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公开(公告)号：US6110987A
公开(公告)日：2000-08-29
申请号：US893390
申请日：1997-07-11
CPC分类号： G03F7/029 , C08F2/50 , C09B11/12 , C09B17/00 , C09B21/00 , C09B23/04 , C09B23/105 , C09D11/101 , C09D4/00
摘要： A photocurable composition comprising an ultraviolet radical polymerization initiator, a cationic dye with absorptions in the visible light region, a quaternary boron salt and optionally a polymerization accelerator, is irradiated with ultraviolet light and visible light either simultaneously or separately, to achieve adequate hardening in air of both the surface and the interior of the cured product, and to provide a cured product with an excellent appearance and without production of coloring substances derived from the polymerization initiator.
摘要翻译： 同时或分别用紫外光和可见光照射包含紫外线自由基聚合引发剂，在可见光区吸收的阳离子染料，季硼盐和任选的聚合促进剂的光固化组合物，以在空气中达到充分的硬化 的固化物的表面和内部，并且提供具有优异外观的固化产物，并且不产生源自聚合引发剂的着色物质。
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公开(公告)号：US6165686A
公开(公告)日：2000-12-26
申请号：US81995
申请日：1998-05-21
CPC分类号： G03F7/029 , C09D4/06 , Y10S430/117 , C08F290/14
摘要： Color reversion of photocured products which have been photocured with cationic dyes and quaternary organo borates can be notably suppressed by addition of phenolic compounds, aromatic thiol compounds, amine compounds and/or phosphorous compounds.
摘要翻译： 通过添加酚类化合物，芳族硫醇化合物，胺化合物和/或磷化合物，可以显着地抑制用阳离子染料和季有机硼酸盐光固化的光固化产物的颜色反转。
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公开(公告)号：US06211260B1
公开(公告)日：2001-04-03
申请号：US09185583
申请日：1998-11-04
IPC分类号： C08F248
CPC分类号： C09D5/004 , C09D4/00 , C09D4/06 , C08F220/18 , C08F290/064
摘要： A photocurable paint composition for road markings is disclosed, comprising (A) a compound having an ethylenically unsaturated group, (B) a filler, (C) a cationic dye represented by formula (1): D+&Circlesolid;A1− (1) (wherein D+ represents a cation having an absorption maximum wavelength in the wavelength region of from 400 to 1,200 nm, and A1− represents an optional anion), (D) a quaternary organic borate-type sensitizer represented by formula (2): (wherein R1, R2, R3 and R4 each independently represents an alkyl group, an aryl group, an aralkyl group, an alkenyl group, an alkynyl group, a silyl group, a heterocyclic group or a halogen atom, and Z+ represents an optional cation) and (E) an ultraviolet radical polymerization initiator capable of generating a radical upon absorption of light at a wavelength of 400 nm or less, or additionally comprising (F) glass beads.
摘要翻译： 公开了一种用于道路标线的光固化涂料组合物，其包含（A）具有烯属不饱和基团的化合物，（B）填料，（C）由式（1）表示的阳离子染料:(其中D +表示具有吸收的阳离子 400〜1200nm的波长区域的最大波长，A1-表示任意的阴离子），（D）式（2）表示的季有机硼酸盐型增感剂:(式中，R1，R2，R3，R4分别独立地表示 表示烷基，芳基，芳烷基，烯基，炔基，甲硅烷基，杂环基或卤素原子，Z +表示任选的阳离子）和（E）紫外线自由基聚合引发剂 在400nm或更小的波长下吸收光，或另外包含（F）玻璃珠而产生自由基。
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4.发明授权Photocurable prepreg sheet for waterproofing, method and apparatus for production of prepreg sheet, and waterproofing method using the sheet 失效用于防水的光固化性预浸片，用于生产预浸片的方法和设备以及使用该片的防水方法公开(公告)号：US06316089B1
公开(公告)日：2001-11-13
申请号：US09205227
申请日：1998-12-04
申请人： Kazuo Ohtani , Tomio Yamamoto , Hidetake Sendai , Toshihiko Kadota , Shuichi Sugita , Hirotoshi Kamata , Takeo Watanabe
发明人： Kazuo Ohtani , Tomio Yamamoto , Hidetake Sendai , Toshihiko Kadota , Shuichi Sugita , Hirotoshi Kamata , Takeo Watanabe
IPC分类号： C08F29006
CPC分类号： C08J3/243 , B29C70/504 , C08J5/24 , C08J2367/06 , Y10T428/1359 , Y10T428/24124 , Y10T428/249942 , Y10T428/24995
摘要： A photocurable prepreg sheet for waterproofing includes (1) a fiber-reinforced resin layer which comprises a sheet-shaped inorganic or organic fibrous reinforcing material impregnated with a resin composition comprising: (A) an unsaturated polyester resin and/or vinyl ester resin: 100 parts by weight, and (B) at least two photopolymerization initiators having photosensitivity in different wavelength ranges from ultraviolet range to near infrared range: 0.01 to 10 parts by weight, and which is treated with light of a specific wavelength to thereby undergo prepolymerization which causes at least one of the polymerization initiators and radical-polymerizable unsaturated groups to remain partially intact; and (2) film which covers an upper surface and a back surface of the fiber-reinforced resin layer. The waterproofing material does not require resin impregnation work, can be installed within a short time with successful resin setting, is free form the risk and cumbersome procedure which are caused when a peroxide catalyst is directly handled, and permits adjustment of the pot life. Also disclosed are method and apparatus for production of the prepreg sheet, and waterproofing method using the sheet.
摘要翻译： 用于防水的光固化性预浸料片包括（1）纤维增强树脂层，其包含浸渍有树脂组合物的片状无机或有机纤维增强材料，所述树脂组合物包含：（A）不饱和聚酯树脂和/或乙烯基酯树脂：100 （B）至少两种具有紫外线范围至近红外范围的不同波长范围内的光敏性的光聚合引发剂：0.01〜10重量份，用特定波长的光进行处理，从而进行预聚合， 至少一种聚合引发剂和可自由基聚合的不饱和基团保持部分完整; 和（2）覆盖纤维增强树脂层的上表面和后表面的膜。 防水材料不需要树脂浸渍工作，可以在短时间内安装成功的树脂固化，自由形成直接处理过氧化物催化剂时引起的风险和麻烦的程序，并允许调整适用期。 还公开了制备预浸渍片材的方法和设备，以及使用该片材的防水方法。
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公开(公告)号：US06207726B1
公开(公告)日：2001-03-27
申请号：US09247824
申请日：1999-02-11
申请人： Kazuo Ohtani , Tomio Yamamoto , Hidetake Sendai , Shuichi Sugita , Hirotoshi Kamata , Takeo Watanabe
发明人： Kazuo Ohtani , Tomio Yamamoto , Hidetake Sendai , Shuichi Sugita , Hirotoshi Kamata , Takeo Watanabe
IPC分类号： C08F250
摘要： A photocurable prepreg composition which is characterized by easy control of a B stage state of a thermosetting resin such as an unsaturated polyester resin or an epoxy acrylate resin, excellent storage stability, and remarkable curability after being shaped; as well as a production method therefor. A photocurable prepreg composition which contains an unsaturated polyester resin and/or an epoxy acrylate resin; at least two photopolymerization initiators with photosensitivity in different wavelength ranges; and an inorganic or an organic fiber-reinforcing material and/or filler, and which composition is treated with light of a specific wavelength such that at least one photopolymerization initiator and radical-polymerizable unsaturated groups remain partially in said resin; a production method therefor; and formed articles produced therefrom.
摘要翻译： 光固化性预浸料组合物，其特征在于容易控制热固性树脂如不饱和聚酯树脂或环氧丙烯酸酯树脂的B阶段状态，优异的储存稳定性和成形后的显着的固化性; 以及其生产方法。 含有不饱和聚酯树脂和/或环氧丙烯酸酯树脂的光固化预浸料组合物; 至少两种具有不同波长范围光敏性的光聚合引发剂; 和无机或有机纤维增强材料和/或填料，并且该组合物用特定波长的光处理，使得至少一个光聚合引发剂和可自由基聚合的不饱和基团部分保留在所述树脂中; 一种生产方法; 和由其制成的成型制品。
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公开(公告)号：US5852067A
公开(公告)日：1998-12-22
申请号：US749975
申请日：1996-11-15
申请人： Hajime Sukejima , Shinji Tomita , Shuichi Sugita , Kazuhiko Ooga
发明人： Hajime Sukejima , Shinji Tomita , Shuichi Sugita , Kazuhiko Ooga
IPC分类号： C08F290/02 , C08F2/50 , C08F283/01 , C08F290/00 , C08F290/06 , C08F290/08 , C08L63/10 , C08L67/06 , C09D4/00 , C09D4/02 , C09D5/34 , C08L1/12 , C08L67/07
CPC分类号： C08L67/06 , C08F283/01 , C08F290/064 , C08L63/10
摘要： A near infrared rays-curing putty composition containing (A) a polymerizable ethylenically unsaturated group-containing resin, (B) a polymerizable ethylenically unsaturated compound and (C) a near infrared rays polymerization initiator, said near infrared rays polymerization initiator (C) being a near infrared rays-absorbing cationic dye and a resin powder consisting of gelation polymer fine particles.
摘要翻译： 一种含有（A）可聚合烯属不饱和基团的树脂，（B）可聚合烯属不饱和化合物和（C）近红外线聚合引发剂的近红外线固化油灰组合物，所述近红外线聚合引发剂（C）为 近红外线吸收阳离子染料和由凝胶化聚合物细颗粒组成的树脂粉末。
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公开(公告)号：US06329442B1
公开(公告)日：2001-12-11
申请号：US09708463
申请日：2000-11-09
IPC分类号： C08F250
CPC分类号： C08F299/0464 , C08F4/12 , C08F283/01 , Y10T428/30 , Y10T428/31511 , Y10T428/31786 , Y10T428/31935 , C08F4/06
摘要： A curable composite material composition comprising (A) a polymerizable unsaturated compound, (B) a fiber reinforcing material and/or fiber, and (C) a polymerization initiator comprising an organic boron compound represented by the general formula (1) wherein R1, R2, R3 and R4 each independently represent an alkyl, aryl, allyl, aralkyl, alkenyl, alkynyl, silyl or heterocyclic group, a halogen atom, or a substituted alkyl, substituted aryl, substituted allyl, substituted aralkyl, substituted alkenyl, substituted alkynyl or substituted silyl group, and Z+ represents a cation, and an acidic compound, as well as a curing process for the curable composite material composition which includes irradiating and/or heating the curable composite material composition.
摘要翻译： 一种可固化复合材料组合物，其包含（A）可聚合不饱和化合物，（B）纤维增强材料和/或纤维，和（C）包含由通式（1）表示的有机硼化合物的聚合引发剂，其中R1，R2 ，R 3和R 4各自独立地表示烷基，芳基，烯丙基，芳烷基，烯基，炔基，甲硅烷基或杂环基，卤素原子或取代的烷基，取代的芳基，取代的烯丙基，取代的芳烷基，取代的烯基，取代的炔基或取代的 甲硅烷基，Z +表示阳离子和酸性化合物，以及包含照射和/或加热固化性复合材料组合物的固化性复合材料组合物的固化方法。
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公开(公告)号：US06171700B2
公开(公告)日：2001-01-09
申请号：US08813237
申请日：1997-03-07
IPC分类号： C08K704
CPC分类号： C08F299/0464 , C08F4/12 , C08F283/01 , Y10T428/30 , Y10T428/31511 , Y10T428/31786 , Y10T428/31935 , C08F4/06
摘要： A curable composite material composition comprising (A) a polymerizable unsaturated compound, (B) a fiber reinforcing material and/or fiber, and (C) a polymerization initiator comprising an organic boron compound represented by the general formula (1) wherein R1, R2, R3 and R4 each independently represent an alkyl, aryl, allyl, aralkyl, alkenyl, alkynyl, silyl or heterocyclic group, a halogen atom, or a substituted alkyl, substituted aryl, substituted allyl, substituted aralkyl, substituted alkenyl, substituted alkynyl or substituted silyl group, and Z+ represents a cation, and an acidic compound, as well as a curing process for the curable composite material composition which includes irradiating and/or heating the curable composite material composition.
摘要翻译： 一种可固化复合材料组合物，其包含（A）可聚合不饱和化合物，（B）纤维增强材料和/或纤维，和（C）包含由通式（1）表示的有机硼化合物的聚合引发剂，其中R1，R2 ，R 3和R 4各自独立地表示烷基，芳基，烯丙基，芳烷基，烯基，炔基，甲硅烷基或杂环基，卤素原子或取代的烷基，取代的芳基，取代的烯丙基，取代的芳烷基，取代的烯基，取代的炔基或取代的 甲硅烷基，Z +表示阳离子和酸性化合物，以及包含照射和/或加热固化性复合材料组合物的固化性复合材料组合物的固化方法。
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公开(公告)号：US08425790B2
公开(公告)日：2013-04-23
申请号：US12933938
申请日：2009-01-27
CPC分类号： H05K3/061 , C09D11/101 , C09D11/30 , H05K3/0076 , H05K2203/013
摘要： An ink composition for ink jet printing is provided which gives a cured object excellent in adhesion to metallic plates, resistance to etchants, and alkali removability and can be stably ejected with an ink jet apparatus. The ink jet composition for etching resists has a viscosity at 25° C. of 3-50 mPa s and includes monomers comprising: either a polymerizable phosphoric ester compound represented by general formula (I); a polyfunctional monomer having two or more ethylenic double-bond groups per molecule and having no phosphoric ester group, the content of the ethylenic double-bond groups being 4×10−3 to 8×10−3 mol/g; and a monofunctional monomer having one ethylenic double-bond group per molecule and having neither phosphoric ester group nor carboxy group. In the formula, X represents C1-3 alkylene, Y represents C2-3 alkylene, and R represents hydrogen or methyl.
摘要翻译： 提供一种用于喷墨印刷的油墨组合物，其提供了对金属板的粘附性优异，耐蚀刻剂和碱可除去性优异的固化物，并且可以用喷墨设备稳定地喷射。 用于抗蚀剂的喷墨组合物在25℃下的粘度为3-50mPa·s，并且包括单体，其包含：由通式（I）表示的可聚合磷酸酯化合物; 每分子具有2个以上的烯属双键基并且不具有磷酸酯基的多官能单体，烯键式双键基团的含量为4×10 -3〜8×10 -3 mol / g; 和每分子具有一个烯属双键基并且既不具有磷酸酯基也不具有羧基的单官能单体。 在该式中，X表示C1-3亚烷基，Y表示C2-3亚烷基，R表示氢或甲基。
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10.发明授权公开(公告)号：US07888859B2
公开(公告)日：2011-02-15
申请号：US11817271
申请日：2006-02-10
申请人： Shuichi Sugita , Hiroshi Kita , Hideo Taka
发明人： Shuichi Sugita , Hiroshi Kita , Hideo Taka
IPC分类号： H05B33/00
CPC分类号： H01L51/004 , C09K11/06 , C09K2211/1029 , C09K2211/1044 , C09K2211/1059 , C09K2211/1092 , C09K2211/186 , C09K2211/188 , H01L51/0059 , H01L51/0062 , H01L51/0077 , H01L51/0081 , H01L51/0084 , H01L51/0085 , H01L51/0094 , H01L51/5012 , H05B33/14 , Y10S428/917
摘要： In an organic electroluminescence element which incorporates a substrate having thereon an anode and a cathode and which incorporates a plurality of organic layers between the aforesaid anode and cathode, wherein at least one of the aforesaid organic layers is a first organic layer incorporating a compound having at most 10 repeating units, the first organic layer being prepared by coating the compound having at least one polymerizable group, followed by polymerization.
摘要翻译： 在一种有机电致发光元件中，该有机电致发光元件包括其上具有阳极和阴极的基底，并且在上述阳极和阴极之间并入多个有机层，其中至少一个上述有机层是第一有机层， 最多10个重复单元，第一有机层通过涂布具有至少一个可聚合基团的化合物，然后聚合制备。
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