用于活性自由基聚合法的催化剂,其包含由碳和与中心元素结合的至少一个卤素原子组成的中心元素。 此外,可以使用烃化合物作为催化剂前体。 具有自由基反应性不饱和键的单体在催化剂的存在下进行自由基聚合反应,因此可以获得具有窄分子量分布的聚合物,从而可显着降低活性自由基聚合的成本。 本发明由于催化剂的毒性低,催化剂用量少,催化剂溶解性高,反应条件温和,无着色/无色性等优点,比现有的活性自由基聚合法更具环保性和经济性, 无异味(不需要对成形品进行后处理)等。